An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil
Identifieur interne : 001488 ( Main/Exploration ); précédent : 001487; suivant : 001489An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil
Auteurs : Christopher V. Grant [États-Unis] ; Siu-Ling Sit [États-Unis] ; Anna A. De Angelis [États-Unis] ; Kelli S. Khuong [États-Unis] ; Chin H. Wu [États-Unis] ; Leigh A. Plesniak [États-Unis] ; Stanley J. Opella [États-Unis]Source :
- Journal of magnetic resonance (San Diego, Calif. : 1997) [ 1090-7807 ] ; 2007.
Abstract
The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of 1H and 31P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.
Url:
DOI: 10.1016/j.jmr.2007.06.016
PubMed: 17719813
PubMed Central: 2097957
Affiliations:
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Grant</name><affiliation wicri:level="2"><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff><country xml:lang="fr">États-Unis</country><placeName><region type="state">Californie</region></placeName><wicri:cityArea> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla</wicri:cityArea></affiliation></author><author><name sortKey="Sit, Siu Ling" sort="Sit, Siu Ling" uniqKey="Sit S" first="Siu-Ling" last="Sit">Siu-Ling Sit</name><affiliation wicri:level="2"><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff><country xml:lang="fr">États-Unis</country><placeName><region type="state">Californie</region></placeName><wicri:cityArea> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla</wicri:cityArea></affiliation></author><author><name sortKey="De Angelis, Anna A" sort="De Angelis, Anna A" uniqKey="De Angelis A" first="Anna A." last="De Angelis">Anna A. De Angelis</name><affiliation wicri:level="2"><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff><country xml:lang="fr">États-Unis</country><placeName><region type="state">Californie</region></placeName><wicri:cityArea> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla</wicri:cityArea></affiliation></author><author><name sortKey="Khuong, Kelli S" sort="Khuong, Kelli S" uniqKey="Khuong K" first="Kelli S." last="Khuong">Kelli S. 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Wu</name><affiliation wicri:level="2"><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff><country xml:lang="fr">États-Unis</country><placeName><region type="state">Californie</region></placeName><wicri:cityArea> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla</wicri:cityArea></affiliation></author><author><name sortKey="Plesniak, Leigh A" sort="Plesniak, Leigh A" uniqKey="Plesniak L" first="Leigh A." last="Plesniak">Leigh A. Plesniak</name><affiliation wicri:level="2"><nlm:aff id="A2"> Department of Chemistry and Biochemistry, University of San Diego, 5998 Alcala Park, San Diego, CA 92110</nlm:aff><country xml:lang="fr">États-Unis</country><placeName><region type="state">Californie</region></placeName><wicri:cityArea> Department of Chemistry and Biochemistry, University of San Diego, 5998 Alcala Park, San Diego</wicri:cityArea></affiliation></author><author><name sortKey="Opella, Stanley J" sort="Opella, Stanley J" uniqKey="Opella S" first="Stanley J." last="Opella">Stanley J. Opella</name><affiliation wicri:level="2"><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff><country xml:lang="fr">États-Unis</country><placeName><region type="state">Californie</region></placeName><wicri:cityArea> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla</wicri:cityArea></affiliation></author></analytic><series><title level="j">Journal of magnetic resonance (San Diego, Calif. : 1997)</title><idno type="ISSN">1090-7807</idno><idno type="eISSN">1096-0856</idno><imprint><date when="2007">2007</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p id="P2">The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of <sup>1</sup>H and <sup>31</sup>P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.</p></div></front></TEI><affiliations><list><country><li>États-Unis</li></country><region><li>Californie</li></region></list><tree><country name="États-Unis"><region name="Californie"><name sortKey="Grant, Christopher V" sort="Grant, Christopher V" uniqKey="Grant C" first="Christopher V." last="Grant">Christopher V. Grant</name></region><name sortKey="De Angelis, Anna A" sort="De Angelis, Anna A" uniqKey="De Angelis A" first="Anna A." last="De Angelis">Anna A. De Angelis</name><name sortKey="Khuong, Kelli S" sort="Khuong, Kelli S" uniqKey="Khuong K" first="Kelli S." last="Khuong">Kelli S. Khuong</name><name sortKey="Opella, Stanley J" sort="Opella, Stanley J" uniqKey="Opella S" first="Stanley J." last="Opella">Stanley J. Opella</name><name sortKey="Plesniak, Leigh A" sort="Plesniak, Leigh A" uniqKey="Plesniak L" first="Leigh A." last="Plesniak">Leigh A. Plesniak</name><name sortKey="Sit, Siu Ling" sort="Sit, Siu Ling" uniqKey="Sit S" first="Siu-Ling" last="Sit">Siu-Ling Sit</name><name sortKey="Wu, Chin H" sort="Wu, Chin H" uniqKey="Wu C" first="Chin H." last="Wu">Chin H. Wu</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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