ThuliumV1, Pmc, Corpus, bibRecord, 000239

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

Identifieur interne : 000239 ( Pmc/Corpus ); précédent : 000238; suivant : 000240

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

Auteurs : Christopher V. Grant ; Siu-Ling Sit ; Anna A. De Angelis ; Kelli S. Khuong ; Chin H. Wu ; Leigh A. Plesniak ; Stanley J. Opella

Source :

Journal of magnetic resonance (San Diego, Calif. : 1997) [ 1090-7807 ] ; 2007.

RBID : PMC:2097957

Abstract

The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of ¹H and ³¹P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC2097957

DOI: 10.1016/j.jmr.2007.06.016
PubMed: 17719813
PubMed Central: 2097957

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PMC:2097957

Le document en format XML

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H/<sup>31</sup>
P double-resonance solid-state NMR probe that utilizes a scroll coil</title>
<author><name sortKey="Grant, Christopher V" sort="Grant, Christopher V" uniqKey="Grant C" first="Christopher V." last="Grant">Christopher V. Grant</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Sit, Siu Ling" sort="Sit, Siu Ling" uniqKey="Sit S" first="Siu-Ling" last="Sit">Siu-Ling Sit</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
<author><name sortKey="De Angelis, Anna A" sort="De Angelis, Anna A" uniqKey="De Angelis A" first="Anna A." last="De Angelis">Anna A. De Angelis</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Khuong, Kelli S" sort="Khuong, Kelli S" uniqKey="Khuong K" first="Kelli S." last="Khuong">Kelli S. Khuong</name>
<affiliation><nlm:aff id="A2"> Department of Chemistry and Biochemistry, University of San Diego, 5998 Alcala Park, San Diego, CA 92110</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Wu, Chin H" sort="Wu, Chin H" uniqKey="Wu C" first="Chin H." last="Wu">Chin H. Wu</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Plesniak, Leigh A" sort="Plesniak, Leigh A" uniqKey="Plesniak L" first="Leigh A." last="Plesniak">Leigh A. Plesniak</name>
<affiliation><nlm:aff id="A2"> Department of Chemistry and Biochemistry, University of San Diego, 5998 Alcala Park, San Diego, CA 92110</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Opella, Stanley J" sort="Opella, Stanley J" uniqKey="Opella S" first="Stanley J." last="Opella">Stanley J. Opella</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
</titleStmt>
<publicationStmt><idno type="wicri:source">PMC</idno>
<idno type="pmid">17719813</idno>
<idno type="pmc">2097957</idno>
<idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC2097957</idno>
<idno type="RBID">PMC:2097957</idno>
<idno type="doi">10.1016/j.jmr.2007.06.016</idno>
<date when="2007">2007</date>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">An efficient <sup>1</sup>
H/<sup>31</sup>
P double-resonance solid-state NMR probe that utilizes a scroll coil</title>
<author><name sortKey="Grant, Christopher V" sort="Grant, Christopher V" uniqKey="Grant C" first="Christopher V." last="Grant">Christopher V. Grant</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Sit, Siu Ling" sort="Sit, Siu Ling" uniqKey="Sit S" first="Siu-Ling" last="Sit">Siu-Ling Sit</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
<author><name sortKey="De Angelis, Anna A" sort="De Angelis, Anna A" uniqKey="De Angelis A" first="Anna A." last="De Angelis">Anna A. De Angelis</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Khuong, Kelli S" sort="Khuong, Kelli S" uniqKey="Khuong K" first="Kelli S." last="Khuong">Kelli S. Khuong</name>
<affiliation><nlm:aff id="A2"> Department of Chemistry and Biochemistry, University of San Diego, 5998 Alcala Park, San Diego, CA 92110</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Wu, Chin H" sort="Wu, Chin H" uniqKey="Wu C" first="Chin H." last="Wu">Chin H. Wu</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Plesniak, Leigh A" sort="Plesniak, Leigh A" uniqKey="Plesniak L" first="Leigh A." last="Plesniak">Leigh A. Plesniak</name>
<affiliation><nlm:aff id="A2"> Department of Chemistry and Biochemistry, University of San Diego, 5998 Alcala Park, San Diego, CA 92110</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Opella, Stanley J" sort="Opella, Stanley J" uniqKey="Opella S" first="Stanley J." last="Opella">Stanley J. Opella</name>
<affiliation><nlm:aff id="A1"> Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</nlm:aff>
</affiliation>
</author>
</analytic>
<series><title level="j">Journal of magnetic resonance (San Diego, Calif. : 1997)</title>
<idno type="ISSN">1090-7807</idno>
<idno type="eISSN">1096-0856</idno>
<imprint><date when="2007">2007</date>
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<front><div type="abstract" xml:lang="en"><p id="P2">The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of <sup>1</sup>
H and <sup>31</sup>
P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.</p>
</div>
</front>
</TEI>
<pmc article-type="research-article" xml:lang="EN"><pmc-comment>The publisher of this article does not allow downloading of the full text in XML form.</pmc-comment>
  <pmc-dir>properties manuscript</pmc-dir>
  <front><journal-meta><journal-id journal-id-type="nlm-journal-id">9707935</journal-id>
<journal-id journal-id-type="pubmed-jr-id">20597</journal-id>
<journal-id journal-id-type="nlm-ta">J Magn Reson</journal-id>
<journal-title>Journal of magnetic resonance (San Diego, Calif. : 1997)</journal-title>
<issn pub-type="ppub">1090-7807</issn>
<issn pub-type="epub">1096-0856</issn>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">17719813</article-id>
<article-id pub-id-type="pmc">2097957</article-id>
<article-id pub-id-type="doi">10.1016/j.jmr.2007.06.016</article-id>
<article-id pub-id-type="manuscript">NIHMS33306</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Article</subject>
</subj-group>
</article-categories>
<title-group><article-title>An efficient <sup>1</sup>
H/<sup>31</sup>
P double-resonance solid-state NMR probe that utilizes a scroll coil</article-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Grant</surname>
<given-names>Christopher V.</given-names>
</name>
<xref rid="A1" ref-type="aff">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Sit</surname>
<given-names>Siu-Ling</given-names>
</name>
<xref rid="A1" ref-type="aff">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>De Angelis</surname>
<given-names>Anna A.</given-names>
</name>
<xref rid="A1" ref-type="aff">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Khuong</surname>
<given-names>Kelli S.</given-names>
</name>
<xref rid="A2" ref-type="aff">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Wu</surname>
<given-names>Chin H.</given-names>
</name>
<xref rid="A1" ref-type="aff">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Plesniak</surname>
<given-names>Leigh A.</given-names>
</name>
<xref rid="A2" ref-type="aff">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Opella</surname>
<given-names>Stanley J.</given-names>
</name>
<xref rid="A1" ref-type="aff">a</xref>
<xref rid="FN1" ref-type="author-notes">*</xref>
</contrib>
</contrib-group>
<aff id="A1"><label>a</label>
 Department of Chemistry and Biochemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093-0307</aff>
<aff id="A2"><label>b</label>
 Department of Chemistry and Biochemistry, University of San Diego, 5998 Alcala Park, San Diego, CA 92110</aff>
<author-notes><corresp id="FN1">* Corresponding Author. <email>sopella@ucsd.edu</email>
, 858.822.4820</corresp>
</author-notes>
<pub-date pub-type="nihms-submitted"><day>7</day>
<month>11</month>
<year>2007</year>
</pub-date>
<pub-date pub-type="epub"><day>6</day>
<month>8</month>
<year>2007</year>
</pub-date>
<pub-date pub-type="ppub"><month>10</month>
<year>2007</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>1</day>
<month>10</month>
<year>2008</year>
</pub-date>
<volume>188</volume>
<issue>2</issue>
<fpage>279</fpage>
<lpage>284</lpage>
<abstract><p id="P2">The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of <sup>1</sup>
H and <sup>31</sup>
P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.</p>
</abstract>
<contract-num rid="GM1">R15 GM068431-02A1
				||GM</contract-num>
<contract-num rid="GM1">R01 GM075877-03
				||GM</contract-num>
<contract-num rid="EB1">R01 EB001966-30
				||EB</contract-num>
<contract-num rid="EB1">P41 EB002031-14
				||EB</contract-num>
<contract-num rid="GM1">F32 GM065833-03
				||GM</contract-num>
<contract-sponsor id="GM1">National Institute of General Medical Sciences : NIGMS</contract-sponsor>
<contract-sponsor id="EB1">National Institute of Biomedical Imaging and Bioengineering : NIBIB</contract-sponsor>
</article-meta>
</front>
</pmc>
</record>

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An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

An efficient 1H/31P double-resonance solid-state NMR probe that utilizes a scroll coil

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Abstract

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