CobaltMaghrebV1, Pmc, Curation, bibRecord, 000363

Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]

Identifieur interne : 000363 ( Pmc/Curation ); précédent : 000362; suivant : 000364

Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]

Auteurs : Asma Lehleh [Algérie] ; Mehdi Boutebdja [Algérie] ; Adel Beghidja [Algérie] ; Chahrazed Beghidja [Algérie] ; Hocine Merazig [Algérie]

Source :

Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2013.

RBID : PMC:3629466

Abstract

The title compound, {[Co(C₁₀H₈N₂)₂(H₂O)₂](NO₃)₂·4H₂O}_n, (C₁₀H₈N₂ = 4,4′-bipyridine = 4,4′-bpy) is a layered coordination polymer built up from a cationic square grid extending in (101) enclosing uncoordinating nitrate ions and water molecules. The Co^II ion has site symmetry 2 and one of the 4,4′-bpy ligands is generated by twofold symmetry [two N atoms and two C atoms lie on the rotation axis and the dihedral angle between the pyridine rings is 45.66 (5)°]. The other 4,4′-bpy ligand is generated by a crystallographic inversion center. The Co^II ion exhibits a slightly distorted octahedral coordination geometry defined by two O atoms of two coordinating water molecules and four N atoms from four bridging 4,4′-bpy ligands. The structure is consolidated by O—H⋯O, C—H⋯O and C—H⋯N hydrogen bonds.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3629466

DOI: 10.1107/S1600536813005230
PubMed: 23633984
PubMed Central: 3629466

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-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]</title>
<author><name sortKey="Lehleh, Asma" sort="Lehleh, Asma" uniqKey="Lehleh A" first="Asma" last="Lehleh">Asma Lehleh</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<author><name sortKey="Boutebdja, Mehdi" sort="Boutebdja, Mehdi" uniqKey="Boutebdja M" first="Mehdi" last="Boutebdja">Mehdi Boutebdja</name>
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<author><name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Poly[[diaquabis(μ<sub>2</sub>
-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]</title>
<author><name sortKey="Lehleh, Asma" sort="Lehleh, Asma" uniqKey="Lehleh A" first="Asma" last="Lehleh">Asma Lehleh</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Boutebdja, Mehdi" sort="Boutebdja, Mehdi" uniqKey="Boutebdja M" first="Mehdi" last="Boutebdja">Mehdi Boutebdja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Beghidja, Adel" sort="Beghidja, Adel" uniqKey="Beghidja A" first="Adel" last="Beghidja">Adel Beghidja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Beghidja, Chahrazed" sort="Beghidja, Chahrazed" uniqKey="Beghidja C" first="Chahrazed" last="Beghidja">Chahrazed Beghidja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
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<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2013">2013</date>
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<front><div type="abstract" xml:lang="en"><p>The title compound, {[Co(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
](NO<sub>3</sub>
)<sub>2</sub>
·4H<sub>2</sub>
O}<sub><italic>n</italic>
</sub>
, (C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
 = 4,4′-bipyridine = 4,4′-bpy) is a layered coordination polymer built up from a cationic square grid extending in (101) enclosing uncoordinating nitrate ions and water molecules. The Co<sup>II</sup>
 ion has site symmetry 2 and one of the 4,4′-bpy ligands is generated by twofold symmetry [two N atoms and two C atoms lie on the rotation axis and the dihedral angle between the pyridine rings is 45.66 (5)°]. The other 4,4′-bpy ligand is generated by a crystallographic inversion center. The Co<sup>II</sup>
 ion exhibits a slightly distorted octahedral coordination geometry defined by two O atoms of two coordinating water molecules and four N atoms from four bridging 4,4′-bpy ligands. The structure is consolidated by O—H⋯O, C—H⋯O and C—H⋯N hydrogen bonds.</p>
</div>
</front>
<back><div1 type="bibliography"><listBibl><biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
</listBibl>
</div1>
</back>
</TEI>
<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
  <front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="iso-abbrev">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Structure Reports Online</journal-title>
</journal-title-group>
<issn pub-type="epub">1600-5368</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">23633984</article-id>
<article-id pub-id-type="pmc">3629466</article-id>
<article-id pub-id-type="publisher-id">hb7035</article-id>
<article-id pub-id-type="doi">10.1107/S1600536813005230</article-id>
<article-id pub-id-type="coden">ACSEBH</article-id>
<article-id pub-id-type="pii">S1600536813005230</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Metal-Organic Papers</subject>
</subj-group>
</article-categories>
<title-group><article-title>Poly[[diaquabis(μ<sub>2</sub>
-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]</article-title>
<alt-title><italic>[Co(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
](NO<sub>3</sub>
)<sub>2</sub>
·4H<sub>2</sub>
O</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Lehleh</surname>
<given-names>Asma</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Boutebdja</surname>
<given-names>Mehdi</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Beghidja</surname>
<given-names>Adel</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Beghidja</surname>
<given-names>Chahrazed</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Merazig</surname>
<given-names>Hocine</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<aff id="a"><label>a</label>
Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>a_beghidja@yahoo.fr</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>4</month>
<year>2013</year>
</pub-date>
<pub-date pub-type="epub"><day>02</day>
<month>3</month>
<year>2013</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>02</day>
<month>3</month>
<year>2013</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the 
 							. </pmc-comment>
      <volume>69</volume>
<issue>Pt 4</issue>
<issue-id pub-id-type="publisher-id">e130400</issue-id>
<fpage>m177</fpage>
<lpage>m178</lpage>
<history><date date-type="received"><day>04</day>
<month>2</month>
<year>2013</year>
</date>
<date date-type="accepted"><day>23</day>
<month>2</month>
<year>2013</year>
</date>
</history>
<permissions><copyright-statement>© Lehleh et al. 2013</copyright-statement>
<copyright-year>2013</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S1600536813005230">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract><p>The title compound, {[Co(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
](NO<sub>3</sub>
)<sub>2</sub>
·4H<sub>2</sub>
O}<sub><italic>n</italic>
</sub>
, (C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
 = 4,4′-bipyridine = 4,4′-bpy) is a layered coordination polymer built up from a cationic square grid extending in (101) enclosing uncoordinating nitrate ions and water molecules. The Co<sup>II</sup>
 ion has site symmetry 2 and one of the 4,4′-bpy ligands is generated by twofold symmetry [two N atoms and two C atoms lie on the rotation axis and the dihedral angle between the pyridine rings is 45.66 (5)°]. The other 4,4′-bpy ligand is generated by a crystallographic inversion center. The Co<sup>II</sup>
 ion exhibits a slightly distorted octahedral coordination geometry defined by two O atoms of two coordinating water molecules and four N atoms from four bridging 4,4′-bpy ligands. The structure is consolidated by O—H⋯O, C—H⋯O and C—H⋯N hydrogen bonds.</p>
</abstract>
</article-meta>
</front>
<floats-group><table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Selected bond lengths (Å)</title>
</caption>
<table frame="hsides" rules="groups"><tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—O1<italic>W</italic>
</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.0741 (10)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N1</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.2235 (10)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N2</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.1898 (13)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N3<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.2306 (14)</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry code: (i) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi7.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
<table-wrap id="table2" position="float"><label>Table 2</label>
<caption><title>Hydrogen-bond geometry (Å, °)</title>
</caption>
<table frame="hsides" rules="groups"><thead valign="bottom"><tr><th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom">H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
</tr>
</thead>
<tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H12⋯O3<italic>W</italic>
<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.877 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.801 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.675 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">174.2 (14)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H13⋯O2<italic>W</italic>
<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.884 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.790 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.6744 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">178.7 (16)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O2<italic>W</italic>
—H14⋯O1</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.878 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.959 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.827 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">170.1 (13)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O2<italic>W</italic>
—H15⋯O2<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.882 (14)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.906 (14)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.765 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">164.2 (14)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O3<italic>W</italic>
—H16⋯O1</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.873 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.908 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.769 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">168.9 (14)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O3<italic>W</italic>
—H17⋯O3<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.887 (11)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.109 (11)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.958 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">159.9 (15)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C1—H1⋯O1<italic>W</italic>
<sup>v</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.54</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.0860 (15)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">117</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C11—H11⋯N1<sup>vi</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.58</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.1974 (15)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">124</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C11—H11⋯O3<sup>vii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.46</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.209 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">137</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry codes: (ii) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi8.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iii) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi9.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iv) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi10.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (v) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi11.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (vi) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi12.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (vii) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi13.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
</record>

Pour manipuler ce document sous Unix (Dilib)

EXPLOR_STEP=$WICRI_ROOT/Wicri/Terre/explor/CobaltMaghrebV1/Data/Pmc/Curation

HfdSelect -h $EXPLOR_STEP/biblio.hfd -nk 000363 | SxmlIndent | more

HfdSelect -h $EXPLOR_AREA/Data/Pmc/Curation/biblio.hfd -nk 000363 | SxmlIndent | more

Pour mettre un lien sur cette page dans le réseau Wicri

{{Explor lien
   |wiki=    Wicri/Terre
   |area=    CobaltMaghrebV1
   |flux=    Pmc
   |étape=   Curation
   |type=    RBID
   |clé=     PMC:3629466
   |texte=   Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]
}}

Pour générer des pages wiki

HfdIndexSelect -h $EXPLOR_AREA/Data/Pmc/Curation/RBID.i   -Sk "pubmed:23633984" \
       | HfdSelect -Kh $EXPLOR_AREA/Data/Pmc/Curation/biblio.hfd   \
       | NlmPubMed2Wicri -a CobaltMaghrebV1

This area was generated with Dilib version V0.6.32.
Data generation: Tue Nov 14 12:56:51 2017. Site generation: Mon Feb 12 07:59:49 2024

	Serveur d'exploration sur le cobalt au Maghreb
	Attention, ce site est en cours de développement ! Attention, site généré par des moyens informatiques à partir de corpus bruts. Les informations ne sont donc pas validées.

Serveur d'exploration sur le cobalt au Maghreb

Poly[[diaqua­bis­(μ2-4,4′-bipyrid­yl)cobalt(II)] dinitrate tetra­hydrate]

Poly[[diaqua­bis­(μ2-4,4′-bipyrid­yl)cobalt(II)] dinitrate tetra­hydrate]

Source :

Abstract

Links toward previous steps (curation, corpus...)

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri

Pour générer des pages wiki

Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]

Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]