Hydrogenated Nitrile Butadiene Rubber and Hindered Phenol Composite. II. Characterization of Hydrogen Bonding
Identifieur interne : 000A65 ( Main/Exploration ); précédent : 000A64; suivant : 000A66Hydrogenated Nitrile Butadiene Rubber and Hindered Phenol Composite. II. Characterization of Hydrogen Bonding
Auteurs : Y. Y. Cao [République populaire de Chine] ; H. Y. Mou [République populaire de Chine] ; F. Shen [États-Unis] ; H. Y. Xu [République populaire de Chine] ; Guo-Hua Hu [France] ; C. F. Wu [République populaire de Chine]Source :
- Polymer Engineering and Science [ 0032-3888 ] ; 2011.
Abstract
This article reports on the relationship between the variation of hydrogen bonding and macroscopic properties of composites composed of hydrogenated nitrile butadiene rubber (HNBR) and 3,9-bis {1,1-dimethyl-2 [β-(3-tert-butyl-4-hydroxy-5-methylphenyl) propionyloxy] ethyl}-2,4,8,10-tetraoxaspiro [5,5]-undecane (AO-80). Hydrogen bonding of the composites was studied by Fourier-transform infrared (FT-IR) and ultraviolet (UV) spectroscopies. FT-IR spectra at room temperature revealed that the stretching vibration peak of OH and CO of AO-80 red shifted with increasing AO-80 content, whereas that of C≡N of HNBR blue shifted only when the AO-80 content exceeded 10 parts per 100 resin (phr). At elevated temperatures, the shift was the opposite for CO and C≡N bands resulting from hydrogen bonding dissociation. In the UV spectra, the E2 band of benzene ring of AO-80 exhibited two peaks differing in shape.
Url:
DOI: 10.1002/pen.21795
Affiliations:
- France, République populaire de Chine, États-Unis
- Grand Est, Lorraine (région)
- Metz, Nancy
- Centre national de la recherche scientifique, Laboratoire réactions et génie des procédés, Université de Lorraine
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F." last="Wu">C. F. Wu</name><affiliation wicri:level="1"><hal:affiliation type="laboratory" xml:id="struct-161125" status="INCOMING"><orgName>Polymer Alloy Lab, School of Materials Science and Engineering</orgName><desc><address><addrLine>Meilong Road, Shanghai, 200237</addrLine><country key="CN"></country></address></desc><listRelation><relation active="#struct-312539" type="direct"></relation></listRelation><tutelles><tutelle active="#struct-312539" type="direct"><org type="institution" xml:id="struct-312539" status="INCOMING"><orgName>East China University of Science and Technology</orgName><desc><address><country key="FR"></country></address></desc></org></tutelle></tutelles></hal:affiliation><country>République populaire de Chine</country></affiliation></author></analytic><idno type="DOI">10.1002/pen.21795</idno><series><title level="j">Polymer Engineering and Science</title><idno type="ISSN">0032-3888</idno><imprint><date type="datePub">2011</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">This article reports on the relationship between the variation of hydrogen bonding and macroscopic properties of composites composed of hydrogenated nitrile butadiene rubber (HNBR) and 3,9-bis {1,1-dimethyl-2 [β-(3-tert-butyl-4-hydroxy-5-methylphenyl) propionyloxy] ethyl}-2,4,8,10-tetraoxaspiro [5,5]-undecane (AO-80). Hydrogen bonding of the composites was studied by Fourier-transform infrared (FT-IR) and ultraviolet (UV) spectroscopies. FT-IR spectra at room temperature revealed that the stretching vibration peak of OH and CO of AO-80 red shifted with increasing AO-80 content, whereas that of C≡N of HNBR blue shifted only when the AO-80 content exceeded 10 parts per 100 resin (phr). At elevated temperatures, the shift was the opposite for CO and C≡N bands resulting from hydrogen bonding dissociation. In the UV spectra, the E2 band of benzene ring of AO-80 exhibited two peaks differing in shape.</div></front></TEI><affiliations><list><country><li>France</li><li>République populaire de Chine</li><li>États-Unis</li></country><region><li>Grand Est</li><li>Lorraine (région)</li></region><settlement><li>Metz</li><li>Nancy</li></settlement><orgName><li>Centre national de la recherche scientifique</li><li>Laboratoire réactions et génie des procédés</li><li>Université de Lorraine</li></orgName></list><tree><country name="République populaire de Chine"><noRegion><name sortKey="Cao, Y Y" sort="Cao, Y Y" uniqKey="Cao Y" first="Y. Y." last="Cao">Y. Y. Cao</name></noRegion><name sortKey="Mou, H Y" sort="Mou, H Y" uniqKey="Mou H" first="H. Y." last="Mou">H. Y. Mou</name><name sortKey="Wu, C F" sort="Wu, C F" uniqKey="Wu C" first="C. F." last="Wu">C. F. Wu</name><name sortKey="Xu, H Y" sort="Xu, H Y" uniqKey="Xu H" first="H. Y." last="Xu">H. Y. Xu</name></country><country name="États-Unis"><noRegion><name sortKey="Shen, F" sort="Shen, F" uniqKey="Shen F" first="F." last="Shen">F. Shen</name></noRegion></country><country name="France"><region name="Grand Est"><name sortKey="Hu, G H" sort="Hu, G H" uniqKey="Hu G" first="G.-H." last="Hu">Guo-Hua Hu</name></region></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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