Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]
Identifieur interne : 000250 ( Ncbi/Curation ); précédent : 000249; suivant : 000251Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]
Auteurs : Asma Lehleh [Algérie] ; Mehdi Boutebdja [Algérie] ; Adel Beghidja [Algérie] ; Chahrazed Beghidja [Algérie] ; Hocine Merazig [Algérie]Source :
- Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2013.
Abstract
The title compound, {[Co(C10H8N2)2(H2O)2](NO3)2·4H2O}
Url:
DOI: 10.1107/S1600536813005230
PubMed: 23633984
PubMed Central: 3629466
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PMC:3629466Le document en format XML
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-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]</title>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Poly[[diaquabis(μ<sub>2</sub>
-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]</title>
<author><name sortKey="Lehleh, Asma" sort="Lehleh, Asma" uniqKey="Lehleh A" first="Asma" last="Lehleh">Asma Lehleh</name>
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<author><name sortKey="Beghidja, Adel" sort="Beghidja, Adel" uniqKey="Beghidja A" first="Adel" last="Beghidja">Adel Beghidja</name>
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</affiliation>
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<author><name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
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<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
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<front><div type="abstract" xml:lang="en"><p>The title compound, {[Co(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
](NO<sub>3</sub>
)<sub>2</sub>
·4H<sub>2</sub>
O}<sub><italic>n</italic>
</sub>
, (C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
= 4,4′-bipyridine = 4,4′-bpy) is a layered coordination polymer built up from a cationic square grid extending in (101) enclosing uncoordinating nitrate ions and water molecules. The Co<sup>II</sup>
ion has site symmetry 2 and one of the 4,4′-bpy ligands is generated by twofold symmetry [two N atoms and two C atoms lie on the rotation axis and the dihedral angle between the pyridine rings is 45.66 (5)°]. The other 4,4′-bpy ligand is generated by a crystallographic inversion center. The Co<sup>II</sup>
ion exhibits a slightly distorted octahedral coordination geometry defined by two O atoms of two coordinating water molecules and four N atoms from four bridging 4,4′-bpy ligands. The structure is consolidated by O—H⋯O, C—H⋯O and C—H⋯N hydrogen bonds.</p>
</div>
</front>
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