UnivTrevesV1, PascalFrancis, Corpus, bibRecord, 001480

Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry

Identifieur interne : 001480 ( PascalFrancis/Corpus ); précédent : 001479; suivant : 001481

Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry

Auteurs : W. Wagner ; S. Sander ; G. Henze

Source :

Fresenius' journal of analytical chemistry [ 0937-0633 ] ; 1996.

RBID : Pascal:96-0044162

Descripteurs français

Pascal (Inist)
- Analyse chimique, Adsorption, Voltammétrie redissolution anodique, Antimoine, Limite détection, Analyse trace, Complexation, Coordinat organique.

English descriptors

KwdEn :
- Adsorption, Anodic stripping voltammetry, Antimony, Chemical analysis, Complexation, Detection limit, Organic ligand, Trace analysis.

Abstract

A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of + 100mV from hydrochloric acid (pH = 3.0) solution. Sb(V) can be determined using an accumulation potential of - 500 mV in HCI (pH = 1.0) solution. The peak potentials in the stripping voltammograms are - 400 mV for Sb(III) and - 140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

A01	`01`	`1`		`@0 0937-0633`
A03		`1`		`@0 Fresenius' j. anal. chem.`
A05				`@2 354`
A06				`@2 1`
A08	`01`	`1`	`ENG`	`@1 Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry`
A11	`01`	`1`		`@1 WAGNER (W.)`
A11	`02`	`1`		`@1 SANDER (S.)`
A11	`03`	`1`		`@1 HENZE (G.)`
A14	`01`			`@1 Univ. Trier, Univ. Kaiserslautern und Abt. anorganische analytische Chemie @2 54228 Trier @3 DEU`
A20				`@1 11-15`
A21				`@1 1996`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 853 @5 354000054958420030`
A44				`@0 0000`
A45				`@0 7 ref.`
A47	`01`	`1`		`@0 96-0044162`
A60				`@1 P`
A61				`@0 A`
A64	`01`	`1`		`@0 Fresenius' journal of analytical chemistry`
A66	`01`			`@0 DEU`
C01	`01`		`ENG`	@0 A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of + 100mV from hydrochloric acid (pH = 3.0) solution. Sb(V) can be determined using an accumulation potential of - 500 mV in HCI (pH = 1.0) solution. The peak potentials in the stripping voltammograms are - 400 mV for Sb(III) and - 140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.
C02	`01`	`X`		`@0 001C04E`
C03	`01`	`1`	`FRE`	`@0 Analyse chimique @3 P @5 01`
C03	`01`	`1`	`ENG`	`@0 Chemical analysis @3 P @5 01`
C03	`02`	`1`	`FRE`	`@0 Adsorption @5 51`
C03	`02`	`1`	`ENG`	`@0 Adsorption @5 51`
C03	`03`	`X`	`FRE`	`@0 Voltammétrie redissolution anodique @5 52`
C03	`03`	`X`	`ENG`	`@0 Anodic stripping voltammetry @5 52`
C03	`03`	`X`	`GER`	`@0 Inversvoltammetrie @5 52`
C03	`03`	`X`	`SPA`	`@0 Voltametría redisolución anódica @5 52`
C03	`04`	`1`	`FRE`	`@0 Antimoine @1 ANA @2 NC @2 FX @2 FR @5 53`
C03	`04`	`1`	`ENG`	`@0 Antimony @1 ANA @2 NC @2 FX @2 FR @5 53`
C03	`05`	`X`	`FRE`	`@0 Limite détection @5 54`
C03	`05`	`X`	`ENG`	`@0 Detection limit @5 54`
C03	`05`	`X`	`GER`	`@0 Nachweisgrenze @5 54`
C03	`05`	`X`	`SPA`	`@0 Límite detección @5 54`
C03	`06`	`1`	`FRE`	`@0 Analyse trace @5 55`
C03	`06`	`1`	`ENG`	`@0 Trace analysis @5 55`
C03	`07`	`1`	`FRE`	`@0 Complexation @5 56`
C03	`07`	`1`	`ENG`	`@0 Complexation @5 56`
C03	`08`	`X`	`FRE`	`@0 Coordinat organique @5 57`
C03	`08`	`X`	`ENG`	`@0 Organic ligand @5 57`
C03	`08`	`X`	`SPA`	`@0 Ligando orgánico @5 57`
N21				`@1 022`

Format Inist (serveur)

NO :	PASCAL 96-0044162 INIST
ET :	Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry
AU :	WAGNER (W.); SANDER (S.); HENZE (G.)
AF :	Univ. Trier, Univ. Kaiserslautern und Abt. anorganische analytische Chemie/54228 Trier/Allemagne
DT :	Publication en série; Niveau analytique
SO :	Fresenius' journal of analytical chemistry; ISSN 0937-0633; Allemagne; Da. 1996; Vol. 354; No. 1; Pp. 11-15; Bibl. 7 ref.
LA :	Anglais
EA :	A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of + 100mV from hydrochloric acid (pH = 3.0) solution. Sb(V) can be determined using an accumulation potential of - 500 mV in HCI (pH = 1.0) solution. The peak potentials in the stripping voltammograms are - 400 mV for Sb(III) and - 140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.
CC :	001C04E
FD :	Analyse chimique; Adsorption; Voltammétrie redissolution anodique; Antimoine; Limite détection; Analyse trace; Complexation; Coordinat organique
ED :	Chemical analysis; Adsorption; Anodic stripping voltammetry; Antimony; Detection limit; Trace analysis; Complexation; Organic ligand
GD :	Inversvoltammetrie; Nachweisgrenze
SD :	Voltametría redisolución anódica; Límite detección; Ligando orgánico
LO :	INIST-853.354000054958420030
ID :	96-0044162

Links to Exploration step

Pascal:96-0044162

Le document en format XML

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<front><div type="abstract" xml:lang="en">A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of + 100mV from hydrochloric acid (pH = 3.0) solution. Sb(V) can be determined using an accumulation potential of - 500 mV in HCI (pH = 1.0) solution. The peak potentials in the stripping voltammograms are - 400 mV for Sb(III) and - 140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.</div>
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<fC01 i1="01" l="ENG"><s0>A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of + 100mV from hydrochloric acid (pH = 3.0) solution. Sb(V) can be determined using an accumulation potential of - 500 mV in HCI (pH = 1.0) solution. The peak potentials in the stripping voltammograms are - 400 mV for Sb(III) and - 140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.</s0>
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<ET>Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry</ET>
<AU>WAGNER (W.); SANDER (S.); HENZE (G.)</AU>
<AF>Univ. Trier, Univ. Kaiserslautern und Abt. anorganische analytische Chemie/54228 Trier/Allemagne</AF>
<DT>Publication en série; Niveau analytique</DT>
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<EA>A sensitive and selective adsorption stripping voltammetric (AdSV) method for the determination of antimony using chloranilic acid (2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone) as complexing reagent is described. The conditions under which its species of both oxidation states, Sb(III) and Sb(V), can be detected have been established. Sb(III) can be adsorbed onto the hanging mercury drop electrode (HMDE) using an accumulation potential of + 100mV from hydrochloric acid (pH = 3.0) solution. Sb(V) can be determined using an accumulation potential of - 500 mV in HCI (pH = 1.0) solution. The peak potentials in the stripping voltammograms are - 400 mV for Sb(III) and - 140 mV for antimony (V). The detection limits are 210 ng/L for Sb(III) with 5 min pre-concentration and 560 ng/L for Sb(V) with 10 min pre-concentration. The method is applicable to the trace analysis and speciation of antimony in water samples and phosphoric acid.</EA>
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Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry

Trace analysis of antimony (III) and antimony (V) by adsorptive stripping voltammetry

Source :

Descripteurs français

English descriptors

Abstract

Notice en format standard (ISO 2709)

Format Inist (serveur)

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri