ThuliumV1, Main, Curation, bibRecord, 000C53

Bis[μ-2-(4-hydroxyphenyl)acetato]-κ3O,O′:O;κ3O:O,O′-bis{aqua(4,4′-bipyridine-κN)[2-(4-hydroxyphenyl)acetato-κ2O,O′]erbium(III)} monohydrate

Identifieur interne : 000C53 ( Main/Curation ); précédent : 000C52; suivant : 000C54

Bis[μ-2-(4-hydroxyphenyl)acetato]-κ3O,O′:O;κ3O:O,O′-bis{aqua(4,4′-bipyridine-κN)[2-(4-hydroxyphenyl)acetato-κ2O,O′]erbium(III)} monohydrate

Auteurs : Jia-Lu Liu [République populaire de Chine] ; Jian-Feng Liu [République populaire de Chine] ; Guo-Liang Zhao [République populaire de Chine]

Source :

Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2010.

RBID : PMC:3011679

Abstract

The title dinuclear complex, [Er₂(C₈H₇O₃)₆(C₁₀H₈N₂)₂(H₂O)₂]·H₂O, contains two Er^III atoms in the asymmetric unit, six 2-(4-hydroxyphenyl)acetate (PAA) anions, two 4,4′-bipyridine (bipy) molecules, two coordinated water molecules and one solvent water molecule. The central Er^III atoms are nine-coordinated. The coordination environment includes six O atoms from three PAA anions, one bridging O atom from a PAA anion, one O atom from a water molecule and an N atom from a bipy ligand in a distorted tricapped trigonal–prismatic geometry. The occurrence of numerous O—H⋯O and O—H⋯N hydrogen bonds involving coordinated and noncoordinated water as well as bipy groups builds up an intricate three-dimensional network.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011679

DOI: 10.1107/S1600536810044752
PubMed: 21589217
PubMed Central: 3011679

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PMC:3011679

Le document en format XML

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<italic>O</italic>
,<italic>O</italic>
′:<italic>O</italic>
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:<italic>O</italic>
,<italic>O</italic>
′-bis{aqua(4,4′-bipyridine-κ<italic>N</italic>
)[2-(4-hydroxyphenyl)acetato-κ<sup>2</sup>
<italic>O</italic>
,<italic>O</italic>
′]erbium(III)} monohydrate</title>
<author><name sortKey="Liu, Jia Lu" sort="Liu, Jia Lu" uniqKey="Liu J" first="Jia-Lu" last="Liu">Jia-Lu Liu</name>
<affiliation wicri:level="1"><nlm:aff id="a">College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
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<country xml:lang="fr">République populaire de Chine</country>
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<author><name sortKey="Liu, Jian Feng" sort="Liu, Jian Feng" uniqKey="Liu J" first="Jian-Feng" last="Liu">Jian-Feng Liu</name>
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<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Zhao, Guo Liang" sort="Zhao, Guo Liang" uniqKey="Zhao G" first="Guo-Liang" last="Zhao">Guo-Liang Zhao</name>
<affiliation wicri:level="1"><nlm:aff id="a">College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People’s Republic of China, and Zhejiang Normal University Xingzhi College, Jinhua 321004,<country>People’s Republic of China</country>
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,<italic>O</italic>
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<front><div type="abstract" xml:lang="en"><p>The title dinuclear complex, [Er<sub>2</sub>
(C<sub>8</sub>
H<sub>7</sub>
O<sub>3</sub>
)<sub>6</sub>
(C<sub>10</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
]·H<sub>2</sub>
O, contains two Er<sup>III</sup>
 atoms in the asymmetric unit, six 2-(4-hydroxyphenyl)acetate (PAA) anions, two 4,4′-bipyridine (bipy) molecules, two coordinated water molecules and one solvent water molecule. The central Er<sup>III</sup>
 atoms are nine-coordinated. The coordination environment includes six O atoms from three PAA anions, one bridging O atom from a PAA anion, one O atom from a water molecule and an N atom from a bipy ligand in a distorted tricapped trigonal–prismatic geometry. The occurrence of numerous O—H⋯O and O—H⋯N hydrogen bonds involving coordinated and noncoordinated water as well as bipy groups builds up an intricate three-dimensional network.</p>
</div>
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Bis[μ-2-(4-hy­droxy­phen­yl)acetato]-κ3O,O′:O;κ3O:O,O′-bis­{aqua­(4,4′-bi­pyridine-κN)[2-(4-hy­droxy­phen­yl)acetato-κ2O,O′]erbium(III)} monohydrate

Bis[μ-2-(4-hy­droxy­phen­yl)acetato]-κ3O,O′:O;κ3O:O,O′-bis­{aqua­(4,4′-bi­pyridine-κN)[2-(4-hy­droxy­phen­yl)acetato-κ2O,O′]erbium(III)} monohydrate

Source :

Abstract

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Bis[μ-2-(4-hydroxyphenyl)acetato]-κ3O,O′:O;κ3O:O,O′-bis{aqua(4,4′-bipyridine-κN)[2-(4-hydroxyphenyl)acetato-κ2O,O′]erbium(III)} monohydrate

Bis[μ-2-(4-hydroxyphenyl)acetato]-κ3O,O′:O;κ3O:O,O′-bis{aqua(4,4′-bipyridine-κN)[2-(4-hydroxyphenyl)acetato-κ2O,O′]erbium(III)} monohydrate