Three‐Dimensional Visualization of Defects Formed during the Synthesis of Metal–Organic Frameworks: A Fluorescence Microscopy Study
Identifieur interne : 000D22 ( Istex/Corpus ); précédent : 000D21; suivant : 000D23Three‐Dimensional Visualization of Defects Formed during the Synthesis of Metal–Organic Frameworks: A Fluorescence Microscopy Study
Auteurs : Ameloot ; Frederik Vermoortele ; Hofkens ; De Schryver ; De Vos ; RoeffaersSource :
- Angewandte Chemie [ 0044-8249 ] ; 2013-01-02.
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Abstract
Kleinste Fehler gnadenlos aufgedeckt: Mithilfe von Fluoreszenzmikroskopie sind Defekte in Metall‐organischen Gerüsten erkennbar, die während der Synthese entstehen. Gegenüber gängigen Techniken bietet die konfokale Fluoreszenzmikroskopie den Vorteil einer dreidimensionalen Wiedergabe von einzelnen Einkristallen sowie die erforderliche Empfindlichkeit, um den Beginn einer Defektbildung aufzuzeigen.
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DOI: 10.1002/ange.201205627
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Gegenüber gängigen Techniken bietet die konfokale Fluoreszenzmikroskopie den Vorteil einer dreidimensionalen Wiedergabe von einzelnen Einkristallen sowie die erforderliche Empfindlichkeit, um den Beginn einer Defektbildung aufzuzeigen.</div></front></TEI><istex><corpusName>wiley</corpusName><author><json:item><name>Dr. Ameloot</name><affiliations><json:string>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</json:string></affiliations></json:item><json:item><name>Frederik Vermoortele</name><affiliations><json:string>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</json:string></affiliations></json:item><json:item><name>Prof. Hofkens</name><affiliations><json:string>Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium)</json:string></affiliations></json:item><json:item><name>Prof. De Schryver</name><affiliations><json:string>Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium)</json:string></affiliations></json:item><json:item><name>Prof. De Vos</name><affiliations><json:string>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</json:string></affiliations></json:item><json:item><name>Prof. Roeffaers</name><affiliations><json:string>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</json:string></affiliations></json:item></author><subject><json:item><lang><json:string>eng</json:string></lang><value>Fluoreszenz</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Fluoreszenzmikroskopie</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Kristallwachstum</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Metall‐organische Gerüstverbindungen</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Mikroporöse Materialien</value></json:item></subject><articleId><json:string>ANGE201205627</json:string></articleId><language><json:string>eng</json:string></language><originalGenre><json:string>shortCommunication</json:string></originalGenre><abstract>Kleinste Fehler gnadenlos aufgedeckt: Mithilfe von Fluoreszenzmikroskopie sind Defekte in Metall‐organischen Gerüsten erkennbar, die während der Synthese entstehen. Gegenüber gängigen Techniken bietet die konfokale Fluoreszenzmikroskopie den Vorteil einer dreidimensionalen Wiedergabe von einzelnen Einkristallen sowie die erforderliche Empfindlichkeit, um den Beginn einer Defektbildung aufzuzeigen.</abstract><qualityIndicators><score>5.059</score><pdfVersion>1.4</pdfVersion><pdfPageSize>595.276 x 841.89 pts (A4)</pdfPageSize><refBibsNative>true</refBibsNative><keywordCount>5</keywordCount><abstractCharCount>400</abstractCharCount><pdfWordCount>4043</pdfWordCount><pdfCharCount>24432</pdfCharCount><pdfPageCount>5</pdfPageCount><abstractWordCount>43</abstractWordCount></qualityIndicators><title>Three‐Dimensional Visualization of Defects Formed during the Synthesis of Metal–Organic Frameworks: A Fluorescence Microscopy Study</title><genre><json:string>brief-communication</json:string></genre><host><volume>125</volume><publisherId><json:string>ANGE</json:string></publisherId><pages><total>5</total><last>423</last><first>419</first></pages><issn><json:string>0044-8249</json:string></issn><issue>1</issue><subject><json:item><value>Zuschrift</value></json:item></subject><genre><json:string>journal</json:string></genre><language><json:string>unknown</json:string></language><eissn><json:string>1521-3757</json:string></eissn><title>Angewandte Chemie</title><doi><json:string>10.1002/(ISSN)1521-3757</json:string></doi></host><publicationDate>2013</publicationDate><copyrightDate>2013</copyrightDate><doi><json:string>10.1002/ange.201205627</json:string></doi><id>A7515CC42322A60E2FEE2F1C8EB423B2A1162C7D</id><score>0.25446233</score><fulltext><json:item><original>true</original><mimetype>application/pdf</mimetype><extension>pdf</extension><uri>https://api.istex.fr/document/A7515CC42322A60E2FEE2F1C8EB423B2A1162C7D/fulltext/pdf</uri></json:item><json:item><original>false</original><mimetype>application/zip</mimetype><extension>zip</extension><uri>https://api.istex.fr/document/A7515CC42322A60E2FEE2F1C8EB423B2A1162C7D/fulltext/zip</uri></json:item><istex:fulltextTEI uri="https://api.istex.fr/document/A7515CC42322A60E2FEE2F1C8EB423B2A1162C7D/fulltext/tei"><teiHeader><fileDesc><titleStmt><title level="a" type="main" xml:lang="en">Three‐Dimensional Visualization of Defects Formed during the Synthesis of Metal–Organic Frameworks: A Fluorescence Microscopy Study</title></titleStmt><publicationStmt><authority>ISTEX</authority><publisher>WILEY‐VCH Verlag</publisher><pubPlace>Weinheim</pubPlace><availability><p>© 2013 The Authors. Published by Wiley‐VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution Non‐Commercial License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited and is not used for commercial purposes.</p></availability><date>2013</date></publicationStmt><notesStmt><note type="content">*This research was supported financially by Belspo (IAP 7), the Flemish government (long‐term structural funding—Methusalem funding CASAS METH/08/04), FWO Vlaanderen (postdoctoral research fellowship to R.A.), and the European Research Council (ERC Starting Grant 307523 to M.B.J.R.).</note><note>Funded Access</note><note>Belspo</note><note>Flemish government - No. METH/08/04;</note><note>European Research Council - No. 307523;</note></notesStmt><sourceDesc><biblStruct type="inbook"><analytic><title level="a" type="main" xml:lang="en">Three‐Dimensional Visualization of Defects Formed during the Synthesis of Metal–Organic Frameworks: A Fluorescence Microscopy Study</title><author xml:id="author-1"><persName><surname>Ameloot</surname></persName><roleName type="degree">Dr.</roleName><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation></author><author xml:id="author-2"><persName><forename type="first">Frederik</forename><surname>Vermoortele</surname></persName><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation></author><author xml:id="author-3"><persName><surname>Hofkens</surname></persName><roleName type="degree">Prof.</roleName><affiliation>Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium)</affiliation></author><author xml:id="author-4"><persName><surname>De Schryver</surname></persName><roleName type="degree">Prof.</roleName><affiliation>Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium)</affiliation></author><author xml:id="author-5"><persName><surname>De Vos</surname></persName><roleName type="degree">Prof.</roleName><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation></author><author xml:id="author-6"><persName><surname>Roeffaers</surname></persName><roleName type="degree">Prof.</roleName><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation></author></analytic><monogr><title level="j">Angewandte Chemie</title><title level="j" type="abbrev">Angew. 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J.</givenNames><familyName>Roeffaers</familyName></personName><contactDetails><email>maarten.roeffaers@biw.kuleuven.be</email></contactDetails></creator></creators><affiliationGroup><affiliation xml:id="aa" type="organization"><unparsedAffiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</unparsedAffiliation></affiliation><affiliation xml:id="ab" type="organization"><unparsedAffiliation>Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium)</unparsedAffiliation></affiliation></affiliationGroup><keywordGroup xml:lang="en" type="author"><keyword xml:id="kwd1">Fluoreszenz</keyword><keyword xml:id="kwd2">Fluoreszenzmikroskopie</keyword><keyword xml:id="kwd3">Kristallwachstum</keyword><keyword xml:id="kwd4">Metall‐organische Gerüstverbindungen</keyword><keyword xml:id="kwd5">Mikroporöse Materialien</keyword></keywordGroup><fundingInfo><fundingAgency>Funded Access</fundingAgency></fundingInfo><fundingInfo><fundingAgency>Belspo</fundingAgency></fundingInfo><fundingInfo><fundingAgency>Flemish government</fundingAgency><fundingNumber>METH/08/04</fundingNumber></fundingInfo><fundingInfo><fundingAgency>European Research Council</fundingAgency><fundingNumber>307523</fundingNumber></fundingInfo><supportingInformation><p>As a service to our authors and readers, this journal provides supporting information supplied by the authors. Such materials are peer reviewed and may be re‐organized for online delivery, but are not copy‐edited or typeset. Technical support issues arising from supporting information (other than missing files) should be addressed to the authors. </p><supportingInfoItem><mediaResource alt="supporting information" href="urn-x:wiley:00448249:media:ange201205627:ange_201205627_sm_miscellaneous_information"></mediaResource><caption>miscellaneous_information</caption></supportingInfoItem><supportingInfoItem><mediaResource alt="supporting information" href="urn-x:wiley:00448249:media:ange201205627:ange_201205627_sm_movie_cubtc"></mediaResource><caption>movie_cubtc</caption></supportingInfoItem><supportingInfoItem><mediaResource alt="supporting information" href="urn-x:wiley:00448249:media:ange201205627:ange_201205627_sm_movie_mof-5"></mediaResource><caption>movie_mof‐5</caption></supportingInfoItem></supportingInformation><abstractGroup><abstract type="graphical" xml:lang="de"><p><b>Kleinste Fehler gnadenlos aufgedeckt</b>: Mithilfe von Fluoreszenzmikroskopie sind Defekte in Metall‐organischen Gerüsten erkennbar, die während der Synthese entstehen. Gegenüber gängigen Techniken bietet die konfokale Fluoreszenzmikroskopie den Vorteil einer dreidimensionalen Wiedergabe von einzelnen Einkristallen sowie die erforderliche Empfindlichkeit, um den Beginn einer Defektbildung aufzuzeigen.<blockFixed type="graphic"><mediaResourceGroup><mediaResource alt="image" eRights="yes" copyright="WILEY-VCH" href="urn:x-wiley:00448249:media:ANGE201205627:content"></mediaResource></mediaResourceGroup></blockFixed></p></abstract></abstractGroup></contentMeta><noteGroup><note xml:id="nss"><p>This research was supported financially by Belspo (IAP 7), the Flemish government (long‐term structural funding—Methusalem funding CASAS METH/08/04), FWO Vlaanderen (postdoctoral research fellowship to R.A.), and the European Research Council (ERC Starting Grant 307523 to M.B.J.R.).</p></note></noteGroup></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Three‐Dimensional Visualization of Defects Formed during the Synthesis of Metal–Organic Frameworks: A Fluorescence Microscopy Study</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Three‐Dimensional Visualization of Defects Formed during the Synthesis of Metal–Organic Frameworks: A Fluorescence Microscopy Study</title></titleInfo><name type="personal"><namePart type="termsOfAddress">Dr.</namePart><namePart type="family">Ameloot</namePart><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Frederik</namePart><namePart type="family">Vermoortele</namePart><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="termsOfAddress">Prof.</namePart><namePart type="family">Hofkens</namePart><affiliation>Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium)</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="termsOfAddress">Prof.</namePart><namePart type="family">De Schryver</namePart><affiliation>Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium)</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="termsOfAddress">Prof.</namePart><namePart type="family">De Vos</namePart><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="termsOfAddress">Prof.</namePart><namePart type="family">Roeffaers</namePart><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation><affiliation>Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="brief-communication" displayLabel="shortCommunication"></genre><originInfo><publisher>WILEY‐VCH Verlag</publisher><place><placeTerm type="text">Weinheim</placeTerm></place><dateIssued encoding="w3cdtf">2013-01-02</dateIssued><dateCaptured encoding="w3cdtf">2012-07-16</dateCaptured><copyrightDate encoding="w3cdtf">2013</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType><extent unit="figures">5</extent><extent unit="references">46</extent></physicalDescription><abstract>Kleinste Fehler gnadenlos aufgedeckt: Mithilfe von Fluoreszenzmikroskopie sind Defekte in Metall‐organischen Gerüsten erkennbar, die während der Synthese entstehen. Gegenüber gängigen Techniken bietet die konfokale Fluoreszenzmikroskopie den Vorteil einer dreidimensionalen Wiedergabe von einzelnen Einkristallen sowie die erforderliche Empfindlichkeit, um den Beginn einer Defektbildung aufzuzeigen.</abstract><note type="content">*This research was supported financially by Belspo (IAP 7), the Flemish government (long‐term structural funding—Methusalem funding CASAS METH/08/04), FWO Vlaanderen (postdoctoral research fellowship to R.A.), and the European Research Council (ERC Starting Grant 307523 to M.B.J.R.).</note><note type="funding">Funded Access</note><note type="funding">Belspo</note><note type="funding">Flemish government - No. METH/08/04; </note><note type="funding">European Research Council - No. 307523; </note><subject lang="en"><genre>keywords</genre><topic>Fluoreszenz</topic><topic>Fluoreszenzmikroskopie</topic><topic>Kristallwachstum</topic><topic>Metall‐organische Gerüstverbindungen</topic><topic>Mikroporöse Materialien</topic></subject><relatedItem type="host"><titleInfo><title>Angewandte Chemie</title></titleInfo><titleInfo type="abbreviated"><title>Angew. Chem.</title></titleInfo><genre type="journal">journal</genre><note type="content"> As a service to our authors and readers, this journal provides supporting information supplied by the authors. Such materials are peer reviewed and may be re‐organized for online delivery, but are not copy‐edited or typeset. Technical support issues arising from supporting information (other than missing files) should be addressed to the authors.Supporting Info Item: miscellaneous_information - movie_cubtc - movie_mof‐5 - </note><subject><genre>article-category</genre><topic>Zuschrift</topic></subject><identifier type="ISSN">0044-8249</identifier><identifier type="eISSN">1521-3757</identifier><identifier type="DOI">10.1002/(ISSN)1521-3757</identifier><identifier type="PublisherID">ANGE</identifier><part><date>2013</date><detail type="volume"><caption>vol.</caption><number>125</number></detail><detail type="issue"><caption>no.</caption><number>1</number></detail><extent unit="pages"><start>419</start><end>423</end><total>5</total></extent></part></relatedItem><identifier type="istex">A7515CC42322A60E2FEE2F1C8EB423B2A1162C7D</identifier><identifier type="DOI">10.1002/ange.201205627</identifier><identifier type="ArticleID">ANGE201205627</identifier><accessCondition type="use and reproduction" contentType="copyright">© 2013 The Authors. Published by Wiley‐VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution Non‐Commercial License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited and is not used for commercial purposes.</accessCondition><recordInfo><recordContentSource>WILEY</recordContentSource><recordOrigin>WILEY‐VCH Verlag</recordOrigin></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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