An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil
Identifieur interne : 001488 ( Main/Exploration ); précédent : 001487; suivant : 001489An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil
Auteurs : Christopher V. Grant [États-Unis] ; Siu-Ling Sit [États-Unis] ; Anna A. De Angelis [États-Unis] ; Kelli S. Khuong [États-Unis] ; Chin H. Wu [États-Unis] ; Leigh A. Plesniak [États-Unis] ; Stanley J. Opella [États-Unis]Source :
- Journal of magnetic resonance (San Diego, Calif. : 1997) [ 1090-7807 ] ; 2007.
Abstract
The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of 1H and 31P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.
Url:
DOI: 10.1016/j.jmr.2007.06.016
PubMed: 17719813
PubMed Central: 2097957
Affiliations:
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Le document en format XML
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">An efficient <sup>1</sup>
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P double-resonance solid-state NMR probe that utilizes a scroll coil</title>
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<front><div type="abstract" xml:lang="en"><p id="P2">The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of <sup>1</sup>
H and <sup>31</sup>
P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.</p>
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<tree><country name="États-Unis"><region name="Californie"><name sortKey="Grant, Christopher V" sort="Grant, Christopher V" uniqKey="Grant C" first="Christopher V." last="Grant">Christopher V. Grant</name>
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<name sortKey="De Angelis, Anna A" sort="De Angelis, Anna A" uniqKey="De Angelis A" first="Anna A." last="De Angelis">Anna A. De Angelis</name>
<name sortKey="Khuong, Kelli S" sort="Khuong, Kelli S" uniqKey="Khuong K" first="Kelli S." last="Khuong">Kelli S. Khuong</name>
<name sortKey="Opella, Stanley J" sort="Opella, Stanley J" uniqKey="Opella S" first="Stanley J." last="Opella">Stanley J. Opella</name>
<name sortKey="Plesniak, Leigh A" sort="Plesniak, Leigh A" uniqKey="Plesniak L" first="Leigh A." last="Plesniak">Leigh A. Plesniak</name>
<name sortKey="Sit, Siu Ling" sort="Sit, Siu Ling" uniqKey="Sit S" first="Siu-Ling" last="Sit">Siu-Ling Sit</name>
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