Hydrogenated Nitrile Butadiene Rubber and Hindered Phenol Composite. II. Characterization of Hydrogen Bonding
Identifieur interne : 000582 ( Hal/Corpus ); précédent : 000581; suivant : 000583Hydrogenated Nitrile Butadiene Rubber and Hindered Phenol Composite. II. Characterization of Hydrogen Bonding
Auteurs : Y. Y. Cao ; H. Y. Mou ; F. Shen ; H. Y. Xu ; G.-H. Hu ; C. F. WuSource :
- Polymer Engineering and Science [ 0032-3888 ] ; 2011.
Abstract
This article reports on the relationship between the variation of hydrogen bonding and macroscopic properties of composites composed of hydrogenated nitrile butadiene rubber (HNBR) and 3,9-bis {1,1-dimethyl-2 [β-(3-tert-butyl-4-hydroxy-5-methylphenyl) propionyloxy] ethyl}-2,4,8,10-tetraoxaspiro [5,5]-undecane (AO-80). Hydrogen bonding of the composites was studied by Fourier-transform infrared (FT-IR) and ultraviolet (UV) spectroscopies. FT-IR spectra at room temperature revealed that the stretching vibration peak of OH and CO of AO-80 red shifted with increasing AO-80 content, whereas that of C≡N of HNBR blue shifted only when the AO-80 content exceeded 10 parts per 100 resin (phr). At elevated temperatures, the shift was the opposite for CO and C≡N bands resulting from hydrogen bonding dissociation. In the UV spectra, the E2 band of benzene ring of AO-80 exhibited two peaks differing in shape.
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DOI: 10.1002/pen.21795
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Hydrogen bonding of the composites was studied by Fourier-transform infrared (FT-IR) and ultraviolet (UV) spectroscopies. FT-IR spectra at room temperature revealed that the stretching vibration peak of OH and CO of AO-80 red shifted with increasing AO-80 content, whereas that of C≡N of HNBR blue shifted only when the AO-80 content exceeded 10 parts per 100 resin (phr). At elevated temperatures, the shift was the opposite for CO and C≡N bands resulting from hydrogen bonding dissociation. In the UV spectra, the E2 band of benzene ring of AO-80 exhibited two peaks differing in shape.</div></front></TEI><hal api="V3"><titleStmt><title xml:lang="en">Hydrogenated Nitrile Butadiene Rubber and Hindered Phenol Composite. II. Characterization of Hydrogen Bonding</title><author role="aut"><persName><forename type="first">Y.Y.</forename><surname>Cao</surname></persName><email></email><idno type="halauthor">623906</idno><affiliation ref="#struct-161125"></affiliation></author><author role="aut"><persName><forename type="first">H.Y.</forename><surname>Mou</surname></persName><email></email><idno type="halauthor">623907</idno><affiliation ref="#struct-161125"></affiliation></author><author role="aut"><persName><forename type="first">F.</forename><surname>Shen</surname></persName><email></email><idno type="halauthor">623908</idno><affiliation ref="#struct-161126"></affiliation></author><author role="aut"><persName><forename type="first">H.Y.</forename><surname>Xu</surname></persName><email></email><idno type="halauthor">623909</idno><affiliation ref="#struct-161125"></affiliation></author><author role="aut"><persName><forename type="first">G.-H.</forename><surname>Hu</surname></persName><email></email><idno type="halauthor">95873</idno><affiliation ref="#struct-211875"></affiliation><affiliation ref="#struct-56663"></affiliation></author><author role="aut"><persName><forename type="first">C.F.</forename><surname>Wu</surname></persName><email></email><idno type="halauthor">623910</idno><affiliation ref="#struct-161125"></affiliation></author><editor role="depositor"><persName><forename>Josiane</forename><surname>Moras</surname></persName><email>josiane.moras@ensic.inpl-nancy.fr</email></editor></titleStmt><editionStmt><edition n="v1" type="current"><date type="whenSubmitted">2011-07-07 09:50:55</date><date type="whenModified">2016-05-17 10:14:31</date><date type="whenReleased">2011-07-07 09:50:55</date><date type="whenProduced">2011</date></edition><respStmt><resp>contributor</resp><name key="109516"><persName><forename>Josiane</forename><surname>Moras</surname></persName><email>josiane.moras@ensic.inpl-nancy.fr</email></name></respStmt></editionStmt><publicationStmt><distributor>CCSD</distributor><idno type="halId">hal-00606681</idno><idno type="halUri">https://hal.archives-ouvertes.fr/hal-00606681</idno><idno type="halBibtex">cao:hal-00606681</idno><idno type="halRefHtml">Polymer Engineering and Science, Wiley-Blackwell, 2011, 51 ((1)), pp. 201-208. <10.1002/pen.21795></idno><idno type="halRef">Polymer Engineering and Science, Wiley-Blackwell, 2011, 51 ((1)), pp. 201-208. <10.1002/pen.21795></idno></publicationStmt><seriesStmt><idno type="stamp" n="CNRS">CNRS - Centre national de la recherche scientifique</idno><idno type="stamp" n="LRGP-UL">LRGP</idno><idno type="stamp" n="UNIV-LORRAINE">Université de Lorraine</idno></seriesStmt><notesStmt><note type="audience" n="2">International</note><note type="popular" n="0">No</note><note type="peer" n="1">Yes</note></notesStmt><sourceDesc><biblStruct><analytic><title xml:lang="en">Hydrogenated Nitrile Butadiene Rubber and Hindered Phenol Composite. II. Characterization of Hydrogen Bonding</title><author role="aut"><persName><forename type="first">Y.Y.</forename><surname>Cao</surname></persName><idno type="halAuthorId">623906</idno><affiliation ref="#struct-161125"></affiliation></author><author role="aut"><persName><forename type="first">H.Y.</forename><surname>Mou</surname></persName><idno type="halAuthorId">623907</idno><affiliation ref="#struct-161125"></affiliation></author><author role="aut"><persName><forename type="first">F.</forename><surname>Shen</surname></persName><idno type="halAuthorId">623908</idno><affiliation ref="#struct-161126"></affiliation></author><author role="aut"><persName><forename type="first">H.Y.</forename><surname>Xu</surname></persName><idno type="halAuthorId">623909</idno><affiliation ref="#struct-161125"></affiliation></author><author role="aut"><persName><forename type="first">G.-H.</forename><surname>Hu</surname></persName><idno type="halAuthorId">95873</idno><affiliation ref="#struct-211875"></affiliation><affiliation ref="#struct-56663"></affiliation></author><author role="aut"><persName><forename type="first">C.F.</forename><surname>Wu</surname></persName><idno type="halAuthorId">623910</idno><affiliation ref="#struct-161125"></affiliation></author></analytic><monogr><idno type="halJournalId" status="VALID">7873</idno><idno type="issn">0032-3888</idno><idno type="eissn">1548-2634</idno><title level="j">Polymer Engineering and Science</title><imprint><publisher>Wiley-Blackwell</publisher><biblScope unit="volume">51</biblScope><biblScope unit="issue">(1)</biblScope><biblScope unit="pp">pp. 201-208</biblScope><date type="datePub">2011</date></imprint></monogr><idno type="doi">10.1002/pen.21795</idno></biblStruct></sourceDesc><profileDesc><langUsage><language ident="en">English</language></langUsage><textClass><classCode scheme="halDomain" n="spi.gproc">Engineering Sciences [physics]/Chemical and Process Engineering</classCode><classCode scheme="halTypology" n="ART">Journal articles</classCode></textClass><abstract xml:lang="en">This article reports on the relationship between the variation of hydrogen bonding and macroscopic properties of composites composed of hydrogenated nitrile butadiene rubber (HNBR) and 3,9-bis {1,1-dimethyl-2 [β-(3-tert-butyl-4-hydroxy-5-methylphenyl) propionyloxy] ethyl}-2,4,8,10-tetraoxaspiro [5,5]-undecane (AO-80). Hydrogen bonding of the composites was studied by Fourier-transform infrared (FT-IR) and ultraviolet (UV) spectroscopies. FT-IR spectra at room temperature revealed that the stretching vibration peak of OH and CO of AO-80 red shifted with increasing AO-80 content, whereas that of C≡N of HNBR blue shifted only when the AO-80 content exceeded 10 parts per 100 resin (phr). At elevated temperatures, the shift was the opposite for CO and C≡N bands resulting from hydrogen bonding dissociation. In the UV spectra, the E2 band of benzene ring of AO-80 exhibited two peaks differing in shape.</abstract></profileDesc></hal></record>Pour manipuler ce document sous Unix (Dilib)
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