Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation
Identifieur interne : 000B79 ( Main/Merge ); précédent : 000B78; suivant : 000B80Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation
Auteurs : Nicolas Freslon [France] ; Germain Bayon [France] ; Dominique Birot [France] ; Claire Bollinger [France] ; Jean Alix Barrat [France]Source :
- Talanta : (Oxford) [ 0039-9140 ] ; 2011.
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- Pascal (Inist)
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- KwdEn :
Abstract
This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)2 coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.
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co-precipitation</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Certified reference material</term>
<term>Chemical enrichment</term>
<term>Coprecipitation</term>
<term>Coupled method</term>
<term>Element abundance</term>
<term>Inductive coupling plasma spectrometry</term>
<term>Lanthanide</term>
<term>Magnesium Hydroxides</term>
<term>Mass spectrometry</term>
<term>Precipitation</term>
<term>Reproducibility</term>
<term>Sample</term>
<term>Seawater</term>
<term>Standard</term>
<term>Thulium</term>
<term>Trace element</term>
<term>Use</term>
<term>Volume</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Lanthanide</term>
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<term>Précipitation</term>
<term>Coprécipitation</term>
<term>Abondance élément</term>
<term>Spectrométrie ICP</term>
<term>Spectrométrie masse</term>
<term>Utilisation</term>
<term>Enrichissement chimique</term>
<term>Thulium</term>
<term>Méthode couplée</term>
<term>Volume</term>
<term>Matériau référence certifié</term>
<term>Etalon</term>
<term>Eau mer</term>
<term>Magnésium Hydroxyde</term>
<term>Echantillon</term>
<term>Reproductibilité</term>
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<front><div type="abstract" xml:lang="en">This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)<sub>2</sub>
coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.</div>
</front>
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<tree><country name="France"><region name="Région Bretagne"><name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
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<name sortKey="Barrat, Jean Alix" sort="Barrat, Jean Alix" uniqKey="Barrat J" first="Jean Alix" last="Barrat">Jean Alix Barrat</name>
<name sortKey="Barrat, Jean Alix" sort="Barrat, Jean Alix" uniqKey="Barrat J" first="Jean Alix" last="Barrat">Jean Alix Barrat</name>
<name sortKey="Bayon, Germain" sort="Bayon, Germain" uniqKey="Bayon G" first="Germain" last="Bayon">Germain Bayon</name>
<name sortKey="Birot, Dominique" sort="Birot, Dominique" uniqKey="Birot D" first="Dominique" last="Birot">Dominique Birot</name>
<name sortKey="Bollinger, Claire" sort="Bollinger, Claire" uniqKey="Bollinger C" first="Claire" last="Bollinger">Claire Bollinger</name>
<name sortKey="Bollinger, Claire" sort="Bollinger, Claire" uniqKey="Bollinger C" first="Claire" last="Bollinger">Claire Bollinger</name>
<name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
<name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
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