UnivTrevesV1, Main, Curation, bibRecord, 002745

Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry

Identifieur interne : 002745 ( Main/Curation ); précédent : 002744; suivant : 002746

Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry

Auteurs : W. Wagner [États-Unis] ; S. Sander [États-Unis] ; G. Henze [États-Unis]

Source :

Fresenius' Journal of Analytical Chemistry [ 0937-0633 ] ; 1996-01-01.

RBID : ISTEX:F670FBF9D0A3AF0C2F6AD9CE22B2974BEF8E41D5

Descripteurs français

Pascal (Inist)
- Adsorption, Analyse chimique, Analyse trace, Antimoine, Complexation, Coordinat organique, Limite détection, Voltammétrie redissolution anodique.
Wicri :
- topic : Antimoine.

English descriptors

KwdEn :
- Adsorption, Anodic stripping voltammetry, Antimony, Chemical analysis, Complexation, Detection limit, Organic ligand, Trace analysis.

Abstract

Abstract.: A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of +100 mV from hydrochloric acid (pH=3.0) solution. Sb(V) can be determined using an accumulation potential of −500 mV in HCl (pH=1.0) solution. The peak potentials in the stripping voltammograms are −400 mV for Sb(III) and −140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.

Url:

https://api.istex.fr/document/F670FBF9D0A3AF0C2F6AD9CE22B2974BEF8E41D5/fulltext/pdf

DOI: 10.1007/s002169600002

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Le document en format XML

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<front><div type="abstract" xml:lang="en">Abstract.: A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of +100 mV from hydrochloric acid (pH=3.0) solution. Sb(V) can be determined using an accumulation potential of −500 mV in HCl (pH=1.0) solution. The peak potentials in the stripping voltammograms are −400 mV for Sb(III) and −140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.</div>
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<front><div type="abstract" xml:lang="en">Abstract.: A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of +100 mV from hydrochloric acid (pH=3.0) solution. Sb(V) can be determined using an accumulation potential of −500 mV in HCl (pH=1.0) solution. The peak potentials in the stripping voltammograms are −400 mV for Sb(III) and −140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.</div>
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Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry

Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry

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Abstract

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