PittsburghV1, PubMed, Corpus, bibRecord, 003883

Tunable acid-sensitive ester protecting groups in oligosaccharide synthesis.

Identifieur interne : 003883 ( PubMed/Corpus ); précédent : 003882; suivant : 003884

Tunable acid-sensitive ester protecting groups in oligosaccharide synthesis.

Auteurs : Yao Li ; Xinyu Liu

Source :

Chemical communications (Cambridge, England) [ 1364-548X ] ; 2014.

RBID : pubmed:24519721

English descriptors

KwdEn :
- Acids (chemistry), Esters (chemistry), Molecular Structure, Oligosaccharides (chemical synthesis), Oligosaccharides (chemistry).
MESH :
- chemical , chemical synthesis : Oligosaccharides.
- chemical , chemistry : Acids, Esters, Oligosaccharides.
- Molecular Structure.

Abstract

A series of acid-cleavable ester-type protecting groups, with acid-sensitivity profiles parallel to those of 2-naphthylmethyl (NAP) or p-methoxybenzyl (PMB) ether, were designed and TFA in toluene was identified as a technically simple and effective deblocking cocktail for their global removal in the context of oligosaccharide synthesis.

DOI: 10.1039/c3cc49205b
PubMed: 24519721

Links to Exploration step

pubmed:24519721

Le document en format XML

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<author><name sortKey="Li, Yao" sort="Li, Yao" uniqKey="Li Y" first="Yao" last="Li">Yao Li</name>
<affiliation><nlm:affiliation>Department of Chemistry, University of Pittsburgh, 219 Parkman Avenue, Pittsburgh, PA 15260, USA. xinyuliu@pitt.edu.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Liu, Xinyu" sort="Liu, Xinyu" uniqKey="Liu X" first="Xinyu" last="Liu">Xinyu Liu</name>
</author>
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<sourceDesc><biblStruct><analytic><title xml:lang="en">Tunable acid-sensitive ester protecting groups in oligosaccharide synthesis.</title>
<author><name sortKey="Li, Yao" sort="Li, Yao" uniqKey="Li Y" first="Yao" last="Li">Yao Li</name>
<affiliation><nlm:affiliation>Department of Chemistry, University of Pittsburgh, 219 Parkman Avenue, Pittsburgh, PA 15260, USA. xinyuliu@pitt.edu.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Liu, Xinyu" sort="Liu, Xinyu" uniqKey="Liu X" first="Xinyu" last="Liu">Xinyu Liu</name>
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<series><title level="j">Chemical communications (Cambridge, England)</title>
<idno type="eISSN">1364-548X</idno>
<imprint><date when="2014" type="published">2014</date>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Acids (chemistry)</term>
<term>Esters (chemistry)</term>
<term>Molecular Structure</term>
<term>Oligosaccharides (chemical synthesis)</term>
<term>Oligosaccharides (chemistry)</term>
</keywords>
<keywords scheme="MESH" type="chemical" qualifier="chemical synthesis" xml:lang="en"><term>Oligosaccharides</term>
</keywords>
<keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Acids</term>
<term>Esters</term>
<term>Oligosaccharides</term>
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<front><div type="abstract" xml:lang="en">A series of acid-cleavable ester-type protecting groups, with acid-sensitivity profiles parallel to those of 2-naphthylmethyl (NAP) or p-methoxybenzyl (PMB) ether, were designed and TFA in toluene was identified as a technically simple and effective deblocking cocktail for their global removal in the context of oligosaccharide synthesis.</div>
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<DateCreated><Year>2014</Year>
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<DateCompleted><Year>2014</Year>
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<DateRevised><Year>2014</Year>
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<Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1364-548X</ISSN>
<JournalIssue CitedMedium="Internet"><Volume>50</Volume>
<Issue>24</Issue>
<PubDate><Year>2014</Year>
<Month>Mar</Month>
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<Title>Chemical communications (Cambridge, England)</Title>
<ISOAbbreviation>Chem. Commun. (Camb.)</ISOAbbreviation>
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<ArticleTitle>Tunable acid-sensitive ester protecting groups in oligosaccharide synthesis.</ArticleTitle>
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<Abstract><AbstractText>A series of acid-cleavable ester-type protecting groups, with acid-sensitivity profiles parallel to those of 2-naphthylmethyl (NAP) or p-methoxybenzyl (PMB) ether, were designed and TFA in toluene was identified as a technically simple and effective deblocking cocktail for their global removal in the context of oligosaccharide synthesis.</AbstractText>
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<AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Li</LastName>
<ForeName>Yao</ForeName>
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<AffiliationInfo><Affiliation>Department of Chemistry, University of Pittsburgh, 219 Parkman Avenue, Pittsburgh, PA 15260, USA. xinyuliu@pitt.edu.</Affiliation>
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<Author ValidYN="Y"><LastName>Liu</LastName>
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<ArticleDate DateType="Electronic"><Year>2014</Year>
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<Day>12</Day>
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<MedlineJournalInfo><Country>England</Country>
<MedlineTA>Chem Commun (Camb)</MedlineTA>
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<ChemicalList><Chemical><RegistryNumber>0</RegistryNumber>
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<MeshHeading><DescriptorName UI="D015394" MajorTopicYN="N">Molecular Structure</DescriptorName>
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<MeshHeading><DescriptorName UI="D009844" MajorTopicYN="N">Oligosaccharides</DescriptorName>
<QualifierName UI="Q000138" MajorTopicYN="Y">chemical synthesis</QualifierName>
<QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName>
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Tunable acid-sensitive ester protecting groups in oligosaccharide synthesis.

Tunable acid-sensitive ester protecting groups in oligosaccharide synthesis.

Source :

English descriptors

Abstract

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri

Pour générer des pages wiki