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Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction

Identifieur interne : 002927 ( Main/Exploration ); précédent : 002926; suivant : 002928

Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction

Auteurs : P. Just [Allemagne] ; U. Greulach [Allemagne] ; G. Henze [Allemagne] ; D. Rinne [Allemagne]

Source :

Fresenius' Journal of Analytical Chemistry [ 0937-0633 ] ; 1995-01-01.

RBID : ISTEX:500A3608B1021BCF936862AE4406F7F7B3899716

Descripteurs français

Pascal (Inist)
- Analyse chimique, Analyse trace, Chromatographie phase gazeuse, Conductimétrie, Dicétone, Détecteur électrochimique, Eau, Eau distribution, Extraction, Fongicide, Hétérocycle oxygène azote, Limite détection, Oxazolidine dérivé, Phase solide, Pollution eau, Ultratrace, Vinclozoline.
Wicri :
- topic : Eau.

English descriptors

KwdEn :
- Chemical analysis, Conductometry, Detection limit, Diketone, Electrochemical detector, Extraction, Fungicide, Gas chromatography, Oxygen nitrogen heterocycle, Solid phase, Tap water, Trace analysis, Water, Water pollution.

Abstract

Abstract: A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step — the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction — was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.

Url:

https://api.istex.fr/document/500A3608B1021BCF936862AE4406F7F7B3899716/fulltext/pdf

DOI: 10.1007/BF00322237

Affiliations:

Le document en format XML

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<front><div type="abstract" xml:lang="en">Abstract: A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step — the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction — was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.</div>
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Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction

Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction

Source :

Descripteurs français

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri

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