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Determination of some heavy metals in food and environmental samples by flame atomic absorption spectrometry after coprecipitation

Identifieur interne : 000237 ( Pascal/Corpus ); précédent : 000236; suivant : 000238

Determination of some heavy metals in food and environmental samples by flame atomic absorption spectrometry after coprecipitation

Auteurs : Mustafa Soylak ; Ayse Aydin

Source :

RBID : Pascal:11-0322576

Descripteurs français

English descriptors

Abstract

A novel preconcentration procedure based coprecipitation of Cu(II), Co(II), Cd(II), Ni(II), Mn(II), Fe(III) and PB(II) on thulium hydroxide precipitate has been presented prior to flame atomic absorption spectrometric determination of them in environmental samples. The analytical parameters that influenced the quantitative coprecipitation of analytes including amount of thulium, pH, duration time, etc. were investigated. The effects of alkali, earth alkali, and some transition metals on the recoveries were also studied. Under the optimized conditions, the detection limits (3 sigma, N =10) for the analytes were in the range of 0.1-1.6 μg/L, respectively. The validation of the presented coprecipitation method was checked by the analysis of certified reference materials (TMDA 54.4 fortified lake water and HR-1 Humber river sediment). The proposed coprecipitation method has been successfully applied for the determination of traces of copper, cobalt, cadmium, nickel, manganese, iron and lead in food and environmental samples.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

pA  
A01 01  1    @0 0278-6915
A02 01      @0 FCTOD7
A03   1    @0 Food chem. toxicol.
A05       @2 49
A06       @2 6
A08 01  1  ENG  @1 Determination of some heavy metals in food and environmental samples by flame atomic absorption spectrometry after coprecipitation
A11 01  1    @1 SOYLAK (Mustafa)
A11 02  1    @1 AYDIN (Ayse)
A14 01      @1 University of Erciyes, Faculty of Science, Chemistry Dept @2 38039 Kayseri @3 TUR @Z 1 aut. @Z 2 aut.
A20       @1 1242-1248
A21       @1 2011
A23 01      @0 ENG
A43 01      @1 INIST @2 10616 @5 354000191617860080
A44       @0 0000 @1 © 2011 INIST-CNRS. All rights reserved.
A45       @0 1 p.1/4
A47 01  1    @0 11-0322576
A60       @1 P
A61       @0 A
A64 01  1    @0 Food and chemical toxicology
A66 01      @0 GBR
C01 01    ENG  @0 A novel preconcentration procedure based coprecipitation of Cu(II), Co(II), Cd(II), Ni(II), Mn(II), Fe(III) and PB(II) on thulium hydroxide precipitate has been presented prior to flame atomic absorption spectrometric determination of them in environmental samples. The analytical parameters that influenced the quantitative coprecipitation of analytes including amount of thulium, pH, duration time, etc. were investigated. The effects of alkali, earth alkali, and some transition metals on the recoveries were also studied. Under the optimized conditions, the detection limits (3 sigma, N =10) for the analytes were in the range of 0.1-1.6 μg/L, respectively. The validation of the presented coprecipitation method was checked by the analysis of certified reference materials (TMDA 54.4 fortified lake water and HR-1 Humber river sediment). The proposed coprecipitation method has been successfully applied for the determination of traces of copper, cobalt, cadmium, nickel, manganese, iron and lead in food and environmental samples.
C02 01  X    @0 002B03L05
C02 02  X    @0 002B03H
C03 01  X  FRE  @0 Dosage @5 02
C03 01  X  ENG  @0 Assay @5 02
C03 01  X  SPA  @0 Dosificación @5 02
C03 02  X  FRE  @0 Analyse quantitative @5 03
C03 02  X  ENG  @0 Quantitative analysis @5 03
C03 02  X  SPA  @0 Análisis cuantitativo @5 03
C03 03  X  FRE  @0 Métal lourd @5 05
C03 03  X  ENG  @0 Heavy metal @5 05
C03 03  X  SPA  @0 Metal pesado @5 05
C03 04  X  FRE  @0 Aliment @5 06
C03 04  X  ENG  @0 Food @5 06
C03 04  X  SPA  @0 Alimento @5 06
C03 05  X  FRE  @0 Environnement @5 08
C03 05  X  ENG  @0 Environment @5 08
C03 05  X  SPA  @0 Medio ambiente @5 08
C03 06  X  FRE  @0 Spectrométrie flamme @5 09
C03 06  X  ENG  @0 Flame spectrometry @5 09
C03 06  X  SPA  @0 Espectrometría llama @5 09
C03 07  X  FRE  @0 Spectrométrie absorption atomique @5 11
C03 07  X  ENG  @0 Atomic absorption spectrometry @5 11
C03 07  X  SPA  @0 Espectrometría absorción atómica @5 11
C03 08  X  FRE  @0 Contamination chimique @5 12
C03 08  X  ENG  @0 Chemical contamination @5 12
C03 08  X  SPA  @0 Contaminación química @5 12
C07 01  X  FRE  @0 Méthode physique @5 61
C07 01  X  ENG  @0 Physical method @5 61
C07 01  X  SPA  @0 Método físico @5 61
N21       @1 220

Format Inist (serveur)

NO : PASCAL 11-0322576 INIST
ET : Determination of some heavy metals in food and environmental samples by flame atomic absorption spectrometry after coprecipitation
AU : SOYLAK (Mustafa); AYDIN (Ayse)
AF : University of Erciyes, Faculty of Science, Chemistry Dept/38039 Kayseri/Turquie (1 aut., 2 aut.)
DT : Publication en série; Niveau analytique
SO : Food and chemical toxicology; ISSN 0278-6915; Coden FCTOD7; Royaume-Uni; Da. 2011; Vol. 49; No. 6; Pp. 1242-1248; Bibl. 1 p.1/4
LA : Anglais
EA : A novel preconcentration procedure based coprecipitation of Cu(II), Co(II), Cd(II), Ni(II), Mn(II), Fe(III) and PB(II) on thulium hydroxide precipitate has been presented prior to flame atomic absorption spectrometric determination of them in environmental samples. The analytical parameters that influenced the quantitative coprecipitation of analytes including amount of thulium, pH, duration time, etc. were investigated. The effects of alkali, earth alkali, and some transition metals on the recoveries were also studied. Under the optimized conditions, the detection limits (3 sigma, N =10) for the analytes were in the range of 0.1-1.6 μg/L, respectively. The validation of the presented coprecipitation method was checked by the analysis of certified reference materials (TMDA 54.4 fortified lake water and HR-1 Humber river sediment). The proposed coprecipitation method has been successfully applied for the determination of traces of copper, cobalt, cadmium, nickel, manganese, iron and lead in food and environmental samples.
CC : 002B03L05; 002B03H
FD : Dosage; Analyse quantitative; Métal lourd; Aliment; Environnement; Spectrométrie flamme; Spectrométrie absorption atomique; Contamination chimique
FG : Méthode physique
ED : Assay; Quantitative analysis; Heavy metal; Food; Environment; Flame spectrometry; Atomic absorption spectrometry; Chemical contamination
EG : Physical method
SD : Dosificación; Análisis cuantitativo; Metal pesado; Alimento; Medio ambiente; Espectrometría llama; Espectrometría absorción atómica; Contaminación química
LO : INIST-10616.354000191617860080
ID : 11-0322576

Links to Exploration step

Pascal:11-0322576

Le document en format XML

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