Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]
Identifieur interne : 000363 ( Pmc/Curation ); précédent : 000362; suivant : 000364Poly[[diaquabis(μ2-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]
Auteurs : Asma Lehleh [Algérie] ; Mehdi Boutebdja [Algérie] ; Adel Beghidja [Algérie] ; Chahrazed Beghidja [Algérie] ; Hocine Merazig [Algérie]Source :
- Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2013.
Abstract
The title compound, {[Co(C10H8N2)2(H2O)2](NO3)2·4H2O}
Url:
DOI: 10.1107/S1600536813005230
PubMed: 23633984
PubMed Central: 3629466
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Poly[[diaquabis(μ<sub>2</sub>
-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]</title>
<author><name sortKey="Lehleh, Asma" sort="Lehleh, Asma" uniqKey="Lehleh A" first="Asma" last="Lehleh">Asma Lehleh</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<author><name sortKey="Boutebdja, Mehdi" sort="Boutebdja, Mehdi" uniqKey="Boutebdja M" first="Mehdi" last="Boutebdja">Mehdi Boutebdja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
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<country xml:lang="fr">Algérie</country>
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<author><name sortKey="Beghidja, Adel" sort="Beghidja, Adel" uniqKey="Beghidja A" first="Adel" last="Beghidja">Adel Beghidja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
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<author><name sortKey="Beghidja, Chahrazed" sort="Beghidja, Chahrazed" uniqKey="Beghidja C" first="Chahrazed" last="Beghidja">Chahrazed Beghidja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
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<author><name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Poly[[diaquabis(μ<sub>2</sub>
-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]</title>
<author><name sortKey="Lehleh, Asma" sort="Lehleh, Asma" uniqKey="Lehleh A" first="Asma" last="Lehleh">Asma Lehleh</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Boutebdja, Mehdi" sort="Boutebdja, Mehdi" uniqKey="Boutebdja M" first="Mehdi" last="Boutebdja">Mehdi Boutebdja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Beghidja, Adel" sort="Beghidja, Adel" uniqKey="Beghidja A" first="Adel" last="Beghidja">Adel Beghidja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Beghidja, Chahrazed" sort="Beghidja, Chahrazed" uniqKey="Beghidja C" first="Chahrazed" last="Beghidja">Chahrazed Beghidja</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
<affiliation wicri:level="1"><nlm:aff id="a">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
</analytic>
<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2013">2013</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
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<front><div type="abstract" xml:lang="en"><p>The title compound, {[Co(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
](NO<sub>3</sub>
)<sub>2</sub>
·4H<sub>2</sub>
O}<sub><italic>n</italic>
</sub>
, (C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
= 4,4′-bipyridine = 4,4′-bpy) is a layered coordination polymer built up from a cationic square grid extending in (101) enclosing uncoordinating nitrate ions and water molecules. The Co<sup>II</sup>
ion has site symmetry 2 and one of the 4,4′-bpy ligands is generated by twofold symmetry [two N atoms and two C atoms lie on the rotation axis and the dihedral angle between the pyridine rings is 45.66 (5)°]. The other 4,4′-bpy ligand is generated by a crystallographic inversion center. The Co<sup>II</sup>
ion exhibits a slightly distorted octahedral coordination geometry defined by two O atoms of two coordinating water molecules and four N atoms from four bridging 4,4′-bpy ligands. The structure is consolidated by O—H⋯O, C—H⋯O and C—H⋯N hydrogen bonds.</p>
</div>
</front>
<back><div1 type="bibliography"><listBibl><biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
</listBibl>
</div1>
</back>
</TEI>
<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
<front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="iso-abbrev">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Structure Reports Online</journal-title>
</journal-title-group>
<issn pub-type="epub">1600-5368</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">23633984</article-id>
<article-id pub-id-type="pmc">3629466</article-id>
<article-id pub-id-type="publisher-id">hb7035</article-id>
<article-id pub-id-type="doi">10.1107/S1600536813005230</article-id>
<article-id pub-id-type="coden">ACSEBH</article-id>
<article-id pub-id-type="pii">S1600536813005230</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Metal-Organic Papers</subject>
</subj-group>
</article-categories>
<title-group><article-title>Poly[[diaquabis(μ<sub>2</sub>
-4,4′-bipyridyl)cobalt(II)] dinitrate tetrahydrate]</article-title>
<alt-title><italic>[Co(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
](NO<sub>3</sub>
)<sub>2</sub>
·4H<sub>2</sub>
O</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Lehleh</surname>
<given-names>Asma</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Boutebdja</surname>
<given-names>Mehdi</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Beghidja</surname>
<given-names>Adel</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Beghidja</surname>
<given-names>Chahrazed</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Merazig</surname>
<given-names>Hocine</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<aff id="a"><label>a</label>
Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale (CHEMS), Faculté des Sciences Exactes, Département de Chimie, Université de Constantine 1, 25000 Constantine,<country>Algeria</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>a_beghidja@yahoo.fr</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>4</month>
<year>2013</year>
</pub-date>
<pub-date pub-type="epub"><day>02</day>
<month>3</month>
<year>2013</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>02</day>
<month>3</month>
<year>2013</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the
. </pmc-comment>
<volume>69</volume>
<issue>Pt 4</issue>
<issue-id pub-id-type="publisher-id">e130400</issue-id>
<fpage>m177</fpage>
<lpage>m178</lpage>
<history><date date-type="received"><day>04</day>
<month>2</month>
<year>2013</year>
</date>
<date date-type="accepted"><day>23</day>
<month>2</month>
<year>2013</year>
</date>
</history>
<permissions><copyright-statement>© Lehleh et al. 2013</copyright-statement>
<copyright-year>2013</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S1600536813005230">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract><p>The title compound, {[Co(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
](NO<sub>3</sub>
)<sub>2</sub>
·4H<sub>2</sub>
O}<sub><italic>n</italic>
</sub>
, (C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
= 4,4′-bipyridine = 4,4′-bpy) is a layered coordination polymer built up from a cationic square grid extending in (101) enclosing uncoordinating nitrate ions and water molecules. The Co<sup>II</sup>
ion has site symmetry 2 and one of the 4,4′-bpy ligands is generated by twofold symmetry [two N atoms and two C atoms lie on the rotation axis and the dihedral angle between the pyridine rings is 45.66 (5)°]. The other 4,4′-bpy ligand is generated by a crystallographic inversion center. The Co<sup>II</sup>
ion exhibits a slightly distorted octahedral coordination geometry defined by two O atoms of two coordinating water molecules and four N atoms from four bridging 4,4′-bpy ligands. The structure is consolidated by O—H⋯O, C—H⋯O and C—H⋯N hydrogen bonds.</p>
</abstract>
</article-meta>
</front>
<floats-group><table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Selected bond lengths (Å)</title>
</caption>
<table frame="hsides" rules="groups"><tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—O1<italic>W</italic>
</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.0741 (10)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N1</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.2235 (10)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N2</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.1898 (13)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N3<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.2306 (14)</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry code: (i) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi7.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
<table-wrap id="table2" position="float"><label>Table 2</label>
<caption><title>Hydrogen-bond geometry (Å, °)</title>
</caption>
<table frame="hsides" rules="groups"><thead valign="bottom"><tr><th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom">H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
</tr>
</thead>
<tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H12⋯O3<italic>W</italic>
<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.877 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.801 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.675 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">174.2 (14)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H13⋯O2<italic>W</italic>
<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.884 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.790 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.6744 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">178.7 (16)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O2<italic>W</italic>
—H14⋯O1</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.878 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.959 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.827 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">170.1 (13)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O2<italic>W</italic>
—H15⋯O2<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.882 (14)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.906 (14)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.765 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">164.2 (14)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O3<italic>W</italic>
—H16⋯O1</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.873 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.908 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.769 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">168.9 (14)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O3<italic>W</italic>
—H17⋯O3<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.887 (11)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.109 (11)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.958 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">159.9 (15)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C1—H1⋯O1<italic>W</italic>
<sup>v</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.54</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.0860 (15)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">117</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C11—H11⋯N1<sup>vi</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.58</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.1974 (15)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">124</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C11—H11⋯O3<sup>vii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.46</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.209 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">137</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry codes: (ii) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi8.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iii) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi9.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iv) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi10.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (v) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi11.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (vi) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi12.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (vii) <inline-formula><inline-graphic xlink:href="e-69-0m177-efi13.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
</record>
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