Methyl N-(3-cyano-picolino-yl)-l-tryptophanate.
Identifieur interne : 000049 ( PubMed/Corpus ); précédent : 000048; suivant : 000050Methyl N-(3-cyano-picolino-yl)-l-tryptophanate.
Auteurs : Olga Ovdiichuk ; Olga Hordiyenko ; Zoia Voitenko ; Axelle Arrault ; Volodymyr MedviedievSource :
- Acta crystallographica. Section E, Structure reports online [ 1600-5368 ] ; 2013.
Abstract
In the title compound, C19H16N4O3, the stereocenter has an l configuration; l-tryptophan methyl ester hydro-chloride being used as a starting material. The indole ring system and the pyridine ring are inclined to one another by 13.55 (14)°. In the crystal, adjacent mol-ecules are linked via N-H⋯O hydrogen bonds, forming chains propagating along the c-axis direction.
DOI: 10.1107/S160053681303153X
PubMed: 24454241
Links to Exploration step
pubmed:24454241Le document en format XML
<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Methyl N-(3-cyano-picolino-yl)-l-tryptophanate.</title>
<author><name sortKey="Ovdiichuk, Olga" sort="Ovdiichuk, Olga" uniqKey="Ovdiichuk O" first="Olga" last="Ovdiichuk">Olga Ovdiichuk</name>
<affiliation><nlm:affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Hordiyenko, Olga" sort="Hordiyenko, Olga" uniqKey="Hordiyenko O" first="Olga" last="Hordiyenko">Olga Hordiyenko</name>
<affiliation><nlm:affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Voitenko, Zoia" sort="Voitenko, Zoia" uniqKey="Voitenko Z" first="Zoia" last="Voitenko">Zoia Voitenko</name>
<affiliation><nlm:affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Arrault, Axelle" sort="Arrault, Axelle" uniqKey="Arrault A" first="Axelle" last="Arrault">Axelle Arrault</name>
<affiliation><nlm:affiliation>Laboratoire de Chimie Physique Macromoleculaire, UMR 7568, ENSIC, BP 451, 54001 Nancy, France.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Medviediev, Volodymyr" sort="Medviediev, Volodymyr" uniqKey="Medviediev V" first="Volodymyr" last="Medviediev">Volodymyr Medviediev</name>
<affiliation><nlm:affiliation>STC "Institute for Single Crystals", National Academy of Science of Ukraine, Lenina ave. 60, 61001, Khar'kov, Ukraine.</nlm:affiliation>
</affiliation>
</author>
</titleStmt>
<publicationStmt><idno type="wicri:source">PubMed</idno>
<date when="2013">2013</date>
<idno type="doi">10.1107/S160053681303153X</idno>
<idno type="RBID">pubmed:24454241</idno>
<idno type="pmid">24454241</idno>
<idno type="wicri:Area/PubMed/Corpus">000049</idno>
<idno type="wicri:explorRef" wicri:stream="PubMed" wicri:step="Corpus" wicri:corpus="PubMed">000049</idno>
</publicationStmt>
<sourceDesc><biblStruct><analytic><title xml:lang="en">Methyl N-(3-cyano-picolino-yl)-l-tryptophanate.</title>
<author><name sortKey="Ovdiichuk, Olga" sort="Ovdiichuk, Olga" uniqKey="Ovdiichuk O" first="Olga" last="Ovdiichuk">Olga Ovdiichuk</name>
<affiliation><nlm:affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Hordiyenko, Olga" sort="Hordiyenko, Olga" uniqKey="Hordiyenko O" first="Olga" last="Hordiyenko">Olga Hordiyenko</name>
<affiliation><nlm:affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Voitenko, Zoia" sort="Voitenko, Zoia" uniqKey="Voitenko Z" first="Zoia" last="Voitenko">Zoia Voitenko</name>
<affiliation><nlm:affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Arrault, Axelle" sort="Arrault, Axelle" uniqKey="Arrault A" first="Axelle" last="Arrault">Axelle Arrault</name>
<affiliation><nlm:affiliation>Laboratoire de Chimie Physique Macromoleculaire, UMR 7568, ENSIC, BP 451, 54001 Nancy, France.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Medviediev, Volodymyr" sort="Medviediev, Volodymyr" uniqKey="Medviediev V" first="Volodymyr" last="Medviediev">Volodymyr Medviediev</name>
<affiliation><nlm:affiliation>STC "Institute for Single Crystals", National Academy of Science of Ukraine, Lenina ave. 60, 61001, Khar'kov, Ukraine.</nlm:affiliation>
</affiliation>
</author>
</analytic>
<series><title level="j">Acta crystallographica. Section E, Structure reports online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2013" type="published">2013</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
</fileDesc>
<profileDesc><textClass></textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">In the title compound, C19H16N4O3, the stereocenter has an l configuration; l-tryptophan methyl ester hydro-chloride being used as a starting material. The indole ring system and the pyridine ring are inclined to one another by 13.55 (14)°. In the crystal, adjacent mol-ecules are linked via N-H⋯O hydrogen bonds, forming chains propagating along the c-axis direction.</div>
</front>
</TEI>
<pubmed><MedlineCitation Owner="NLM" Status="PubMed-not-MEDLINE"><PMID Version="1">24454241</PMID>
<DateCreated><Year>2014</Year>
<Month>01</Month>
<Day>23</Day>
</DateCreated>
<DateCompleted><Year>2014</Year>
<Month>01</Month>
<Day>23</Day>
</DateCompleted>
<DateRevised><Year>2014</Year>
<Month>01</Month>
<Day>27</Day>
</DateRevised>
<Article PubModel="Electronic-eCollection"><Journal><ISSN IssnType="Electronic">1600-5368</ISSN>
<JournalIssue CitedMedium="Print"><Volume>69</Volume>
<Issue>Pt 12</Issue>
<PubDate><Year>2013</Year>
<Month>Nov</Month>
<Day>23</Day>
</PubDate>
</JournalIssue>
<Title>Acta crystallographica. Section E, Structure reports online</Title>
<ISOAbbreviation>Acta Crystallogr Sect E Struct Rep Online</ISOAbbreviation>
</Journal>
<ArticleTitle>Methyl N-(3-cyano-picolino-yl)-l-tryptophanate.</ArticleTitle>
<Pagination><MedlinePgn>o1810</MedlinePgn>
</Pagination>
<ELocationID EIdType="doi" ValidYN="Y">10.1107/S160053681303153X</ELocationID>
<Abstract><AbstractText>In the title compound, C19H16N4O3, the stereocenter has an l configuration; l-tryptophan methyl ester hydro-chloride being used as a starting material. The indole ring system and the pyridine ring are inclined to one another by 13.55 (14)°. In the crystal, adjacent mol-ecules are linked via N-H⋯O hydrogen bonds, forming chains propagating along the c-axis direction.</AbstractText>
</Abstract>
<AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Ovdiichuk</LastName>
<ForeName>Olga</ForeName>
<Initials>O</Initials>
<AffiliationInfo><Affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Hordiyenko</LastName>
<ForeName>Olga</ForeName>
<Initials>O</Initials>
<AffiliationInfo><Affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Voitenko</LastName>
<ForeName>Zoia</ForeName>
<Initials>Z</Initials>
<AffiliationInfo><Affiliation>Kyiv National Taras Shevchenko University, Department of Chemistry, Volodymyrska str. 64, 01601 Kyiv, Ukraine.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Arrault</LastName>
<ForeName>Axelle</ForeName>
<Initials>A</Initials>
<AffiliationInfo><Affiliation>Laboratoire de Chimie Physique Macromoleculaire, UMR 7568, ENSIC, BP 451, 54001 Nancy, France.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Medviediev</LastName>
<ForeName>Volodymyr</ForeName>
<Initials>V</Initials>
<AffiliationInfo><Affiliation>STC "Institute for Single Crystals", National Academy of Science of Ukraine, Lenina ave. 60, 61001, Khar'kov, Ukraine.</Affiliation>
</AffiliationInfo>
</Author>
</AuthorList>
<Language>eng</Language>
<PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType>
</PublicationTypeList>
<ArticleDate DateType="Electronic"><Year>2013</Year>
<Month>11</Month>
<Day>23</Day>
</ArticleDate>
</Article>
<MedlineJournalInfo><Country>United States</Country>
<MedlineTA>Acta Crystallogr Sect E Struct Rep Online</MedlineTA>
<NlmUniqueID>101089178</NlmUniqueID>
<ISSNLinking>1600-5368</ISSNLinking>
</MedlineJournalInfo>
<OtherID Source="NLM">PMC3885065</OtherID>
</MedlineCitation>
<PubmedData><History><PubMedPubDate PubStatus="ecollection"><Year>2013</Year>
<Month>12</Month>
<Day>01</Day>
</PubMedPubDate>
<PubMedPubDate PubStatus="received"><Year>2013</Year>
<Month>11</Month>
<Day>13</Day>
</PubMedPubDate>
<PubMedPubDate PubStatus="accepted"><Year>2013</Year>
<Month>11</Month>
<Day>19</Day>
</PubMedPubDate>
<PubMedPubDate PubStatus="epublish"><Year>2013</Year>
<Month>11</Month>
<Day>23</Day>
</PubMedPubDate>
<PubMedPubDate PubStatus="entrez"><Year>2014</Year>
<Month>1</Month>
<Day>24</Day>
<Hour>6</Hour>
<Minute>0</Minute>
</PubMedPubDate>
<PubMedPubDate PubStatus="pubmed"><Year>2014</Year>
<Month>1</Month>
<Day>24</Day>
<Hour>6</Hour>
<Minute>0</Minute>
</PubMedPubDate>
<PubMedPubDate PubStatus="medline"><Year>2014</Year>
<Month>1</Month>
<Day>24</Day>
<Hour>6</Hour>
<Minute>1</Minute>
</PubMedPubDate>
</History>
<PublicationStatus>epublish</PublicationStatus>
<ArticleIdList><ArticleId IdType="doi">10.1107/S160053681303153X</ArticleId>
<ArticleId IdType="pii">su2666</ArticleId>
<ArticleId IdType="pubmed">24454241</ArticleId>
<ArticleId IdType="pmc">PMC3885065</ArticleId>
</ArticleIdList>
</PubmedData>
</pubmed>
</record>
Pour manipuler ce document sous Unix (Dilib)
EXPLOR_STEP=$WICRI_ROOT/Wicri/Lorraine/explor/LrgpV1/Data/PubMed/Corpus
HfdSelect -h $EXPLOR_STEP/biblio.hfd -nk 000049 | SxmlIndent | more
Ou
HfdSelect -h $EXPLOR_AREA/Data/PubMed/Corpus/biblio.hfd -nk 000049 | SxmlIndent | more
Pour mettre un lien sur cette page dans le réseau Wicri
{{Explor lien |wiki= Wicri/Lorraine |area= LrgpV1 |flux= PubMed |étape= Corpus |type= RBID |clé= pubmed:24454241 |texte= Methyl N-(3-cyano-picolino-yl)-l-tryptophanate. }}
Pour générer des pages wiki
HfdIndexSelect -h $EXPLOR_AREA/Data/PubMed/Corpus/RBID.i -Sk "pubmed:24454241" \ | HfdSelect -Kh $EXPLOR_AREA/Data/PubMed/Corpus/biblio.hfd \ | NlmPubMed2Wicri -a LrgpV1
![]() | This area was generated with Dilib version V0.6.32. | ![]() |