Methyl N-(3-cyanopicolinoyl)-l-tryptophanate
Identifieur interne : 000294 ( Ncbi/Merge ); précédent : 000293; suivant : 000295Methyl N-(3-cyanopicolinoyl)-l-tryptophanate
Auteurs : Olga Ovdiichuk [Ukraine] ; Olga Hordiyenko [Ukraine] ; Zoia Voitenko [Ukraine] ; Axelle Arrault [France] ; Volodymyr Medviediev [Ukraine]Source :
- Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2013.
Abstract
In the title compound, C19H16N4O3, the stereocenter has an
Url:
DOI: 10.1107/S160053681303153X
PubMed: 24454241
PubMed Central: 3885065
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PMC:3885065Le document en format XML
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-(3-cyanopicolinoyl)-<sc>l</sc>
-tryptophanate</title>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Methyl <italic>N</italic>
-(3-cyanopicolinoyl)-<sc>l</sc>
-tryptophanate</title>
<author><name sortKey="Ovdiichuk, Olga" sort="Ovdiichuk, Olga" uniqKey="Ovdiichuk O" first="Olga" last="Ovdiichuk">Olga Ovdiichuk</name>
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<country xml:lang="fr">Ukraine</country>
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<front><div type="abstract" xml:lang="en"><p>In the title compound, C<sub>19</sub>
H<sub>16</sub>
N<sub>4</sub>
O<sub>3</sub>
, the stereocenter has an <sc>l</sc>
configuration; <sc>l</sc>
-tryptophan methyl ester hydrochloride being used as a starting material. The indole ring system and the pyridine ring are inclined to one another by 13.55 (14)°. In the crystal, adjacent molecules are linked <italic>via</italic>
N—H⋯O hydrogen bonds, forming chains propagating along the <italic>c</italic>
-axis direction.</p>
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<double pmid="24454241"><pmc><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Methyl <italic>N</italic>
-(3-cyanopicolinoyl)-<sc>l</sc>
-tryptophanate</title>
<author><name sortKey="Ovdiichuk, Olga" sort="Ovdiichuk, Olga" uniqKey="Ovdiichuk O" first="Olga" last="Ovdiichuk">Olga Ovdiichuk</name>
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</nlm:aff>
<country xml:lang="fr">Ukraine</country>
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</nlm:aff>
<country xml:lang="fr">Ukraine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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-(3-cyanopicolinoyl)-<sc>l</sc>
-tryptophanate</title>
<author><name sortKey="Ovdiichuk, Olga" sort="Ovdiichuk, Olga" uniqKey="Ovdiichuk O" first="Olga" last="Ovdiichuk">Olga Ovdiichuk</name>
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</nlm:aff>
<country xml:lang="fr">Ukraine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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</author>
<author><name sortKey="Hordiyenko, Olga" sort="Hordiyenko, Olga" uniqKey="Hordiyenko O" first="Olga" last="Hordiyenko">Olga Hordiyenko</name>
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</nlm:aff>
<country xml:lang="fr">Ukraine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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</nlm:aff>
<country xml:lang="fr">Ukraine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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</nlm:aff>
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<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<front><div type="abstract" xml:lang="en"><p>In the title compound, C<sub>19</sub>
H<sub>16</sub>
N<sub>4</sub>
O<sub>3</sub>
, the stereocenter has an <sc>l</sc>
configuration; <sc>l</sc>
-tryptophan methyl ester hydrochloride being used as a starting material. The indole ring system and the pyridine ring are inclined to one another by 13.55 (14)°. In the crystal, adjacent molecules are linked <italic>via</italic>
N—H⋯O hydrogen bonds, forming chains propagating along the <italic>c</italic>
-axis direction.</p>
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<author><name sortKey="Medviediev, Volodymyr" sort="Medviediev, Volodymyr" uniqKey="Medviediev V" first="Volodymyr" last="Medviediev">Volodymyr Medviediev</name>
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<author><name sortKey="Hordiyenko, Olga" sort="Hordiyenko, Olga" uniqKey="Hordiyenko O" first="Olga" last="Hordiyenko">Olga Hordiyenko</name>
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<affiliation wicri:level="3"><nlm:affiliation>Laboratoire de Chimie Physique Macromoleculaire, UMR 7568, ENSIC, BP 451, 54001 Nancy, France.</nlm:affiliation>
<country xml:lang="fr">France</country>
<wicri:regionArea>Laboratoire de Chimie Physique Macromoleculaire, UMR 7568, ENSIC, BP 451, 54001 Nancy</wicri:regionArea>
<placeName><region type="region" nuts="2">Grand Est</region>
<region type="old region" nuts="2">Lorraine (région)</region>
<settlement type="city">Nancy</settlement>
</placeName>
</affiliation>
</author>
<author><name sortKey="Medviediev, Volodymyr" sort="Medviediev, Volodymyr" uniqKey="Medviediev V" first="Volodymyr" last="Medviediev">Volodymyr Medviediev</name>
<affiliation wicri:level="1"><nlm:affiliation>STC "Institute for Single Crystals", National Academy of Science of Ukraine, Lenina ave. 60, 61001, Khar'kov, Ukraine.</nlm:affiliation>
<country xml:lang="fr">Ukraine</country>
<wicri:regionArea>STC "Institute for Single Crystals", National Academy of Science of Ukraine, Lenina ave. 60, 61001, Khar'kov</wicri:regionArea>
<wicri:noRegion>Khar'kov</wicri:noRegion>
</affiliation>
</author>
</analytic>
<series><title level="j">Acta crystallographica. Section E, Structure reports online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2013" type="published">2013</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
</fileDesc>
<profileDesc><textClass></textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">In the title compound, C19H16N4O3, the stereocenter has an l configuration; l-tryptophan methyl ester hydro-chloride being used as a starting material. The indole ring system and the pyridine ring are inclined to one another by 13.55 (14)°. In the crystal, adjacent mol-ecules are linked via N-H⋯O hydrogen bonds, forming chains propagating along the c-axis direction.</div>
</front>
</TEI>
</pubmed>
</double>
</record>
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