Bis(3-aminopyrazine-2-carboxylato-κ2N1,O)diaquacobalt(II)
Identifieur interne : 000211 ( Pmc/Checkpoint ); précédent : 000210; suivant : 000212Bis(3-aminopyrazine-2-carboxylato-κ2N1,O)diaquacobalt(II)
Auteurs : Rafika Bouchene [Algérie] ; Sofiane Bouacida [Algérie] ; Fadila Berrah [Algérie] ; Ratiba Belhouas [Algérie] ; Hocine Merazig [Algérie]Source :
- Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2013.
Abstract
In the title compound, [Co(C5H4N3O2)2(H2O)2], the CoII atom is situated on a twofold rotation axis and is
Url:
DOI: 10.1107/S1600536813002183
PubMed: 23424419
PubMed Central: 3569217
Affiliations:
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Bis(3-aminopyrazine-2-carboxylato-κ<sup>2</sup>
<italic>N</italic>
<sup>1</sup>
,<italic>O</italic>
)diaquacobalt(II)</title>
<author><name sortKey="Bouchene, Rafika" sort="Bouchene, Rafika" uniqKey="Bouchene R" first="Rafika" last="Bouchene">Rafika Bouchene</name>
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</nlm:aff>
<country xml:lang="fr">Algérie</country>
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<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
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<author><name sortKey="Bouacida, Sofiane" sort="Bouacida, Sofiane" uniqKey="Bouacida S" first="Sofiane" last="Bouacida">Sofiane Bouacida</name>
<affiliation wicri:level="1"><nlm:aff id="c">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
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<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
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<author><name sortKey="Berrah, Fadila" sort="Berrah, Fadila" uniqKey="Berrah F" first="Fadila" last="Berrah">Fadila Berrah</name>
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</nlm:aff>
<country xml:lang="fr">Algérie</country>
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<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
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<country xml:lang="fr">Algérie</country>
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<author><name sortKey="Belhouas, Ratiba" sort="Belhouas, Ratiba" uniqKey="Belhouas R" first="Ratiba" last="Belhouas">Ratiba Belhouas</name>
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<country xml:lang="fr">Algérie</country>
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<author><name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Bis(3-aminopyrazine-2-carboxylato-κ<sup>2</sup>
<italic>N</italic>
<sup>1</sup>
,<italic>O</italic>
)diaquacobalt(II)</title>
<author><name sortKey="Bouchene, Rafika" sort="Bouchene, Rafika" uniqKey="Bouchene R" first="Rafika" last="Bouchene">Rafika Bouchene</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie Appliquée et Technologie des Matériaux LCATM, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Bouacida, Sofiane" sort="Bouacida, Sofiane" uniqKey="Bouacida S" first="Sofiane" last="Bouacida">Sofiane Bouacida</name>
<affiliation wicri:level="1"><nlm:aff id="c">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Berrah, Fadila" sort="Berrah, Fadila" uniqKey="Berrah F" first="Fadila" last="Berrah">Fadila Berrah</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie Appliquée et Technologie des Matériaux LCATM, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Belhouas, Ratiba" sort="Belhouas, Ratiba" uniqKey="Belhouas R" first="Ratiba" last="Belhouas">Ratiba Belhouas</name>
<affiliation wicri:level="1"><nlm:aff id="c">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
<affiliation wicri:level="1"><nlm:aff id="c">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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</analytic>
<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2013">2013</date>
</imprint>
</series>
</biblStruct>
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<front><div type="abstract" xml:lang="en"><p>In the title compound, [Co(C<sub>5</sub>
H<sub>4</sub>
N<sub>3</sub>
O<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
], the Co<sup>II</sup>
atom is situated on a twofold rotation axis and is <italic>N</italic>
,<italic>O</italic>
-chelated by two 3-aminopyrazine-2-carboxylate anions and additionally bonded to the O atoms of two water molecules, leading to a slightly distorted octahedral coordination environment. The crystal packing is dominated by intermolecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonding involving the water molecules and amino groups as donors and carboxylate O atoms, as well as the non-coordinating heterocyclic N atoms as acceptors, resulting in a three-dimensional network. An intramolecular N—H⋯O hydrogen bond is also observed.</p>
</div>
</front>
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<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
<front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="iso-abbrev">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Structure Reports Online</journal-title>
</journal-title-group>
<issn pub-type="epub">1600-5368</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">23424419</article-id>
<article-id pub-id-type="pmc">3569217</article-id>
<article-id pub-id-type="publisher-id">wm2721</article-id>
<article-id pub-id-type="doi">10.1107/S1600536813002183</article-id>
<article-id pub-id-type="coden">ACSEBH</article-id>
<article-id pub-id-type="pii">S1600536813002183</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Metal-Organic Papers</subject>
</subj-group>
</article-categories>
<title-group><article-title>Bis(3-aminopyrazine-2-carboxylato-κ<sup>2</sup>
<italic>N</italic>
<sup>1</sup>
,<italic>O</italic>
)diaquacobalt(II)</article-title>
<alt-title><italic>[Co(C<sub>5</sub>
H<sub>4</sub>
N<sub>3</sub>
O<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
]</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Bouchene</surname>
<given-names>Rafika</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Bouacida</surname>
<given-names>Sofiane</given-names>
</name>
<xref ref-type="aff" rid="c">c</xref>
<xref ref-type="aff" rid="b">b</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Berrah</surname>
<given-names>Fadila</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Belhouas</surname>
<given-names>Ratiba</given-names>
</name>
<xref ref-type="aff" rid="c">c</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Merazig</surname>
<given-names>Hocine</given-names>
</name>
<xref ref-type="aff" rid="c">c</xref>
</contrib>
<aff id="a"><label>a</label>
Laboratoire de Chimie Appliquée et Technologie des Matériaux LCATM, Université Oum El Bouaghi,<country>Algeria</country>
</aff>
<aff id="b"><label>b</label>
Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</aff>
<aff id="c"><label>c</label>
Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>bouacida_sofiane@yahoo.fr</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>2</month>
<year>2013</year>
</pub-date>
<pub-date pub-type="epub"><day>31</day>
<month>1</month>
<year>2013</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>31</day>
<month>1</month>
<year>2013</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the
. </pmc-comment>
<volume>69</volume>
<issue>Pt 2</issue>
<issue-id pub-id-type="publisher-id">e130200</issue-id>
<fpage>m129</fpage>
<lpage>m130</lpage>
<history><date date-type="received"><day>17</day>
<month>1</month>
<year>2013</year>
</date>
<date date-type="accepted"><day>22</day>
<month>1</month>
<year>2013</year>
</date>
</history>
<permissions><copyright-statement>© Bouchene et al. 2013</copyright-statement>
<copyright-year>2013</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S1600536813002183">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract><p>In the title compound, [Co(C<sub>5</sub>
H<sub>4</sub>
N<sub>3</sub>
O<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
], the Co<sup>II</sup>
atom is situated on a twofold rotation axis and is <italic>N</italic>
,<italic>O</italic>
-chelated by two 3-aminopyrazine-2-carboxylate anions and additionally bonded to the O atoms of two water molecules, leading to a slightly distorted octahedral coordination environment. The crystal packing is dominated by intermolecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonding involving the water molecules and amino groups as donors and carboxylate O atoms, as well as the non-coordinating heterocyclic N atoms as acceptors, resulting in a three-dimensional network. An intramolecular N—H⋯O hydrogen bond is also observed.</p>
</abstract>
</article-meta>
</front>
<floats-group><table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Hydrogen-bond geometry (Å, °)</title>
</caption>
<table frame="hsides" rules="groups"><thead valign="bottom"><tr><th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom">H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
</tr>
</thead>
<tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H1<italic>W</italic>
⋯N2<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.761 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.070 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.8254 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">172.2 (17)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H2<italic>W</italic>
⋯O52<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.762 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.898 (17)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.6470 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">167.1 (16)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">N3—H3<italic>A</italic>
⋯O51<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.86</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.33</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.0525 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">141</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">N3—H3<italic>B</italic>
⋯O52</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.86</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.07</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.7036 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">130</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry codes: (i) <inline-formula><inline-graphic xlink:href="e-69-0m129-efi3.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (ii) <inline-formula><inline-graphic xlink:href="e-69-0m129-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iii) <inline-formula><inline-graphic xlink:href="e-69-0m129-efi5.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
<affiliations><list><country><li>Algérie</li>
</country>
</list>
<tree><country name="Algérie"><noRegion><name sortKey="Bouchene, Rafika" sort="Bouchene, Rafika" uniqKey="Bouchene R" first="Rafika" last="Bouchene">Rafika Bouchene</name>
</noRegion>
<name sortKey="Belhouas, Ratiba" sort="Belhouas, Ratiba" uniqKey="Belhouas R" first="Ratiba" last="Belhouas">Ratiba Belhouas</name>
<name sortKey="Berrah, Fadila" sort="Berrah, Fadila" uniqKey="Berrah F" first="Fadila" last="Berrah">Fadila Berrah</name>
<name sortKey="Berrah, Fadila" sort="Berrah, Fadila" uniqKey="Berrah F" first="Fadila" last="Berrah">Fadila Berrah</name>
<name sortKey="Bouacida, Sofiane" sort="Bouacida, Sofiane" uniqKey="Bouacida S" first="Sofiane" last="Bouacida">Sofiane Bouacida</name>
<name sortKey="Bouacida, Sofiane" sort="Bouacida, Sofiane" uniqKey="Bouacida S" first="Sofiane" last="Bouacida">Sofiane Bouacida</name>
<name sortKey="Bouchene, Rafika" sort="Bouchene, Rafika" uniqKey="Bouchene R" first="Rafika" last="Bouchene">Rafika Bouchene</name>
<name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
</country>
</tree>
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HfdIndexSelect -h $EXPLOR_AREA/Data/Pmc/Checkpoint/RBID.i -Sk "pubmed:23424419" \ | HfdSelect -Kh $EXPLOR_AREA/Data/Pmc/Checkpoint/biblio.hfd \ | NlmPubMed2Wicri -a CobaltMaghrebV1
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