ThuliumV1, PubMed, Corpus, bibRecord, 000602

Poly[tetra-aqua-μ(4)-bromido-di-μ(2)-bromido-μ(2)-hydroxido-di-μ(3)-iso-nicotinato-tetra-μ(2)-isonicotinato-tetra-copper(I)dithulium(III)].

Identifieur interne : 000602 ( PubMed/Corpus ); précédent : 000601; suivant : 000603

Poly[tetra-aqua-μ(4)-bromido-di-μ(2)-bromido-μ(2)-hydroxido-di-μ(3)-iso-nicotinato-tetra-μ(2)-isonicotinato-tetra-copper(I)dithulium(III)].

Auteurs : Guo-Ming Wang ; Zeng-Xin Li ; Qing-Hua Zheng ; Hui-Luan Liu

Source :

Acta crystallographica. Section E, Structure reports online [ 1600-5368 ] ; 2008.

RBID : pubmed:21201015

Abstract

A new thulium(III)-copper(I) heterometallic coordination polymer, [Cu(4)Tm(2)Br(3)(C(6)H(4)NO(2))(6)(OH)(H(2)O)(4)](n), has been prepared by a hydro-thermal method. The Tm and both Cu atoms lie on mirror planes. The Tm atom is seven-coordinate with a capped distorted trigonal-prismatic coordination geometry, while the Cu atoms adopt trigonal CuBrN(2) and tetra-hedral CuBr(3)N coordination modes, respectively. The Cu atom in the trigonal coordination environment is disordered over two sites of equal occupancy. The crystal structure is constructed from two distinct units of dimeric [Tm(2)(μ(2)-OH(IN)(6)(H(2)O)(4)] cores (IN = isonicotinate) and one-dimensional inorganic [Cu(4)Br(3)](n) chains, which are linked together, forming heterometallic Cu-halide-lanthanide-organic layers.

DOI: 10.1107/S1600536808028675
PubMed: 21201015

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pubmed:21201015

Le document en format XML

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<author><name sortKey="Wang, Guo Ming" sort="Wang, Guo Ming" uniqKey="Wang G" first="Guo-Ming" last="Wang">Guo-Ming Wang</name>
<affiliation><nlm:affiliation>Department of Chemistry, Teachers College of Qingdao University, Qingdao, Shandong 266071, People's Republic of China.</nlm:affiliation>
</affiliation>
</author>
<author><name sortKey="Li, Zeng Xin" sort="Li, Zeng Xin" uniqKey="Li Z" first="Zeng-Xin" last="Li">Zeng-Xin Li</name>
</author>
<author><name sortKey="Zheng, Qing Hua" sort="Zheng, Qing Hua" uniqKey="Zheng Q" first="Qing-Hua" last="Zheng">Qing-Hua Zheng</name>
</author>
<author><name sortKey="Liu, Hui Luan" sort="Liu, Hui Luan" uniqKey="Liu H" first="Hui-Luan" last="Liu">Hui-Luan Liu</name>
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<author><name sortKey="Wang, Guo Ming" sort="Wang, Guo Ming" uniqKey="Wang G" first="Guo-Ming" last="Wang">Guo-Ming Wang</name>
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<author><name sortKey="Li, Zeng Xin" sort="Li, Zeng Xin" uniqKey="Li Z" first="Zeng-Xin" last="Li">Zeng-Xin Li</name>
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<author><name sortKey="Zheng, Qing Hua" sort="Zheng, Qing Hua" uniqKey="Zheng Q" first="Qing-Hua" last="Zheng">Qing-Hua Zheng</name>
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<author><name sortKey="Liu, Hui Luan" sort="Liu, Hui Luan" uniqKey="Liu H" first="Hui-Luan" last="Liu">Hui-Luan Liu</name>
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<front><div type="abstract" xml:lang="en">A new thulium(III)-copper(I) heterometallic coordination polymer, [Cu(4)Tm(2)Br(3)(C(6)H(4)NO(2))(6)(OH)(H(2)O)(4)](n), has been prepared by a hydro-thermal method. The Tm and both Cu atoms lie on mirror planes. The Tm atom is seven-coordinate with a capped distorted trigonal-prismatic coordination geometry, while the Cu atoms adopt trigonal CuBrN(2) and tetra-hedral CuBr(3)N coordination modes, respectively. The Cu atom in the trigonal coordination environment is disordered over two sites of equal occupancy. The crystal structure is constructed from two distinct units of dimeric [Tm(2)(μ(2)-OH(IN)(6)(H(2)O)(4)] cores (IN = isonicotinate) and one-dimensional inorganic [Cu(4)Br(3)](n) chains, which are linked together, forming heterometallic Cu-halide-lanthanide-organic layers.</div>
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<Abstract><AbstractText>A new thulium(III)-copper(I) heterometallic coordination polymer, [Cu(4)Tm(2)Br(3)(C(6)H(4)NO(2))(6)(OH)(H(2)O)(4)](n), has been prepared by a hydro-thermal method. The Tm and both Cu atoms lie on mirror planes. The Tm atom is seven-coordinate with a capped distorted trigonal-prismatic coordination geometry, while the Cu atoms adopt trigonal CuBrN(2) and tetra-hedral CuBr(3)N coordination modes, respectively. The Cu atom in the trigonal coordination environment is disordered over two sites of equal occupancy. The crystal structure is constructed from two distinct units of dimeric [Tm(2)(μ(2)-OH(IN)(6)(H(2)O)(4)] cores (IN = isonicotinate) and one-dimensional inorganic [Cu(4)Br(3)](n) chains, which are linked together, forming heterometallic Cu-halide-lanthanide-organic layers.</AbstractText>
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<CommentsCorrections RefType="Cites"><RefSource>Chem Rev. 2002 Jun;102(6):2187-210</RefSource>
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</CommentsCorrections>
<CommentsCorrections RefType="Cites"><RefSource>Chem Rev. 2002 Jun;102(6):2369-88</RefSource>
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<CommentsCorrections RefType="Cites"><RefSource>Angew Chem Int Ed Engl. 2007;46(16):2851-4</RefSource>
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</CommentsCorrections>
<CommentsCorrections RefType="Cites"><RefSource>J Am Chem Soc. 2004 Mar 17;126(10):3012-3</RefSource>
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<CommentsCorrections RefType="Cites"><RefSource>J Am Chem Soc. 2004 Dec 1;126(47):15394-5</RefSource>
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<CommentsCorrections RefType="Cites"><RefSource>Angew Chem Int Ed Engl. 2006 May 12;45(20):3287-91</RefSource>
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</CommentsCorrections>
<CommentsCorrections RefType="Cites"><RefSource>Inorg Chem. 2006 Oct 16;45(21):8468-70</RefSource>
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<CommentsCorrections RefType="Cites"><RefSource>Angew Chem Int Ed Engl. 2003 Feb 3;42(5):532-5</RefSource>
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Poly[tetra-aqua-μ(4)-bromido-di-μ(2)-bromido-μ(2)-hydroxido-di-μ(3)-iso-nicotinato-tetra-μ(2)-isonicotinato-tetra-copper(I)dithulium(III)].

Poly[tetra-aqua-μ(4)-bromido-di-μ(2)-bromido-μ(2)-hydroxido-di-μ(3)-iso-nicotinato-tetra-μ(2)-isonicotinato-tetra-copper(I)dithulium(III)].

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Abstract

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