Poly[diaqua-penta-kis(μ(4)-benzene-1,2-dicarboxyl-ato)(μ(3)-benzene-1,2-dicarboxyl-ato)tetra-thulium(III)].
Identifieur interne : 000601 ( PubMed/Curation ); précédent : 000600; suivant : 000602Poly[diaqua-penta-kis(μ(4)-benzene-1,2-dicarboxyl-ato)(μ(3)-benzene-1,2-dicarboxyl-ato)tetra-thulium(III)].
Auteurs : Guo-Ming Wang [République populaire de Chine] ; Chun-Sheng Duan ; Hui-Luan Liu ; Hui LiSource :
- Acta crystallographica. Section E, Structure reports online [ 1600-5368 ] ; 2008.
Abstract
The title compound, [Tm(4)(C(8)H(4)O(4))(6)(H(2)O)(2)](n), has been synthesized hydro-thermally. The asymmetric unit has four unique Tm(III) ions that are six-, seven-, eight- and nine-coordinate. The cations are inter-connected by bridging benzene-1,2-dicarboxyl-ate (BDC) anions to form an infinite two-dimensional framework, in which the BDC ligands adopt three different coordination modes. Adjacent sheets are further packed to form a three-dimensional supra-molecular framework through O-H⋯O hydrogen bonds.
DOI: 10.1107/S1600536808003620
PubMed: 21201858
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<author><name sortKey="Wang, Guo Ming" sort="Wang, Guo Ming" uniqKey="Wang G" first="Guo-Ming" last="Wang">Guo-Ming Wang</name>
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<author><name sortKey="Duan, Chun Sheng" sort="Duan, Chun Sheng" uniqKey="Duan C" first="Chun-Sheng" last="Duan">Chun-Sheng Duan</name>
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<author><name sortKey="Liu, Hui Luan" sort="Liu, Hui Luan" uniqKey="Liu H" first="Hui-Luan" last="Liu">Hui-Luan Liu</name>
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<front><div type="abstract" xml:lang="en">The title compound, [Tm(4)(C(8)H(4)O(4))(6)(H(2)O)(2)](n), has been synthesized hydro-thermally. The asymmetric unit has four unique Tm(III) ions that are six-, seven-, eight- and nine-coordinate. The cations are inter-connected by bridging benzene-1,2-dicarboxyl-ate (BDC) anions to form an infinite two-dimensional framework, in which the BDC ligands adopt three different coordination modes. Adjacent sheets are further packed to form a three-dimensional supra-molecular framework through O-H⋯O hydrogen bonds.</div>
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<Abstract><AbstractText>The title compound, [Tm(4)(C(8)H(4)O(4))(6)(H(2)O)(2)](n), has been synthesized hydro-thermally. The asymmetric unit has four unique Tm(III) ions that are six-, seven-, eight- and nine-coordinate. The cations are inter-connected by bridging benzene-1,2-dicarboxyl-ate (BDC) anions to form an infinite two-dimensional framework, in which the BDC ligands adopt three different coordination modes. Adjacent sheets are further packed to form a three-dimensional supra-molecular framework through O-H⋯O hydrogen bonds.</AbstractText>
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<CommentsCorrections RefType="Cites"><RefSource>Chem Commun (Camb). 2003 Jun 21;(12):1346-7</RefSource>
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