Bis[μ-2-(4-hydroxyphenyl)acetato]-κ3O,O′:O;κ3O:O,O′-bis{aqua(4,4′-bipyridine-κN)[2-(4-hydroxyphenyl)acetato-κ2O,O′]erbium(III)} monohydrate
Identifieur interne : 000350 ( Pmc/Curation ); précédent : 000349; suivant : 000351Bis[μ-2-(4-hydroxyphenyl)acetato]-κ3O,O′:O;κ3O:O,O′-bis{aqua(4,4′-bipyridine-κN)[2-(4-hydroxyphenyl)acetato-κ2O,O′]erbium(III)} monohydrate
Auteurs : Jia-Lu Liu [République populaire de Chine] ; Jian-Feng Liu [République populaire de Chine] ; Guo-Liang Zhao [République populaire de Chine]Source :
- Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2010.
Abstract
The title dinuclear complex, [Er2(C8H7O3)6(C10H8N2)2(H2O)2]·H2O, contains two ErIII atoms in the asymmetric unit, six 2-(4-hydroxyphenyl)acetate (PAA) anions, two 4,4′-bipyridine (bipy) molecules, two coordinated water molecules and one solvent water molecule. The central ErIII atoms are nine-coordinated. The coordination environment includes six O atoms from three PAA anions, one bridging O atom from a PAA anion, one O atom from a water molecule and an N atom from a bipy ligand in a distorted tricapped trigonal–prismatic geometry. The occurrence of numerous O—H⋯O and O—H⋯N hydrogen bonds involving coordinated and noncoordinated water as well as bipy groups builds up an intricate three-dimensional network.
Url:
DOI: 10.1107/S1600536810044752
PubMed: 21589217
PubMed Central: 3011679
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PMC:3011679Le document en format XML
<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Bis[μ-2-(4-hydroxyphenyl)acetato]-κ<sup>3</sup>
<italic>O</italic>
,<italic>O</italic>
′:<italic>O</italic>
;κ<sup>3</sup>
<italic>O</italic>
:<italic>O</italic>
,<italic>O</italic>
′-bis{aqua(4,4′-bipyridine-κ<italic>N</italic>
)[2-(4-hydroxyphenyl)acetato-κ<sup>2</sup>
<italic>O</italic>
,<italic>O</italic>
′]erbium(III)} monohydrate</title>
<author><name sortKey="Liu, Jia Lu" sort="Liu, Jia Lu" uniqKey="Liu J" first="Jia-Lu" last="Liu">Jia-Lu Liu</name>
<affiliation wicri:level="1"><nlm:aff id="a">College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Liu, Jian Feng" sort="Liu, Jian Feng" uniqKey="Liu J" first="Jian-Feng" last="Liu">Jian-Feng Liu</name>
<affiliation wicri:level="1"><nlm:aff id="a">College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Zhao, Guo Liang" sort="Zhao, Guo Liang" uniqKey="Zhao G" first="Guo-Liang" last="Zhao">Guo-Liang Zhao</name>
<affiliation wicri:level="1"><nlm:aff id="a">College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Bis[μ-2-(4-hydroxyphenyl)acetato]-κ<sup>3</sup>
<italic>O</italic>
,<italic>O</italic>
′:<italic>O</italic>
;κ<sup>3</sup>
<italic>O</italic>
:<italic>O</italic>
,<italic>O</italic>
′-bis{aqua(4,4′-bipyridine-κ<italic>N</italic>
)[2-(4-hydroxyphenyl)acetato-κ<sup>2</sup>
<italic>O</italic>
,<italic>O</italic>
′]erbium(III)} monohydrate</title>
<author><name sortKey="Liu, Jia Lu" sort="Liu, Jia Lu" uniqKey="Liu J" first="Jia-Lu" last="Liu">Jia-Lu Liu</name>
<affiliation wicri:level="1"><nlm:aff id="a">College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Liu, Jian Feng" sort="Liu, Jian Feng" uniqKey="Liu J" first="Jian-Feng" last="Liu">Jian-Feng Liu</name>
<affiliation wicri:level="1"><nlm:aff id="a">College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Zhao, Guo Liang" sort="Zhao, Guo Liang" uniqKey="Zhao G" first="Guo-Liang" last="Zhao">Guo-Liang Zhao</name>
<affiliation wicri:level="1"><nlm:aff id="a">College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
</analytic>
<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2010">2010</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
</fileDesc>
<profileDesc><textClass></textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en"><p>The title dinuclear complex, [Er<sub>2</sub>
(C<sub>8</sub>
H<sub>7</sub>
O<sub>3</sub>
)<sub>6</sub>
(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
]·H<sub>2</sub>
O, contains two Er<sup>III</sup>
atoms in the asymmetric unit, six 2-(4-hydroxyphenyl)acetate (PAA) anions, two 4,4′-bipyridine (bipy) molecules, two coordinated water molecules and one solvent water molecule. The central Er<sup>III</sup>
atoms are nine-coordinated. The coordination environment includes six O atoms from three PAA anions, one bridging O atom from a PAA anion, one O atom from a water molecule and an N atom from a bipy ligand in a distorted tricapped trigonal–prismatic geometry. The occurrence of numerous O—H⋯O and O—H⋯N hydrogen bonds involving coordinated and noncoordinated water as well as bipy groups builds up an intricate three-dimensional network.</p>
</div>
</front>
<back><div1 type="bibliography"><listBibl><biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
</listBibl>
</div1>
</back>
</TEI>
<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
<front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Structure Reports Online</journal-title>
</journal-title-group>
<issn pub-type="epub">1600-5368</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">21589217</article-id>
<article-id pub-id-type="pmc">3011679</article-id>
<article-id pub-id-type="publisher-id">om2372</article-id>
<article-id pub-id-type="doi">10.1107/S1600536810044752</article-id>
<article-id pub-id-type="coden">ACSEBH</article-id>
<article-id pub-id-type="pii">S1600536810044752</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Metal-Organic Papers</subject>
</subj-group>
</article-categories>
<title-group><article-title>Bis[μ-2-(4-hydroxyphenyl)acetato]-κ<sup>3</sup>
<italic>O</italic>
,<italic>O</italic>
′:<italic>O</italic>
;κ<sup>3</sup>
<italic>O</italic>
:<italic>O</italic>
,<italic>O</italic>
′-bis{aqua(4,4′-bipyridine-κ<italic>N</italic>
)[2-(4-hydroxyphenyl)acetato-κ<sup>2</sup>
<italic>O</italic>
,<italic>O</italic>
′]erbium(III)} monohydrate</article-title>
<alt-title><italic>[Er<sub>2</sub>
(C<sub>8</sub>
H<sub>7</sub>
O<sub>3</sub>
)<sub>6</sub>
(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
]·H<sub>2</sub>
O</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Liu</surname>
<given-names>Jia-Lu</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Liu</surname>
<given-names>Jian-Feng</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Zhao</surname>
<given-names>Guo-Liang</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<aff id="a"><label>a</label>
College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>sky53@zjnu.cn</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>12</month>
<year>2010</year>
</pub-date>
<pub-date pub-type="epub"><day>06</day>
<month>11</month>
<year>2010</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>06</day>
<month>11</month>
<year>2010</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the
. </pmc-comment>
<volume>66</volume>
<issue>Pt 12</issue>
<issue-id pub-id-type="publisher-id">e101200</issue-id>
<fpage>m1513</fpage>
<lpage>m1513</lpage>
<history><date date-type="received"><day>17</day>
<month>10</month>
<year>2010</year>
</date>
<date date-type="accepted"><day>02</day>
<month>11</month>
<year>2010</year>
</date>
</history>
<permissions><copyright-statement>© Liu et al. 2010</copyright-statement>
<copyright-year>2010</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S1600536810044752">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract><p>The title dinuclear complex, [Er<sub>2</sub>
(C<sub>8</sub>
H<sub>7</sub>
O<sub>3</sub>
)<sub>6</sub>
(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
]·H<sub>2</sub>
O, contains two Er<sup>III</sup>
atoms in the asymmetric unit, six 2-(4-hydroxyphenyl)acetate (PAA) anions, two 4,4′-bipyridine (bipy) molecules, two coordinated water molecules and one solvent water molecule. The central Er<sup>III</sup>
atoms are nine-coordinated. The coordination environment includes six O atoms from three PAA anions, one bridging O atom from a PAA anion, one O atom from a water molecule and an N atom from a bipy ligand in a distorted tricapped trigonal–prismatic geometry. The occurrence of numerous O—H⋯O and O—H⋯N hydrogen bonds involving coordinated and noncoordinated water as well as bipy groups builds up an intricate three-dimensional network.</p>
</abstract>
</article-meta>
</front>
<floats-group><table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Hydrogen-bond geometry (Å, °)</title>
</caption>
<table frame="hsides" rules="groups"><thead valign="bottom"><tr><th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom">H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
</tr>
</thead>
<tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O3—H3<italic>B</italic>
⋯O12<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.82</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.742 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">169</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O6—H6<italic>B</italic>
⋯O3<italic>W</italic>
<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.82</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.86</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.650 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">160</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O9—H9<italic>A</italic>
⋯O17<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.82</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.86</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.674 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">173</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O12—H12⋯O11<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.82</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.94</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.751 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">168</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O15—H15<italic>C</italic>
⋯O6<sup>v</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.82</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.90</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.716 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">174</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O18—H18<italic>B</italic>
⋯O9<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.82</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.95</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.768 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">174</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O2<italic>W</italic>
—H2<italic>WA</italic>
⋯O5</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.83 (4)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.97 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.732 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">151 (3)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O2<italic>W</italic>
—H2<italic>WB</italic>
⋯N2<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.81 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.06 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.839 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">162 (4)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O3<italic>W</italic>
—H3<italic>WB</italic>
⋯O3</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.82 (4)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.99 (4)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.793 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">167 (4)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H1<italic>WA</italic>
⋯O13</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.83 (4)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.96 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.7333 (19)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">156 (3)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H1<italic>WB</italic>
⋯N4<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.83 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.96 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.781 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">171 (3)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O3<italic>W</italic>
—H3<italic>WA</italic>
⋯O1<sup>vi</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.84 (4)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.94 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.778 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">176 (4)</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry codes: (i) <inline-formula><inline-graphic xlink:href="e-66-m1513-efi2.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (ii) <inline-formula><inline-graphic xlink:href="e-66-m1513-efi3.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iii) <inline-formula><inline-graphic xlink:href="e-66-m1513-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iv) <inline-formula><inline-graphic xlink:href="e-66-m1513-efi5.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (v) <inline-formula><inline-graphic xlink:href="e-66-m1513-efi6.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (vi) <inline-formula><inline-graphic xlink:href="e-66-m1513-efi7.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
</record>
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{{Explor lien |wiki= Wicri/Terre |area= ThuliumV1 |flux= Pmc |étape= Curation |type= RBID |clé= PMC:3011679 |texte= Bis[μ-2-(4-hydroxyphenyl)acetato]-κ3O,O′:O;κ3O:O,O′-bis{aqua(4,4′-bipyridine-κN)[2-(4-hydroxyphenyl)acetato-κ2O,O′]erbium(III)} monohydrate }}
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