Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction
Identifieur interne : 000745 ( Istex/Corpus ); précédent : 000744; suivant : 000746Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction
Auteurs : P. Just ; U. Greulach ; G. Henze ; D. RinneSource :
- Fresenius' Journal of Analytical Chemistry [ 0937-0633 ] ; 1995-01-01.
Abstract
Abstract: A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step — the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction — was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.
Url:
DOI: 10.1007/BF00322237
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ISTEX:500A3608B1021BCF936862AE4406F7F7B3899716Le document en format XML
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Just</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</mods:affiliation></affiliation><affiliation><mods:affiliation>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Greulach, U" sort="Greulach, U" uniqKey="Greulach U" first="U." last="Greulach">U. Greulach</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</mods:affiliation></affiliation><affiliation><mods:affiliation>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Henze, G" sort="Henze, G" uniqKey="Henze G" first="G." last="Henze">G. 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Rinne</name><affiliation><mods:affiliation>Landesamt für Wasserwirtschaft Rheinland-Pfalz, Am Zollhafen 9, D-55116, Mainz, Germany</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j">Fresenius' Journal of Analytical Chemistry</title><title level="j" type="abbrev">Fresenius J Anal Chem</title><idno type="ISSN">0937-0633</idno><idno type="eISSN">1432-1130</idno><imprint><publisher>Springer-Verlag</publisher><pubPlace>Berlin/Heidelberg</pubPlace><date type="published" when="1995-01-01">1995-01-01</date><biblScope unit="volume">352</biblScope><biblScope unit="issue">3-4</biblScope><biblScope unit="page" from="385">385</biblScope><biblScope unit="page" to="387">387</biblScope></imprint><idno type="ISSN">0937-0633</idno></series><idno type="istex">500A3608B1021BCF936862AE4406F7F7B3899716</idno><idno type="DOI">10.1007/BF00322237</idno><idno type="ArticleID">BF00322237</idno><idno type="ArticleID">Art13</idno></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0937-0633</idno></seriesStmt></fileDesc><profileDesc><textClass></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Abstract: A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step — the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction — was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.</div></front></TEI><istex><corpusName>springer</corpusName><author><json:item><name>P. Just</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</json:string><json:string>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</json:string></affiliations></json:item><json:item><name>U. Greulach</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</json:string><json:string>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</json:string></affiliations></json:item><json:item><name>G. Henze</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</json:string><json:string>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</json:string></affiliations></json:item><json:item><name>D. 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The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.</abstract><qualityIndicators><score>3.112</score><pdfVersion>1.3</pdfVersion><pdfPageSize>598 x 785 pts</pdfPageSize><refBibsNative>false</refBibsNative><keywordCount>0</keywordCount><abstractCharCount>668</abstractCharCount><pdfWordCount>1852</pdfWordCount><pdfCharCount>11456</pdfCharCount><pdfPageCount>3</pdfPageCount><abstractWordCount>105</abstractWordCount></qualityIndicators><title>Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction</title><refBibs><json:item><host><author><json:item><name>W Perkow</name></json:item></author><title>Wirksubstanzen der Pflanzenschutz-und Sch~idlingsbekO.mpfungsmittel. 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R. Kakkar with Xma x at 430 nm. The method is highly sensitive. 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electrolytic conductivity detection and solid-phase extraction</title><author xml:id="author-1"><persName><forename type="first">P.</forename><surname>Just</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</affiliation><affiliation>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</affiliation></author><author xml:id="author-2"><persName><forename type="first">U.</forename><surname>Greulach</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</affiliation><affiliation>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</affiliation></author><author xml:id="author-3" corresp="yes"><persName><forename type="first">G.</forename><surname>Henze</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</affiliation><affiliation>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</affiliation></author><author xml:id="author-4"><persName><forename type="first">D.</forename><surname>Rinne</surname></persName><affiliation>Landesamt für Wasserwirtschaft Rheinland-Pfalz, Am Zollhafen 9, D-55116, Mainz, Germany</affiliation></author></analytic><monogr><title level="j">Fresenius' Journal of Analytical Chemistry</title><title level="j" type="abbrev">Fresenius J Anal Chem</title><idno type="journal-ID">216</idno><idno type="pISSN">0937-0633</idno><idno type="eISSN">1432-1130</idno><idno type="issue-article-count">21</idno><idno type="volume-issue-count">8</idno><imprint><publisher>Springer-Verlag</publisher><pubPlace>Berlin/Heidelberg</pubPlace><date type="published" when="1995-01-01"></date><biblScope unit="volume">352</biblScope><biblScope unit="issue">3-4</biblScope><biblScope unit="page" 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Each step — the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction — was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.</p></abstract><textClass><keywords scheme="Journal Subject"><list><head>Chemistry</head><item><term>Analytical Chemistry</term></item><item><term>Food Science</term></item><item><term>Inorganic Chemistry</term></item><item><term>Physical Chemistry</term></item><item><term>Monitoring/Environmental Analysis/Environmental Ecotoxicology</term></item></list></keywords></textClass></profileDesc><revisionDesc><change when="1994-07-12">Created</change><change when="1995-01-01">Published</change><change xml:id="refBibs-istex" who="#ISTEX-API" when="2016-11-22">References added</change><change xml:id="refBibs-istex" who="#ISTEX-API" when="2017-01-21">References 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Note</ArticleCategory><ArticleFirstPage>385</ArticleFirstPage><ArticleLastPage>387</ArticleLastPage><ArticleHistory><RegistrationDate><Year>2004</Year><Month>8</Month><Day>27</Day></RegistrationDate><Received><Year>1994</Year><Month>7</Month><Day>12</Day></Received><Revised><Year>1994</Year><Month>8</Month><Day>25</Day></Revised><Accepted><Year>1995</Year><Month>2</Month><Day>9</Day></Accepted></ArticleHistory><ArticleCopyright><CopyrightHolderName>Springer-Verlag</CopyrightHolderName><CopyrightYear>1995</CopyrightYear></ArticleCopyright><ArticleGrants Type="Regular"><MetadataGrant Grant="OpenAccess"></MetadataGrant><AbstractGrant Grant="OpenAccess"></AbstractGrant><BodyPDFGrant Grant="Restricted"></BodyPDFGrant><BodyHTMLGrant Grant="Restricted"></BodyHTMLGrant><BibliographyGrant Grant="Restricted"></BibliographyGrant><ESMGrant Grant="Restricted"></ESMGrant></ArticleGrants><ArticleContext><JournalID>216</JournalID><VolumeIDStart>352</VolumeIDStart><VolumeIDEnd>352</VolumeIDEnd><IssueIDStart>3</IssueIDStart><IssueIDEnd>4</IssueIDEnd></ArticleContext></ArticleInfo><ArticleHeader><AuthorGroup><Author AffiliationIDS="Aff1 Aff2"><AuthorName DisplayOrder="Western"><GivenName>P.</GivenName><FamilyName>Just</FamilyName></AuthorName></Author><Author AffiliationIDS="Aff1 Aff2"><AuthorName DisplayOrder="Western"><GivenName>U.</GivenName><FamilyName>Greulach</FamilyName></AuthorName></Author><Author AffiliationIDS="Aff1 Aff2" CorrespondingAffiliationID="Aff1"><AuthorName DisplayOrder="Western"><GivenName>G.</GivenName><FamilyName>Henze</FamilyName></AuthorName></Author><Author AffiliationIDS="Aff3"><AuthorName DisplayOrder="Western"><GivenName>D.</GivenName><FamilyName>Rinne</FamilyName></AuthorName></Author><Affiliation ID="Aff1"><OrgDivision>Fachbereich Chemie</OrgDivision><OrgName>Universität Kaiserslautern</OrgName><OrgAddress><Postbox>Postfach 3825</Postbox><Postcode>D-54286</Postcode><City>Trier</City><Country>Germany</Country></OrgAddress></Affiliation><Affiliation ID="Aff2"><OrgDivision>Abteilung für Anorganische und Analytische Chemie</OrgDivision><OrgName>Universität Trier</OrgName><OrgAddress><Postbox>Postfach 3825</Postbox><Postcode>D-54286</Postcode><City>Trier</City><Country>Germany</Country></OrgAddress></Affiliation><Affiliation ID="Aff3"><OrgName>Landesamt für Wasserwirtschaft Rheinland-Pfalz</OrgName><OrgAddress><Street>Am Zollhafen 9</Street><Postcode>D-55116</Postcode><City>Mainz</City><Country>Germany</Country></OrgAddress></Affiliation></AuthorGroup><Abstract ID="Abs1" Language="En"><Heading>Abstract</Heading><Para>A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step — the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction — was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.</Para></Abstract></ArticleHeader><NoBody></NoBody></Article></Issue></Volume></Journal></Publisher></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction</title></titleInfo><name type="personal"><namePart type="given">P.</namePart><namePart type="family">Just</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</affiliation><affiliation>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">U.</namePart><namePart type="family">Greulach</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</affiliation><affiliation>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal" displayLabel="corresp"><namePart type="given">G.</namePart><namePart type="family">Henze</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautern, Postfach 3825, D-54286, Trier, Germany</affiliation><affiliation>Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286, Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">D.</namePart><namePart type="family">Rinne</namePart><affiliation>Landesamt für Wasserwirtschaft Rheinland-Pfalz, Am Zollhafen 9, D-55116, Mainz, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="research-article" displayLabel="OriginalPaper"></genre><originInfo><publisher>Springer-Verlag</publisher><place><placeTerm type="text">Berlin/Heidelberg</placeTerm></place><dateCreated encoding="w3cdtf">1994-07-12</dateCreated><dateIssued encoding="w3cdtf">1995-01-01</dateIssued><copyrightDate encoding="w3cdtf">1995</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="en">Abstract: A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step — the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction — was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.</abstract><note>Current Research Note</note><relatedItem type="host"><titleInfo><title>Fresenius' Journal of Analytical Chemistry</title></titleInfo><titleInfo type="abbreviated"><title>Fresenius J Anal Chem</title></titleInfo><genre type="journal" displayLabel="Archive Journal"></genre><originInfo><dateIssued encoding="w3cdtf">1995-01-01</dateIssued><copyrightDate encoding="w3cdtf">1995</copyrightDate></originInfo><subject><genre>Chemistry</genre><topic>Analytical Chemistry</topic><topic>Food Science</topic><topic>Inorganic Chemistry</topic><topic>Physical Chemistry</topic><topic>Monitoring/Environmental Analysis/Environmental Ecotoxicology</topic></subject><identifier type="ISSN">0937-0633</identifier><identifier type="eISSN">1432-1130</identifier><identifier type="JournalID">216</identifier><identifier type="IssueArticleCount">21</identifier><identifier type="VolumeIssueCount">8</identifier><part><date>1995</date><detail type="volume"><number>352</number><caption>vol.</caption></detail><detail type="issue"><number>3-4</number><caption>no.</caption></detail><extent unit="pages"><start>385</start><end>387</end></extent></part><recordInfo><recordOrigin>Springer-Verlag, 1995</recordOrigin></recordInfo></relatedItem><identifier type="istex">500A3608B1021BCF936862AE4406F7F7B3899716</identifier><identifier type="DOI">10.1007/BF00322237</identifier><identifier type="ArticleID">BF00322237</identifier><identifier type="ArticleID">Art13</identifier><accessCondition type="use and reproduction" contentType="copyright">Springer-Verlag, 1995</accessCondition><recordInfo><recordContentSource>SPRINGER</recordContentSource><recordOrigin>Springer-Verlag, 1995</recordOrigin></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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