ThuliumV1, Pascal, Checkpoint, bibRecord, 000243

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Identifieur interne : 000243 ( Pascal/Checkpoint ); précédent : 000242; suivant : 000244

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Auteurs : Nicolas Freslon [France] ; Germain Bayon [France] ; Dominique Birot [France] ; Claire Bollinger [France] ; Jean Alix Barrat [France]

Source :

Talanta : (Oxford) [ 0039-9140 ] ; 2011.

RBID : Pascal:11-0374675

Descripteurs français

Pascal (Inist)
- Lanthanide, Elément trace, Précipitation, Coprécipitation, Abondance élément, Spectrométrie ICP, Spectrométrie masse, Utilisation, Enrichissement chimique, Thulium, Méthode couplée, Volume, Matériau référence certifié, Etalon, Eau mer, Magnésium Hydroxyde, Echantillon, Reproductibilité.

English descriptors

KwdEn :
- Certified reference material, Chemical enrichment, Coprecipitation, Coupled method, Element abundance, Inductive coupling plasma spectrometry, Lanthanide, Magnesium Hydroxides, Mass spectrometry, Precipitation, Reproducibility, Sample, Seawater, Standard, Thulium, Trace element, Use, Volume.

Abstract

This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)₂ coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.

Affiliations:

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Pascal:11-0374675

Le document en format XML

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<front><div type="abstract" xml:lang="en">This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)<sub>2</sub>
 coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.</div>
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 coprecipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11 % RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.</s0>
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<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Uso</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE"><s0>Enrichissement chimique</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Chemical enrichment</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Enriquecimiento químico</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Thulium</s0>
<s2>NC</s2>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Thulium</s0>
<s2>NC</s2>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Tulio</s0>
<s2>NC</s2>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Méthode couplée</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Coupled method</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Método acoplado</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Volume</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Volume</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Volumen</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Matériau référence certifié</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Certified reference material</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Material estandar</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>Etalon</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>Standard</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Marco</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Eau mer</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG"><s0>Seawater</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA"><s0>Agua mar</s0>
<s5>15</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>Magnésium Hydroxyde</s0>
<s2>NC</s2>
<s2>FR</s2>
<s2>NA</s2>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG"><s0>Magnesium Hydroxides</s0>
<s2>NC</s2>
<s2>FR</s2>
<s2>NA</s2>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA"><s0>Magnesio Hidróxido</s0>
<s2>NC</s2>
<s2>FR</s2>
<s2>NA</s2>
<s5>16</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Echantillon</s0>
<s5>22</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG"><s0>Sample</s0>
<s5>22</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA"><s0>Muestra</s0>
<s5>22</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Reproductibilité</s0>
<s5>23</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Reproducibility</s0>
<s5>23</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Reproductividad</s0>
<s5>23</s5>
</fC03>
<fN21><s1>255</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
</standard>
</inist>
<affiliations><list><country><li>France</li>
</country>
<region><li>Région Bretagne</li>
</region>
<settlement><li>Plouzané</li>
<li>Rennes</li>
</settlement>
</list>
<tree><country name="France"><region name="Région Bretagne"><name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
</region>
<name sortKey="Barrat, Jean Alix" sort="Barrat, Jean Alix" uniqKey="Barrat J" first="Jean Alix" last="Barrat">Jean Alix Barrat</name>
<name sortKey="Barrat, Jean Alix" sort="Barrat, Jean Alix" uniqKey="Barrat J" first="Jean Alix" last="Barrat">Jean Alix Barrat</name>
<name sortKey="Bayon, Germain" sort="Bayon, Germain" uniqKey="Bayon G" first="Germain" last="Bayon">Germain Bayon</name>
<name sortKey="Birot, Dominique" sort="Birot, Dominique" uniqKey="Birot D" first="Dominique" last="Birot">Dominique Birot</name>
<name sortKey="Bollinger, Claire" sort="Bollinger, Claire" uniqKey="Bollinger C" first="Claire" last="Bollinger">Claire Bollinger</name>
<name sortKey="Bollinger, Claire" sort="Bollinger, Claire" uniqKey="Bollinger C" first="Claire" last="Bollinger">Claire Bollinger</name>
<name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
<name sortKey="Freslon, Nicolas" sort="Freslon, Nicolas" uniqKey="Freslon N" first="Nicolas" last="Freslon">Nicolas Freslon</name>
</country>
</tree>
</affiliations>
</record>

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   |texte=   Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation
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Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

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