CobaltMaghrebV1, Pmc, Checkpoint, bibRecord, 000211

Bis(3-aminopyrazine-2-carboxylato-κ2N1,O)diaquacobalt(II)

Identifieur interne : 000211 ( Pmc/Checkpoint ); précédent : 000210; suivant : 000212

Bis(3-aminopyrazine-2-carboxylato-κ2N1,O)diaquacobalt(II)

Auteurs : Rafika Bouchene [Algérie] ; Sofiane Bouacida [Algérie] ; Fadila Berrah [Algérie] ; Ratiba Belhouas [Algérie] ; Hocine Merazig [Algérie]

Source :

Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2013.

RBID : PMC:3569217

Abstract

In the title compound, [Co(C₅H₄N₃O₂)₂(H₂O)₂], the Co^II atom is situated on a twofold rotation axis and is N,O-chelated by two 3-aminopyrazine-2-carboxylate anions and additionally bonded to the O atoms of two water molecules, leading to a slightly distorted octahedral coordination environment. The crystal packing is dominated by intermolecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonding involving the water molecules and amino groups as donors and carboxylate O atoms, as well as the non-coordinating heterocyclic N atoms as acceptors, resulting in a three-dimensional network. An intramolecular N—H⋯O hydrogen bond is also observed.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3569217

DOI: 10.1107/S1600536813002183
PubMed: 23424419
PubMed Central: 3569217

Affiliations:

Algérie

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to stream Pmc, to step Corpus: 000361
to stream Pmc, to step Curation: 000360

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PMC:3569217

Le document en format XML

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<italic>N</italic>
<sup>1</sup>
,<italic>O</italic>
)diaquacobalt(II)</title>
<author><name sortKey="Bouchene, Rafika" sort="Bouchene, Rafika" uniqKey="Bouchene R" first="Rafika" last="Bouchene">Rafika Bouchene</name>
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</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Bouacida, Sofiane" sort="Bouacida, Sofiane" uniqKey="Bouacida S" first="Sofiane" last="Bouacida">Sofiane Bouacida</name>
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</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
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</nlm:aff>
<country xml:lang="fr">Algérie</country>
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<country xml:lang="fr">Algérie</country>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Bis(3-aminopyrazine-2-carboxylato-κ<sup>2</sup>
<italic>N</italic>
<sup>1</sup>
,<italic>O</italic>
)diaquacobalt(II)</title>
<author><name sortKey="Bouchene, Rafika" sort="Bouchene, Rafika" uniqKey="Bouchene R" first="Rafika" last="Bouchene">Rafika Bouchene</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie Appliquée et Technologie des Matériaux LCATM, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Bouacida, Sofiane" sort="Bouacida, Sofiane" uniqKey="Bouacida S" first="Sofiane" last="Bouacida">Sofiane Bouacida</name>
<affiliation wicri:level="1"><nlm:aff id="c">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Berrah, Fadila" sort="Berrah, Fadila" uniqKey="Berrah F" first="Fadila" last="Berrah">Fadila Berrah</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie Appliquée et Technologie des Matériaux LCATM, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
<affiliation wicri:level="1"><nlm:aff id="b">Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Belhouas, Ratiba" sort="Belhouas, Ratiba" uniqKey="Belhouas R" first="Ratiba" last="Belhouas">Ratiba Belhouas</name>
<affiliation wicri:level="1"><nlm:aff id="c">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
<affiliation wicri:level="1"><nlm:aff id="c">Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</nlm:aff>
<country xml:lang="fr">Algérie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
</analytic>
<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2013">2013</date>
</imprint>
</series>
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<front><div type="abstract" xml:lang="en"><p>In the title compound, [Co(C<sub>5</sub>
H<sub>4</sub>
N<sub>3</sub>
O<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
], the Co<sup>II</sup>
 atom is situated on a twofold rotation axis and is <italic>N</italic>
,<italic>O</italic>
-chelated by two 3-aminopyrazine-2-carboxylate anions and additionally bonded to the O atoms of two water molecules, leading to a slightly distorted octahedral coordination environment. The crystal packing is dominated by intermolecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonding involving the water molecules and amino groups as donors and carboxylate O atoms, as well as the non-coordinating heterocyclic N atoms as acceptors, resulting in a three-dimensional network. An intramolecular N—H⋯O hydrogen bond is also observed.</p>
</div>
</front>
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<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
  <front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="iso-abbrev">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Structure Reports Online</journal-title>
</journal-title-group>
<issn pub-type="epub">1600-5368</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">23424419</article-id>
<article-id pub-id-type="pmc">3569217</article-id>
<article-id pub-id-type="publisher-id">wm2721</article-id>
<article-id pub-id-type="doi">10.1107/S1600536813002183</article-id>
<article-id pub-id-type="coden">ACSEBH</article-id>
<article-id pub-id-type="pii">S1600536813002183</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Metal-Organic Papers</subject>
</subj-group>
</article-categories>
<title-group><article-title>Bis(3-aminopyrazine-2-carboxylato-κ<sup>2</sup>
<italic>N</italic>
<sup>1</sup>
,<italic>O</italic>
)diaquacobalt(II)</article-title>
<alt-title><italic>[Co(C<sub>5</sub>
H<sub>4</sub>
N<sub>3</sub>
O<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
]</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Bouchene</surname>
<given-names>Rafika</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Bouacida</surname>
<given-names>Sofiane</given-names>
</name>
<xref ref-type="aff" rid="c">c</xref>
<xref ref-type="aff" rid="b">b</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Berrah</surname>
<given-names>Fadila</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Belhouas</surname>
<given-names>Ratiba</given-names>
</name>
<xref ref-type="aff" rid="c">c</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Merazig</surname>
<given-names>Hocine</given-names>
</name>
<xref ref-type="aff" rid="c">c</xref>
</contrib>
<aff id="a"><label>a</label>
Laboratoire de Chimie Appliquée et Technologie des Matériaux LCATM, Université Oum El Bouaghi,<country>Algeria</country>
</aff>
<aff id="b"><label>b</label>
Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi,<country>Algeria</country>
</aff>
<aff id="c"><label>c</label>
Unité de Recherche de Chimie de l’Environnement et Moléculaire Structurale, CHEMS, Faculté des Sciences Exactes, Université Mentouri Constantine 25000,<country>Algeria</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>bouacida_sofiane@yahoo.fr</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>2</month>
<year>2013</year>
</pub-date>
<pub-date pub-type="epub"><day>31</day>
<month>1</month>
<year>2013</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>31</day>
<month>1</month>
<year>2013</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the 
 							. </pmc-comment>
      <volume>69</volume>
<issue>Pt 2</issue>
<issue-id pub-id-type="publisher-id">e130200</issue-id>
<fpage>m129</fpage>
<lpage>m130</lpage>
<history><date date-type="received"><day>17</day>
<month>1</month>
<year>2013</year>
</date>
<date date-type="accepted"><day>22</day>
<month>1</month>
<year>2013</year>
</date>
</history>
<permissions><copyright-statement>© Bouchene et al. 2013</copyright-statement>
<copyright-year>2013</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S1600536813002183">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract><p>In the title compound, [Co(C<sub>5</sub>
H<sub>4</sub>
N<sub>3</sub>
O<sub>2</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>2</sub>
], the Co<sup>II</sup>
 atom is situated on a twofold rotation axis and is <italic>N</italic>
,<italic>O</italic>
-chelated by two 3-aminopyrazine-2-carboxylate anions and additionally bonded to the O atoms of two water molecules, leading to a slightly distorted octahedral coordination environment. The crystal packing is dominated by intermolecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonding involving the water molecules and amino groups as donors and carboxylate O atoms, as well as the non-coordinating heterocyclic N atoms as acceptors, resulting in a three-dimensional network. An intramolecular N—H⋯O hydrogen bond is also observed.</p>
</abstract>
</article-meta>
</front>
<floats-group><table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Hydrogen-bond geometry (Å, °)</title>
</caption>
<table frame="hsides" rules="groups"><thead valign="bottom"><tr><th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom">H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
</tr>
</thead>
<tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H1<italic>W</italic>
⋯N2<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.761 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.070 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.8254 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">172.2 (17)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1<italic>W</italic>
—H2<italic>W</italic>
⋯O52<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.762 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.898 (17)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.6470 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">167.1 (16)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">N3—H3<italic>A</italic>
⋯O51<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.86</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.33</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.0525 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">141</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">N3—H3<italic>B</italic>
⋯O52</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.86</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.07</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.7036 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">130</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry codes: (i) <inline-formula><inline-graphic xlink:href="e-69-0m129-efi3.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (ii) <inline-formula><inline-graphic xlink:href="e-69-0m129-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iii) <inline-formula><inline-graphic xlink:href="e-69-0m129-efi5.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
<affiliations><list><country><li>Algérie</li>
</country>
</list>
<tree><country name="Algérie"><noRegion><name sortKey="Bouchene, Rafika" sort="Bouchene, Rafika" uniqKey="Bouchene R" first="Rafika" last="Bouchene">Rafika Bouchene</name>
</noRegion>
<name sortKey="Belhouas, Ratiba" sort="Belhouas, Ratiba" uniqKey="Belhouas R" first="Ratiba" last="Belhouas">Ratiba Belhouas</name>
<name sortKey="Berrah, Fadila" sort="Berrah, Fadila" uniqKey="Berrah F" first="Fadila" last="Berrah">Fadila Berrah</name>
<name sortKey="Berrah, Fadila" sort="Berrah, Fadila" uniqKey="Berrah F" first="Fadila" last="Berrah">Fadila Berrah</name>
<name sortKey="Bouacida, Sofiane" sort="Bouacida, Sofiane" uniqKey="Bouacida S" first="Sofiane" last="Bouacida">Sofiane Bouacida</name>
<name sortKey="Bouacida, Sofiane" sort="Bouacida, Sofiane" uniqKey="Bouacida S" first="Sofiane" last="Bouacida">Sofiane Bouacida</name>
<name sortKey="Bouchene, Rafika" sort="Bouchene, Rafika" uniqKey="Bouchene R" first="Rafika" last="Bouchene">Rafika Bouchene</name>
<name sortKey="Merazig, Hocine" sort="Merazig, Hocine" uniqKey="Merazig H" first="Hocine" last="Merazig">Hocine Merazig</name>
</country>
</tree>
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</record>

Pour manipuler ce document sous Unix (Dilib)

EXPLOR_STEP=$WICRI_ROOT/Wicri/Terre/explor/CobaltMaghrebV1/Data/Pmc/Checkpoint

HfdSelect -h $EXPLOR_STEP/biblio.hfd -nk 000211 | SxmlIndent | more

HfdSelect -h $EXPLOR_AREA/Data/Pmc/Checkpoint/biblio.hfd -nk 000211 | SxmlIndent | more

Pour mettre un lien sur cette page dans le réseau Wicri

{{Explor lien
   |wiki=    Wicri/Terre
   |area=    CobaltMaghrebV1
   |flux=    Pmc
   |étape=   Checkpoint
   |type=    RBID
   |clé=     PMC:3569217
   |texte=   Bis(3-aminopyrazine-2-carboxylato-κ2N1,O)diaquacobalt(II)
}}

Pour générer des pages wiki

HfdIndexSelect -h $EXPLOR_AREA/Data/Pmc/Checkpoint/RBID.i   -Sk "pubmed:23424419" \
       | HfdSelect -Kh $EXPLOR_AREA/Data/Pmc/Checkpoint/biblio.hfd   \
       | NlmPubMed2Wicri -a CobaltMaghrebV1

This area was generated with Dilib version V0.6.32.
Data generation: Tue Nov 14 12:56:51 2017. Site generation: Mon Feb 12 07:59:49 2024

	Serveur d'exploration sur le cobalt au Maghreb
	Attention, ce site est en cours de développement ! Attention, site généré par des moyens informatiques à partir de corpus bruts. Les informations ne sont donc pas validées.

Serveur d'exploration sur le cobalt au Maghreb

Bis(3-amino­pyrazine-2-carboxyl­ato-κ2N1,O)diaqua­cobalt(II)

Bis(3-amino­pyrazine-2-carboxyl­ato-κ2N1,O)diaqua­cobalt(II)

Source :

Abstract

Links toward previous steps (curation, corpus...)

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri

Pour générer des pages wiki

Bis(3-aminopyrazine-2-carboxylato-κ2N1,O)diaquacobalt(II)

Bis(3-aminopyrazine-2-carboxylato-κ2N1,O)diaquacobalt(II)