UnivTrevesV1, PascalFrancis, Curation, bibRecord, 001504

Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction

Identifieur interne : 001504 ( PascalFrancis/Curation ); précédent : 001503; suivant : 001505

Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction

Auteurs : P. Just [Allemagne] ; U. Greulach [Allemagne] ; G. Henze [Allemagne] ; D. Rinne

Source :

Fresenius' journal of analytical chemistry [ 0937-0633 ] ; 1995.

RBID : Pascal:95-0352416

Descripteurs français

Pascal (Inist)
- Analyse chimique, Analyse trace, Chromatographie phase gazeuse, Détecteur électrochimique, Conductimétrie, Extraction, Phase solide, Fongicide, Hétérocycle oxygène azote, Dicétone, Limite détection, Eau, Eau distribution, Pollution eau, Vinclozoline, Oxazolidine dérivé, Ultratrace.
Wicri :
- topic : Eau.

English descriptors

KwdEn :
- Chemical analysis, Conductometry, Detection limit, Diketone, Electrochemical detector, Extraction, Fungicide, Gas chromatography, Oxygen nitrogen heterocycle, Solid phase, Tap water, Trace analysis, Water, Water pollution.

Abstract

A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step - the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction - was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.

A01	`01`	`1`		`@0 0937-0633`
A03		`1`		`@0 Fresenius' j. anal. chem.`
A05				`@2 352`
A06				`@2 3-4`
A08	`01`	`1`	`ENG`	`@1 Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction`
A11	`01`	`1`		`@1 JUST (P.)`
A11	`02`	`1`		`@1 GREULACH (U.)`
A11	`03`	`1`		`@1 HENZE (G.)`
A11	`04`	`1`		`@1 RINNE (D.)`
A14	`01`			`@1 Univ. Trier, Univ. Kaiserslautern, Fachbereich Chemie @2 54286 Trier @3 DEU @Z 1 aut. @Z 2 aut. @Z 3 aut.`
A20				`@1 385-387`
A21				`@1 1995`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 853 @5 354000050913100130`
A44				`@0 0000`
A45				`@0 10 ref.`
A47	`01`	`1`		`@0 95-0352416`
A60				`@1 P`
A61				`@0 A`
A64	`01`	`1`		`@0 Fresenius' journal of analytical chemistry`
A66	`01`			`@0 DEU`
C01	`01`		`ENG`	@0 A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step - the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction - was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.
C02	`01`	`X`		`@0 001C04B01`
C03	`01`	`X`	`FRE`	`@0 Analyse chimique @5 01`
C03	`01`	`X`	`ENG`	`@0 Chemical analysis @5 01`
C03	`01`	`X`	`GER`	`@0 Chemische Analyse @5 01`
C03	`01`	`X`	`SPA`	`@0 Análisis químico @5 01`
C03	`02`	`X`	`FRE`	`@0 Analyse trace @5 02`
C03	`02`	`X`	`ENG`	`@0 Trace analysis @5 02`
C03	`02`	`X`	`GER`	`@0 Spurenanalyse @5 02`
C03	`02`	`X`	`SPA`	`@0 Análisis huella @5 02`
C03	`03`	`X`	`FRE`	`@0 Chromatographie phase gazeuse @5 03`
C03	`03`	`X`	`ENG`	`@0 Gas chromatography @5 03`
C03	`03`	`X`	`GER`	`@0 Gaschromatographie @5 03`
C03	`03`	`X`	`SPA`	`@0 Cromatografía fase gaseosa @5 03`
C03	`04`	`X`	`FRE`	`@0 Détecteur électrochimique @5 04`
C03	`04`	`X`	`ENG`	`@0 Electrochemical detector @5 04`
C03	`04`	`X`	`SPA`	`@0 Detector electroquímico @5 04`
C03	`05`	`X`	`FRE`	`@0 Conductimétrie @5 05`
C03	`05`	`X`	`ENG`	`@0 Conductometry @5 05`
C03	`05`	`X`	`GER`	`@0 Konduktometrische Titration @5 05`
C03	`05`	`X`	`SPA`	`@0 Conductometría @5 05`
C03	`06`	`X`	`FRE`	`@0 Extraction @5 06`
C03	`06`	`X`	`ENG`	`@0 Extraction @5 06`
C03	`06`	`X`	`SPA`	`@0 Extracción @5 06`
C03	`07`	`X`	`FRE`	`@0 Phase solide @5 07`
C03	`07`	`X`	`ENG`	`@0 Solid phase @5 07`
C03	`07`	`X`	`SPA`	`@0 Fase sólida @5 07`
C03	`08`	`X`	`FRE`	`@0 Fongicide @5 08`
C03	`08`	`X`	`ENG`	`@0 Fungicide @5 08`
C03	`08`	`X`	`SPA`	`@0 Fungicida @5 08`
C03	`09`	`X`	`FRE`	`@0 Hétérocycle oxygène azote @5 10`
C03	`09`	`X`	`ENG`	`@0 Oxygen nitrogen heterocycle @5 10`
C03	`09`	`X`	`SPA`	`@0 Heterociclo oxígeno nitrógeno @5 10`
C03	`10`	`X`	`FRE`	`@0 Dicétone @5 11`
C03	`10`	`X`	`ENG`	`@0 Diketone @5 11`
C03	`10`	`X`	`SPA`	`@0 Dicetona @5 11`
C03	`11`	`X`	`FRE`	`@0 Limite détection @5 12`
C03	`11`	`X`	`ENG`	`@0 Detection limit @5 12`
C03	`11`	`X`	`GER`	`@0 Nachweisgrenze @5 12`
C03	`11`	`X`	`SPA`	`@0 Límite detección @5 12`
C03	`12`	`X`	`FRE`	`@0 Eau @1 SUB @5 15`
C03	`12`	`X`	`ENG`	`@0 Water @1 SUB @5 15`
C03	`12`	`X`	`GER`	`@0 Wasser @1 SUB @5 15`
C03	`12`	`X`	`SPA`	`@0 Agua @1 SUB @5 15`
C03	`13`	`X`	`FRE`	`@0 Eau distribution @5 16`
C03	`13`	`X`	`ENG`	`@0 Tap water @5 16`
C03	`13`	`X`	`SPA`	`@0 Agua distribución @5 16`
C03	`14`	`X`	`FRE`	`@0 Pollution eau @5 17`
C03	`14`	`X`	`ENG`	`@0 Water pollution @5 17`
C03	`14`	`X`	`GER`	`@0 Wasserverschmutzung @5 17`
C03	`14`	`X`	`SPA`	`@0 Contaminación agua @5 17`
C03	`15`	`X`	`FRE`	`@0 Vinclozoline @2 FF @4 INC @5 32`
C03	`16`	`X`	`FRE`	`@0 Oxazolidine dérivé @2 NK @4 INC @5 33`
C03	`17`	`X`	`FRE`	`@0 Ultratrace @4 INC @5 34`
N21				`@1 199`

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Le document en format XML

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<front><div type="abstract" xml:lang="en">A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step - the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction - was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.</div>
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<fC01 i1="01" l="ENG"><s0>A procedure for the analysis of vinclozoline in tap and surface water by GC and Hall detector has been developed. Each step - the analysis of vinclozoline in acetone standard solution, in deionized water and in tap water after solid-phase extraction - was checked by statistical tests (variance homogeneity, linearity test, residue analysis, runaway tests, F-test, t-test). The detection limits and determination limits were calculated from the calibration curve and its prediction interval (according to the DFG). The detection limit for vinclozoline in tap water was found to be 0.03 μg/l and the determination limit is 0.06 μg/l by a recovery rate of 89%.</s0>
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<fC02 i1="01" i2="X"><s0>001C04B01</s0>
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<s5>01</s5>
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<s5>01</s5>
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<s5>01</s5>
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<s5>01</s5>
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<s5>02</s5>
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<fC03 i1="02" i2="X" l="ENG"><s0>Trace analysis</s0>
<s5>02</s5>
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<s5>02</s5>
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<s5>02</s5>
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<s5>03</s5>
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<fC03 i1="03" i2="X" l="ENG"><s0>Gas chromatography</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="GER"><s0>Gaschromatographie</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA"><s0>Cromatografía fase gaseosa</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE"><s0>Détecteur électrochimique</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG"><s0>Electrochemical detector</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA"><s0>Detector electroquímico</s0>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE"><s0>Conductimétrie</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="ENG"><s0>Conductometry</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="GER"><s0>Konduktometrische Titration</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="SPA"><s0>Conductometría</s0>
<s5>05</s5>
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<s5>06</s5>
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<fC03 i1="06" i2="X" l="ENG"><s0>Extraction</s0>
<s5>06</s5>
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<fC03 i1="06" i2="X" l="SPA"><s0>Extracción</s0>
<s5>06</s5>
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<fC03 i1="07" i2="X" l="FRE"><s0>Phase solide</s0>
<s5>07</s5>
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<fC03 i1="07" i2="X" l="ENG"><s0>Solid phase</s0>
<s5>07</s5>
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<fC03 i1="07" i2="X" l="SPA"><s0>Fase sólida</s0>
<s5>07</s5>
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<s5>08</s5>
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<s5>08</s5>
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<s5>08</s5>
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<s5>10</s5>
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<s5>10</s5>
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<s5>10</s5>
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<fC03 i1="10" i2="X" l="FRE"><s0>Dicétone</s0>
<s5>11</s5>
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<fC03 i1="10" i2="X" l="ENG"><s0>Diketone</s0>
<s5>11</s5>
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<fC03 i1="10" i2="X" l="SPA"><s0>Dicetona</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Limite détection</s0>
<s5>12</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Detection limit</s0>
<s5>12</s5>
</fC03>
<fC03 i1="11" i2="X" l="GER"><s0>Nachweisgrenze</s0>
<s5>12</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Límite detección</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Eau</s0>
<s1>SUB</s1>
<s5>15</s5>
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<fC03 i1="12" i2="X" l="ENG"><s0>Water</s0>
<s1>SUB</s1>
<s5>15</s5>
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<fC03 i1="12" i2="X" l="GER"><s0>Wasser</s0>
<s1>SUB</s1>
<s5>15</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Agua</s0>
<s1>SUB</s1>
<s5>15</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Eau distribution</s0>
<s5>16</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Tap water</s0>
<s5>16</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Agua distribución</s0>
<s5>16</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>Pollution eau</s0>
<s5>17</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>Water pollution</s0>
<s5>17</s5>
</fC03>
<fC03 i1="14" i2="X" l="GER"><s0>Wasserverschmutzung</s0>
<s5>17</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Contaminación agua</s0>
<s5>17</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Vinclozoline</s0>
<s2>FF</s2>
<s4>INC</s4>
<s5>32</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>Oxazolidine dérivé</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>33</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Ultratrace</s0>
<s4>INC</s4>
<s5>34</s5>
</fC03>
<fN21><s1>199</s1>
</fN21>
</pA>
</standard>
</inist>
</record>

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   |texte=   Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction
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Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction

Trace analysis of vinclozoline by gas chromatography with electrolytic conductivity detection and solid-phase extraction

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