Tunable acid-sensitive ester protecting groups in oligosaccharide synthesis.
Identifieur interne : 000D28 ( PubMed/Checkpoint ); précédent : 000D27; suivant : 000D29Tunable acid-sensitive ester protecting groups in oligosaccharide synthesis.
Auteurs : Yao Li [États-Unis] ; Xinyu LiuSource :
- Chemical communications (Cambridge, England) [ 1364-548X ] ; 2014.
Descripteurs français
- KwdFr :
- MESH :
- synthèse chimique : Oligosaccharides.
- Acides, Esters, Oligosaccharides, Structure moléculaire.
English descriptors
- KwdEn :
- MESH :
- chemical , chemical synthesis : Oligosaccharides.
- chemical , chemistry : Acids, Esters, Oligosaccharides.
- Molecular Structure.
Abstract
A series of acid-cleavable ester-type protecting groups, with acid-sensitivity profiles parallel to those of 2-naphthylmethyl (NAP) or p-methoxybenzyl (PMB) ether, were designed and TFA in toluene was identified as a technically simple and effective deblocking cocktail for their global removal in the context of oligosaccharide synthesis.
DOI: 10.1039/c3cc49205b
PubMed: 24519721
Affiliations:
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Links to Exploration step
pubmed:24519721Le document en format XML
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<front><div type="abstract" xml:lang="en">A series of acid-cleavable ester-type protecting groups, with acid-sensitivity profiles parallel to those of 2-naphthylmethyl (NAP) or p-methoxybenzyl (PMB) ether, were designed and TFA in toluene was identified as a technically simple and effective deblocking cocktail for their global removal in the context of oligosaccharide synthesis.</div>
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