ThuliumV1, Pascal, Corpus, bibRecord, 000215

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Identifieur interne : 000215 ( Pascal/Corpus ); précédent : 000214; suivant : 000216

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Auteurs : Nicolas Freslon ; Germain Bayon ; Dominique Birot ; Claire Bollinger ; Jean Alix Barrat

Source :

Talanta : (Oxford) [ 0039-9140 ] ; 2011.

RBID : Pascal:11-0374675

Descripteurs français

Pascal (Inist)
- Lanthanide, Elément trace, Précipitation, Coprécipitation, Abondance élément, Spectrométrie ICP, Spectrométrie masse, Utilisation, Enrichissement chimique, Thulium, Méthode couplée, Volume, Matériau référence certifié, Etalon, Eau mer, Magnésium Hydroxyde, Echantillon, Reproductibilité.

English descriptors

KwdEn :
- Certified reference material, Chemical enrichment, Coprecipitation, Coupled method, Element abundance, Inductive coupling plasma spectrometry, Lanthanide, Magnesium Hydroxides, Mass spectrometry, Precipitation, Reproducibility, Sample, Seawater, Standard, Thulium, Trace element, Use, Volume.

Abstract

This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)₂ coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

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A11	`01`	`1`		`@1 FRESLON (Nicolas)`
A11	`02`	`1`		`@1 BAYON (Germain)`
A11	`03`	`1`		`@1 BIROT (Dominique)`
A11	`04`	`1`		`@1 BOLLINGER (Claire)`
A11	`05`	`1`		`@1 BARRAT (Jean Alix)`
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A43	`01`			`@1 INIST @2 9221 @5 354000191089690830`
A44				`@0 0000 @1 © 2011 INIST-CNRS. All rights reserved.`
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C01	`01`		`ENG`	@0 This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)₂ coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.
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C03	`02`	`X`	`FRE`	`@0 Elément trace @5 02`
C03	`02`	`X`	`ENG`	`@0 Trace element @5 02`
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C03	`03`	`X`	`FRE`	`@0 Précipitation @5 03`
C03	`03`	`X`	`ENG`	`@0 Precipitation @5 03`
C03	`03`	`X`	`SPA`	`@0 Precipitación @5 03`
C03	`04`	`X`	`FRE`	`@0 Coprécipitation @5 04`
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C03	`05`	`3`	`FRE`	`@0 Abondance élément @5 05`
C03	`05`	`3`	`ENG`	`@0 Element abundance @5 05`
C03	`06`	`X`	`FRE`	`@0 Spectrométrie ICP @5 06`
C03	`06`	`X`	`ENG`	`@0 Inductive coupling plasma spectrometry @5 06`
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C03	`07`	`X`	`ENG`	`@0 Mass spectrometry @5 07`
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C03	`09`	`X`	`FRE`	`@0 Enrichissement chimique @5 09`
C03	`09`	`X`	`ENG`	`@0 Chemical enrichment @5 09`
C03	`09`	`X`	`SPA`	`@0 Enriquecimiento químico @5 09`
C03	`10`	`X`	`FRE`	`@0 Thulium @2 NC @5 10`
C03	`10`	`X`	`ENG`	`@0 Thulium @2 NC @5 10`
C03	`10`	`X`	`SPA`	`@0 Tulio @2 NC @5 10`
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C03	`12`	`X`	`FRE`	`@0 Volume @5 12`
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C03	`16`	`X`	`ENG`	`@0 Magnesium Hydroxides @2 NC @2 FR @2 NA @5 16`
C03	`16`	`X`	`SPA`	`@0 Magnesio Hidróxido @2 NC @2 FR @2 NA @5 16`
C03	`17`	`X`	`FRE`	`@0 Echantillon @5 22`
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C03	`18`	`X`	`ENG`	`@0 Reproducibility @5 23`
C03	`18`	`X`	`SPA`	`@0 Reproductividad @5 23`
N21				`@1 255`
N44	`01`			`@1 OTO`
N82				`@1 OTO`

Format Inist (serveur)

NO :	PASCAL 11-0374675 INIST
ET :	Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)₂ co-precipitation
AU :	FRESLON (Nicolas); BAYON (Germain); BIROT (Dominique); BOLLINGER (Claire); BARRAT (Jean Alix)
AF :	Departement Géosciences Marines, IFREMER/29280 Plouzané/France (1 aut., 2 aut., 3 aut.); Université Europeenne de Bretagne/35000 Rennes/France (1 aut., 4 aut., 5 aut.); CNRS UMR6538, IUEM, Université de Brest/29280 Plouzané/France (1 aut., 4 aut., 5 aut.)
DT :	Publication en série; Niveau analytique
SO :	Talanta : (Oxford); ISSN 0039-9140; Coden TLNTA2; Pays-Bas; Da. 2011; Vol. 85; No. 1; Pp. 582-587; Bibl. 29 ref.
LA :	Anglais
EA :	This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)₂ coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.
CC :	001C04C
FD :	Lanthanide; Elément trace; Précipitation; Coprécipitation; Abondance élément; Spectrométrie ICP; Spectrométrie masse; Utilisation; Enrichissement chimique; Thulium; Méthode couplée; Volume; Matériau référence certifié; Etalon; Eau mer; Magnésium Hydroxyde; Echantillon; Reproductibilité
ED :	Lanthanide; Trace element; Precipitation; Coprecipitation; Element abundance; Inductive coupling plasma spectrometry; Mass spectrometry; Use; Chemical enrichment; Thulium; Coupled method; Volume; Certified reference material; Standard; Seawater; Magnesium Hydroxides; Sample; Reproducibility
SD :	Lantánido; Elemento traza; Precipitación; Coprecipitación; Espectrometría ICP; Espectrometría masa; Uso; Enriquecimiento químico; Tulio; Método acoplado; Volumen; Material estandar; Marco; Agua mar; Magnesio Hidróxido; Muestra; Reproductividad
LO :	INIST-9221.354000191089690830
ID :	11-0374675

Links to Exploration step

Pascal:11-0374675

Le document en format XML

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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)<sub>2</sub>
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<front><div type="abstract" xml:lang="en">This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)<sub>2</sub>
 coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.</div>
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<fA11 i1="05" i2="1"><s1>BARRAT (Jean Alix)</s1>
</fA11>
<fA14 i1="01"><s1>Departement Géosciences Marines, IFREMER</s1>
<s2>29280 Plouzané</s2>
<s3>FRA</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>Université Europeenne de Bretagne</s1>
<s2>35000 Rennes</s2>
<s3>FRA</s3>
<sZ>1 aut.</sZ>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
</fA14>
<fA14 i1="03"><s1>CNRS UMR6538, IUEM, Université de Brest</s1>
<s2>29280 Plouzané</s2>
<s3>FRA</s3>
<sZ>1 aut.</sZ>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
</fA14>
<fA20><s1>582-587</s1>
</fA20>
<fA21><s1>2011</s1>
</fA21>
<fA23 i1="01"><s0>ENG</s0>
</fA23>
<fA43 i1="01"><s1>INIST</s1>
<s2>9221</s2>
<s5>354000191089690830</s5>
</fA43>
<fA44><s0>0000</s0>
<s1>© 2011 INIST-CNRS. All rights reserved.</s1>
</fA44>
<fA45><s0>29 ref.</s0>
</fA45>
<fA47 i1="01" i2="1"><s0>11-0374675</s0>
</fA47>
<fA60><s1>P</s1>
</fA60>
<fA61><s0>A</s0>
</fA61>
<fA64 i1="01" i2="1"><s0>Talanta : (Oxford)</s0>
</fA64>
<fA66 i1="01"><s0>NLD</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)<sub>2</sub>
 coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.</s0>
</fC01>
<fC02 i1="01" i2="X"><s0>001C04C</s0>
</fC02>
<fC03 i1="01" i2="X" l="FRE"><s0>Lanthanide</s0>
<s2>NC</s2>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="ENG"><s0>Lanthanide</s0>
<s2>NC</s2>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="SPA"><s0>Lantánido</s0>
<s2>NC</s2>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="X" l="FRE"><s0>Elément trace</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="ENG"><s0>Trace element</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="SPA"><s0>Elemento traza</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="X" l="FRE"><s0>Précipitation</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG"><s0>Precipitation</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA"><s0>Precipitación</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE"><s0>Coprécipitation</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG"><s0>Coprecipitation</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA"><s0>Coprecipitación</s0>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE"><s0>Abondance élément</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG"><s0>Element abundance</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Spectrométrie ICP</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Inductive coupling plasma spectrometry</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Espectrometría ICP</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE"><s0>Spectrométrie masse</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG"><s0>Mass spectrometry</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA"><s0>Espectrometría masa</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Utilisation</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG"><s0>Use</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Uso</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE"><s0>Enrichissement chimique</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Chemical enrichment</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Enriquecimiento químico</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Thulium</s0>
<s2>NC</s2>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Thulium</s0>
<s2>NC</s2>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Tulio</s0>
<s2>NC</s2>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Méthode couplée</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Coupled method</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Método acoplado</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Volume</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Volume</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Volumen</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Matériau référence certifié</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Certified reference material</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Material estandar</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>Etalon</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>Standard</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Marco</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Eau mer</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG"><s0>Seawater</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA"><s0>Agua mar</s0>
<s5>15</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>Magnésium Hydroxyde</s0>
<s2>NC</s2>
<s2>FR</s2>
<s2>NA</s2>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG"><s0>Magnesium Hydroxides</s0>
<s2>NC</s2>
<s2>FR</s2>
<s2>NA</s2>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA"><s0>Magnesio Hidróxido</s0>
<s2>NC</s2>
<s2>FR</s2>
<s2>NA</s2>
<s5>16</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Echantillon</s0>
<s5>22</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG"><s0>Sample</s0>
<s5>22</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA"><s0>Muestra</s0>
<s5>22</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Reproductibilité</s0>
<s5>23</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Reproducibility</s0>
<s5>23</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Reproductividad</s0>
<s5>23</s5>
</fC03>
<fN21><s1>255</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
</standard>
<server><NO>PASCAL 11-0374675 INIST</NO>
<ET>Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)<sub>2</sub>
 co-precipitation</ET>
<AU>FRESLON (Nicolas); BAYON (Germain); BIROT (Dominique); BOLLINGER (Claire); BARRAT (Jean Alix)</AU>
<AF>Departement Géosciences Marines, IFREMER/29280 Plouzané/France (1 aut., 2 aut., 3 aut.); Université Europeenne de Bretagne/35000 Rennes/France (1 aut., 4 aut., 5 aut.); CNRS UMR6538, IUEM, Université de Brest/29280 Plouzané/France (1 aut., 4 aut., 5 aut.)</AF>
<DT>Publication en série; Niveau analytique</DT>
<SO>Talanta : (Oxford); ISSN 0039-9140; Coden TLNTA2; Pays-Bas; Da. 2011; Vol. 85; No. 1; Pp. 582-587; Bibl. 29 ref.</SO>
<LA>Anglais</LA>
<EA>This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)<sub>2</sub>
 coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.</EA>
<CC>001C04C</CC>
<FD>Lanthanide; Elément trace; Précipitation; Coprécipitation; Abondance élément; Spectrométrie ICP; Spectrométrie masse; Utilisation; Enrichissement chimique; Thulium; Méthode couplée; Volume; Matériau référence certifié; Etalon; Eau mer; Magnésium Hydroxyde; Echantillon; Reproductibilité</FD>
<ED>Lanthanide; Trace element; Precipitation; Coprecipitation; Element abundance; Inductive coupling plasma spectrometry; Mass spectrometry; Use; Chemical enrichment; Thulium; Coupled method; Volume; Certified reference material; Standard; Seawater; Magnesium Hydroxides; Sample; Reproducibility</ED>
<SD>Lantánido; Elemento traza; Precipitación; Coprecipitación; Espectrometría ICP; Espectrometría masa; Uso; Enriquecimiento químico; Tulio; Método acoplado; Volumen; Material estandar; Marco; Agua mar; Magnesio Hidróxido; Muestra; Reproductividad</SD>
<LO>INIST-9221.354000191089690830</LO>
<ID>11-0374675</ID>
</server>
</inist>
</record>

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Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

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