Some new biologically active metal-based sulfonamide
Identifieur interne : 000081 ( PascalFrancis/Checkpoint ); précédent : 000080; suivant : 000082Some new biologically active metal-based sulfonamide
Auteurs : Zahid H. Chohan [Pakistan] ; Hazoor A. Shad [Pakistan] ; Moulay H. Youssoufi [Maroc] ; TAIBI BEN HADDA [Maroc]Source :
- European journal of medicinal chemistry [ 0223-5234 ] ; 2010.
Descripteurs français
- Pascal (Inist)
- Sulfonamide, Métal divalent Complexe, Antibactérien, Antifongique, Cytotoxicité, Activité biologique, In vitro, Synthèse chimique, Cuivre Complexe, Cobalt Complexe, Nickel Complexe, Zinc Complexe, Base Schiff, Brome Composé organique, Complexe aqua, Coordinat organique, Conductivité ionique, Susceptibilité magnétique, Imine, Propriété électrique, Propriété magnétique, Benzènesulfonamide(N-[pyrimidin-2-yl]-4-[5-bromo-2-hydroxybenzylidèneamino]).
English descriptors
- KwdEn :
- Antibacterial agent, Antifungal agent, Aqua complex, Biological activity, Bromine Organic compounds, Chemical synthesis, Cobalt Complexes, Copper Complexes, Cytotoxicity, Divalent metal Complexes, Electrical properties, Imine, In vitro, Ionic conductivity, Magnetic properties, Magnetic susceptibility, Nickel Complexes, Organic ligand, Schiff base, Sulfonamide, Zinc Complexes.
Abstract
A new series of sulfonamide derived Schiff bases has been synthesized by a condensation reaction of various sulfonamides with aromatic aldehydes. The so obtained sulfonamide were further investigated for their chelation and biological properties with first row d-transition metal ions [cobalt(II), copper(II), nickel(II) and zinc(II)]. The nature of bonding and structure of all the synthesized compounds have been inferred from magnetic susceptibility and conductivity measurements, IR, 1H and 13C NMR, electronic spectral, mass spectrometry and CHN analysis data. The structure of ligand, 4-{[(E)-(5-bromo-2-hydroxy phenyl)methyldene]amino}-N-(4,6-dimethylpyrimidin-2-yl)benzenesulfonamide has also been determined by X-ray diffraction method. An octahedral geometry has been suggested for all the complexes. The ligands and their metal complexes have been screened for in vitro antibacterial, antifungal and cytotoxic properties. The result of these studies have revealed that all compounds showed moderate to significant antibacterial activity against one or more bacterial strains and good antifungal activity against various fungal strains.
Affiliations:
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Shad</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Chemistry, Bahauddin Zakariya University</s1><s2>Multan-60800</s2><s3>PAK</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ></inist:fA14><country>Pakistan</country><wicri:noRegion>Multan-60800</wicri:noRegion></affiliation></author><author><name sortKey="Youssoufi, Moulay H" sort="Youssoufi, Moulay H" uniqKey="Youssoufi M" first="Moulay H." last="Youssoufi">Moulay H. 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Chohan</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Chemistry, Bahauddin Zakariya University</s1><s2>Multan-60800</s2><s3>PAK</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ></inist:fA14><country>Pakistan</country><wicri:noRegion>Multan-60800</wicri:noRegion></affiliation></author><author><name sortKey="Shad, Hazoor A" sort="Shad, Hazoor A" uniqKey="Shad H" first="Hazoor A." last="Shad">Hazoor A. Shad</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Chemistry, Bahauddin Zakariya University</s1><s2>Multan-60800</s2><s3>PAK</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ></inist:fA14><country>Pakistan</country><wicri:noRegion>Multan-60800</wicri:noRegion></affiliation></author><author><name sortKey="Youssoufi, Moulay H" sort="Youssoufi, Moulay H" uniqKey="Youssoufi M" first="Moulay H." last="Youssoufi">Moulay H. Youssoufi</name><affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Laboratoire Chimie des Matériaux, Faculté des Sciences, Université Mohammed Premier</s1><s2>60000 Oujda</s2><s3>MAR</s3><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>Maroc</country><wicri:noRegion>60000 Oujda</wicri:noRegion></affiliation></author><author><name sortKey="Taibi Ben Hadda" sort="Taibi Ben Hadda" uniqKey="Taibi Ben Hadda" last="Taibi Ben Hadda">TAIBI BEN HADDA</name><affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Laboratoire Chimie des Matériaux, Faculté des Sciences, Université Mohammed Premier</s1><s2>60000 Oujda</s2><s3>MAR</s3><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>Maroc</country><wicri:noRegion>60000 Oujda</wicri:noRegion></affiliation></author></analytic><series><title level="j" type="main">European journal of medicinal chemistry</title><title level="j" type="abbreviated">Eur. j. med. chem.</title><idno type="ISSN">0223-5234</idno><imprint><date when="2010">2010</date></imprint></series></biblStruct></sourceDesc><seriesStmt><title level="j" type="main">European journal of medicinal chemistry</title><title level="j" type="abbreviated">Eur. j. med. chem.</title><idno type="ISSN">0223-5234</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Antibacterial agent</term><term>Antifungal agent</term><term>Aqua complex</term><term>Biological activity</term><term>Bromine Organic compounds</term><term>Chemical synthesis</term><term>Cobalt Complexes</term><term>Copper Complexes</term><term>Cytotoxicity</term><term>Divalent metal Complexes</term><term>Electrical properties</term><term>Imine</term><term>In vitro</term><term>Ionic conductivity</term><term>Magnetic properties</term><term>Magnetic susceptibility</term><term>Nickel Complexes</term><term>Organic ligand</term><term>Schiff base</term><term>Sulfonamide</term><term>Zinc Complexes</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Sulfonamide</term><term>Métal divalent Complexe</term><term>Antibactérien</term><term>Antifongique</term><term>Cytotoxicité</term><term>Activité biologique</term><term>In vitro</term><term>Synthèse chimique</term><term>Cuivre Complexe</term><term>Cobalt Complexe</term><term>Nickel Complexe</term><term>Zinc Complexe</term><term>Base Schiff</term><term>Brome Composé organique</term><term>Complexe aqua</term><term>Coordinat organique</term><term>Conductivité ionique</term><term>Susceptibilité magnétique</term><term>Imine</term><term>Propriété électrique</term><term>Propriété magnétique</term><term>Benzènesulfonamide(N-[pyrimidin-2-yl]-4-[5-bromo-2-hydroxybenzylidèneamino])</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">A new series of sulfonamide derived Schiff bases has been synthesized by a condensation reaction of various sulfonamides with aromatic aldehydes. The so obtained sulfonamide were further investigated for their chelation and biological properties with first row d-transition metal ions [cobalt(II), copper(II), nickel(II) and zinc(II)]. The nature of bonding and structure of all the synthesized compounds have been inferred from magnetic susceptibility and conductivity measurements, IR, <sup>1</sup>H and <sup>13</sup>C NMR, electronic spectral, mass spectrometry and CHN analysis data. The structure of ligand, 4-{[(E)-(5-bromo-2-hydroxy phenyl)methyldene]amino}-N-(4,6-dimethylpyrimidin-2-yl)benzenesulfonamide has also been determined by X-ray diffraction method. An octahedral geometry has been suggested for all the complexes. The ligands and their metal complexes have been screened for in vitro antibacterial, antifungal and cytotoxic properties. The result of these studies have revealed that all compounds showed moderate to significant antibacterial activity against one or more bacterial strains and good antifungal activity against various fungal strains.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0223-5234</s0></fA01><fA02 i1="01"><s0>EJMCA5</s0></fA02><fA03 i2="1"><s0>Eur. j. med. chem.</s0></fA03><fA05><s2>45</s2></fA05><fA06><s2>7</s2></fA06><fA08 i1="01" i2="1" l="ENG"><s1>Some new biologically active metal-based sulfonamide</s1></fA08><fA11 i1="01" i2="1"><s1>CHOHAN (Zahid H.)</s1></fA11><fA11 i1="02" i2="1"><s1>SHAD (Hazoor A.)</s1></fA11><fA11 i1="03" i2="1"><s1>YOUSSOUFI (Moulay H.)</s1></fA11><fA11 i1="04" i2="1"><s1>TAIBI BEN HADDA</s1></fA11><fA14 i1="01"><s1>Department of Chemistry, Bahauddin Zakariya University</s1><s2>Multan-60800</s2><s3>PAK</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ></fA14><fA14 i1="02"><s1>Laboratoire Chimie des Matériaux, Faculté des Sciences, Université Mohammed Premier</s1><s2>60000 Oujda</s2><s3>MAR</s3><sZ>3 aut.</sZ><sZ>4 aut.</sZ></fA14><fA20><s1>2893-2901</s1></fA20><fA21><s1>2010</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>12640</s2><s5>354000182195100240</s5></fA43><fA44><s0>0000</s0><s1>© 2010 INIST-CNRS. All rights reserved.</s1></fA44><fA45><s0>66 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>10-0437154</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>European journal of medicinal chemistry</s0></fA64><fA66 i1="01"><s0>GBR</s0></fA66><fC01 i1="01" l="ENG"><s0>A new series of sulfonamide derived Schiff bases has been synthesized by a condensation reaction of various sulfonamides with aromatic aldehydes. The so obtained sulfonamide were further investigated for their chelation and biological properties with first row d-transition metal ions [cobalt(II), copper(II), nickel(II) and zinc(II)]. The nature of bonding and structure of all the synthesized compounds have been inferred from magnetic susceptibility and conductivity measurements, IR, <sup>1</sup>H and <sup>13</sup>C NMR, electronic spectral, mass spectrometry and CHN analysis data. The structure of ligand, 4-{[(E)-(5-bromo-2-hydroxy phenyl)methyldene]amino}-N-(4,6-dimethylpyrimidin-2-yl)benzenesulfonamide has also been determined by X-ray diffraction method. An octahedral geometry has been suggested for all the complexes. The ligands and their metal complexes have been screened for in vitro antibacterial, antifungal and cytotoxic properties. The result of these studies have revealed that all compounds showed moderate to significant antibacterial activity against one or more bacterial strains and good antifungal activity against various fungal strains.</s0></fC01><fC02 i1="01" i2="X"><s0>002B02S04</s0></fC02><fC02 i1="02" i2="X"><s0>002B02S02</s0></fC02><fC03 i1="01" i2="X" l="FRE"><s0>Sulfonamide</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="ENG"><s0>Sulfonamide</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="SPA"><s0>Sulfonamida</s0><s5>01</s5></fC03><fC03 i1="02" i2="X" l="FRE"><s0>Métal divalent Complexe</s0><s2>NC</s2><s2>NA</s2><s5>02</s5></fC03><fC03 i1="02" i2="X" l="ENG"><s0>Divalent metal Complexes</s0><s2>NC</s2><s2>NA</s2><s5>02</s5></fC03><fC03 i1="02" i2="X" l="SPA"><s0>Metal divalente Complejo</s0><s2>NC</s2><s2>NA</s2><s5>02</s5></fC03><fC03 i1="03" i2="X" l="FRE"><s0>Antibactérien</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" l="ENG"><s0>Antibacterial agent</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" 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i1="20" i2="X" l="ENG"><s0>Electrical properties</s0><s5>33</s5></fC03><fC03 i1="20" i2="X" l="SPA"><s0>Propiedad eléctrica</s0><s5>33</s5></fC03><fC03 i1="21" i2="X" l="FRE"><s0>Propriété magnétique</s0><s5>34</s5></fC03><fC03 i1="21" i2="X" l="ENG"><s0>Magnetic properties</s0><s5>34</s5></fC03><fC03 i1="21" i2="X" l="SPA"><s0>Propiedad magnética</s0><s5>34</s5></fC03><fC03 i1="22" i2="X" l="FRE"><s0>Benzènesulfonamide(N-[pyrimidin-2-yl]-4-[5-bromo-2-hydroxybenzylidèneamino])</s0><s2>NK</s2><s2>FC</s2><s4>INC</s4><s5>76</s5></fC03><fC07 i1="01" i2="X" l="FRE"><s0>Métal transition Complexe</s0><s2>NC</s2><s2>NA</s2><s5>13</s5></fC07><fC07 i1="01" i2="X" l="ENG"><s0>Transition metal Complexes</s0><s2>NC</s2><s2>NA</s2><s5>13</s5></fC07><fC07 i1="01" i2="X" l="SPA"><s0>Metal transición Complejo</s0><s2>NC</s2><s2>NA</s2><s5>13</s5></fC07><fN21><s1>284</s1></fN21></pA></standard></inist><affiliations><list><country><li>Maroc</li><li>Pakistan</li></country></list><tree><country name="Pakistan"><noRegion><name sortKey="Chohan, Zahid H" sort="Chohan, Zahid H" uniqKey="Chohan Z" first="Zahid H." last="Chohan">Zahid H. Chohan</name></noRegion><name sortKey="Shad, Hazoor A" sort="Shad, Hazoor A" uniqKey="Shad H" first="Hazoor A." last="Shad">Hazoor A. Shad</name></country><country name="Maroc"><noRegion><name sortKey="Youssoufi, Moulay H" sort="Youssoufi, Moulay H" uniqKey="Youssoufi M" first="Moulay H." last="Youssoufi">Moulay H. Youssoufi</name></noRegion><name sortKey="Taibi Ben Hadda" sort="Taibi Ben Hadda" uniqKey="Taibi Ben Hadda" last="Taibi Ben Hadda">TAIBI BEN HADDA</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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