Crystal structure of strontium dicobalt iron(III) tris(orthophosphate): SrCo2Fe(PO4)3
Identifieur interne : 000036 ( Pmc/Checkpoint ); précédent : 000035; suivant : 000037Crystal structure of strontium dicobalt iron(III) tris(orthophosphate): SrCo2Fe(PO4)3
Auteurs : Adam Bouraima [Maroc, Gabon] ; Thomas Makani [Gabon] ; Abderrazzak Assani [Maroc] ; Mohamed Saadi [Maroc] ; Lahcen El Ammari [Maroc]Source :
- Acta Crystallographica Section E: Crystallographic Communications [ 2056-9890 ] ; 2016.
Abstract
The transition metal orthophosphate, SrCo2Fe(PO4)3, crystallizes in an alluaudite-type structure. The chains characterizing the alluaudite structure are built up from edge-sharing [CoO6] octahedra linked together by PO4 tetrahedra.
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DOI: 10.1107/S2056989016011373
PubMed: 27536399
PubMed Central: 4971858
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Crystal structure of strontium dicobalt iron(III) tris(orthophosphate): SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub></title><author><name sortKey="Bouraima, Adam" sort="Bouraima, Adam" uniqKey="Bouraima A" first="Adam" last="Bouraima">Adam Bouraima</name><affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation><affiliation wicri:level="1"><nlm:aff id="b">Département de Chimie, Faculté des Sciences, Université des Sciences et Techniques de Masuku, BP 943, Franceville,<country>Gabon</country></nlm:aff><country xml:lang="fr">Gabon</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="Makani, Thomas" sort="Makani, Thomas" uniqKey="Makani T" first="Thomas" last="Makani">Thomas Makani</name><affiliation wicri:level="1"><nlm:aff id="b">Département de Chimie, Faculté des Sciences, Université des Sciences et Techniques de Masuku, BP 943, Franceville,<country>Gabon</country></nlm:aff><country xml:lang="fr">Gabon</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="Assani, Abderrazzak" sort="Assani, Abderrazzak" uniqKey="Assani A" first="Abderrazzak" last="Assani">Abderrazzak Assani</name><affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="Saadi, Mohamed" sort="Saadi, Mohamed" uniqKey="Saadi M" first="Mohamed" last="Saadi">Mohamed Saadi</name><affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="El Ammari, Lahcen" sort="El Ammari, Lahcen" uniqKey="El Ammari L" first="Lahcen" last="El Ammari">Lahcen El Ammari</name><affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">PMC</idno><idno type="pmid">27536399</idno><idno type="pmc">4971858</idno><idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC4971858</idno><idno type="RBID">PMC:4971858</idno><idno type="doi">10.1107/S2056989016011373</idno><date when="2016">2016</date><idno type="wicri:Area/Pmc/Corpus">000057</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Corpus" wicri:corpus="PMC">000057</idno><idno type="wicri:Area/Pmc/Curation">000057</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Curation">000057</idno><idno type="wicri:Area/Pmc/Checkpoint">000036</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Checkpoint">000036</idno></publicationStmt><sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Crystal structure of strontium dicobalt iron(III) tris(orthophosphate): SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub></title><author><name sortKey="Bouraima, Adam" sort="Bouraima, Adam" uniqKey="Bouraima A" first="Adam" last="Bouraima">Adam Bouraima</name><affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation><affiliation wicri:level="1"><nlm:aff id="b">Département de Chimie, Faculté des Sciences, Université des Sciences et Techniques de Masuku, BP 943, Franceville,<country>Gabon</country></nlm:aff><country xml:lang="fr">Gabon</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="Makani, Thomas" sort="Makani, Thomas" uniqKey="Makani T" first="Thomas" last="Makani">Thomas Makani</name><affiliation wicri:level="1"><nlm:aff id="b">Département de Chimie, Faculté des Sciences, Université des Sciences et Techniques de Masuku, BP 943, Franceville,<country>Gabon</country></nlm:aff><country xml:lang="fr">Gabon</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="Assani, Abderrazzak" sort="Assani, Abderrazzak" uniqKey="Assani A" first="Abderrazzak" last="Assani">Abderrazzak Assani</name><affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="Saadi, Mohamed" sort="Saadi, Mohamed" uniqKey="Saadi M" first="Mohamed" last="Saadi">Mohamed Saadi</name><affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author><author><name sortKey="El Ammari, Lahcen" sort="El Ammari, Lahcen" uniqKey="El Ammari L" first="Lahcen" last="El Ammari">Lahcen El Ammari</name><affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea># see nlm:aff country strict</wicri:regionArea></affiliation></author></analytic><series><title level="j">Acta Crystallographica Section E: Crystallographic Communications</title><idno type="eISSN">2056-9890</idno><imprint><date when="2016">2016</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p>The transition metal orthophosphate, SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub>, crystallizes in an alluaudite-type structure. The chains characterizing the alluaudite structure are built up from edge-sharing [CoO<sub>6</sub>] octahedra linked together by PO<sub>4</sub> tetrahedra.</p></div></front><back><div1 type="bibliography"><listBibl><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct><biblStruct></biblStruct></listBibl></div1></back></TEI><pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
<front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr E Crystallogr Commun</journal-id><journal-id journal-id-type="iso-abbrev">Acta Crystallogr E Crystallogr Commun</journal-id><journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id><journal-title-group><journal-title>Acta Crystallographica Section E: Crystallographic Communications</journal-title></journal-title-group><issn pub-type="epub">2056-9890</issn><publisher><publisher-name>International Union of Crystallography</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="pmid">27536399</article-id><article-id pub-id-type="pmc">4971858</article-id><article-id pub-id-type="publisher-id">pk2584</article-id><article-id pub-id-type="doi">10.1107/S2056989016011373</article-id><article-id pub-id-type="coden">ACSECI</article-id><article-id pub-id-type="pii">S2056989016011373</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Communications</subject></subj-group></article-categories><title-group><article-title>Crystal structure of strontium dicobalt iron(III) tris(orthophosphate): SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub></article-title><alt-title><italic>SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub></italic></alt-title></title-group><contrib-group><contrib contrib-type="author"><name><surname>Bouraima</surname><given-names>Adam</given-names></name><xref ref-type="aff" rid="a">a</xref><xref ref-type="aff" rid="b">b</xref><xref ref-type="corresp" rid="cor">*</xref></contrib><contrib contrib-type="author"><name><surname>Makani</surname><given-names>Thomas</given-names></name><xref ref-type="aff" rid="b">b</xref></contrib><contrib contrib-type="author"><name><surname>Assani</surname><given-names>Abderrazzak</given-names></name><xref ref-type="aff" rid="a">a</xref></contrib><contrib contrib-type="author"><name><surname>Saadi</surname><given-names>Mohamed</given-names></name><xref ref-type="aff" rid="a">a</xref></contrib><contrib contrib-type="author"><name><surname>El Ammari</surname><given-names>Lahcen</given-names></name><xref ref-type="aff" rid="a">a</xref></contrib><aff id="a"><label>a</label>Laboratoire de Chimie du Solide Appliquée, Faculty of Sciences, Mohammed V University in Rabat, Avenue Ibn Battouta, BP 1014, Rabat,<country>Morocco</country></aff><aff id="b"><label>b</label>Département de Chimie, Faculté des Sciences, Université des Sciences et Techniques de Masuku, BP 943, Franceville,<country>Gabon</country></aff></contrib-group><author-notes><corresp id="cor">Correspondence e-mail: <email>adam_bouraima@yahoo.fr</email></corresp></author-notes><pub-date pub-type="collection"><day>01</day><month>8</month><year>2016</year></pub-date><pub-date pub-type="epub"><day>19</day><month>7</month><year>2016</year></pub-date><pub-date pub-type="pmc-release"><day>19</day><month>7</month><year>2016</year></pub-date><pmc-comment> PMC Release delay is 0 months and 0 days and was based on the
<volume>72</volume><issue>Pt 8</issue><issue-id pub-id-type="publisher-id">e160800</issue-id><fpage>1143</fpage><lpage>1146</lpage><history><date date-type="received"><day>24</day><month>6</month><year>2016</year></date><date date-type="accepted"><day>12</day><month>7</month><year>2016</year></date></history><permissions><copyright-statement>© Bouraima et al. 2016</copyright-statement><copyright-year>2016</copyright-year><license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under
the terms of the Creative Commons Attribution
Licence, which permits unrestricted use,
distribution, and reproduction in any medium,
provided the original authors and source are
cited.</license-p></license></permissions><self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S2056989016011373">A full version of this
article is available from Crystallography Journals Online.</self-uri><abstract abstract-type="toc"><p>The transition metal orthophosphate, SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub>, crystallizes in an alluaudite-type structure. The chains characterizing the alluaudite structure are built up from edge-sharing [CoO<sub>6</sub>] octahedra linked together by PO<sub>4</sub> tetrahedra.</p></abstract><abstract><p>The title compound, SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub>, has been synthesized by a solid-state reaction. It crystallizes with the α-CrPO<sub>4</sub> type structure. In this structure, all atoms are on special positions of the <italic>Imma</italic> space group, except for two O atoms which are located on general positions. The three-dimensional network in the crystal structure is made up of two types of layers stacked normal to (100). The first layer is built from two edge-sharing CoO<sub>6</sub> octahedra, leading to the formation of Co<sub>2</sub>O<sub>10</sub> dimers that are connected to two PO<sub>4</sub> tetrahedra by a common edge and corners. The second layer results from apex-sharing FeO<sub>6</sub> octahedra and PO<sub>4</sub> tetrahedra, which form linear chains alternating with a zigzag chain of Sr<sup>II</sup> cations. These layers are linked together by common vertices of PO<sub>4</sub> tetrahedra and FeO<sub>6</sub> octahedra to form an open three-dimensional framework that delimits two types of channels parallel to [100] and [010] where the Sr<sup>II</sup> cations are located. Each Sr<sup>II</sup> cation is surrounded by eight O atoms.</p></abstract><kwd-group><kwd>crystal structure</kwd><kwd>SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub></kwd><kwd>transition metal phosphate</kwd><kwd>solid-state reaction synthesis</kwd><kwd>alluaudite-like structure</kwd></kwd-group></article-meta></front><floats-group><fig id="fig1" position="float"><label>Figure 1</label><caption><p>The principal building units in the structure of the title compound. Displacement ellipsoids are drawn at the 50% probability level. [Symmetry codes: (i) −<italic>x</italic> + 2, −<italic>y</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, <italic>z</italic> + 1; (ii) <italic>x</italic>, <italic>y</italic>, <italic>z</italic> + 1; (iii) −<italic>x</italic> + 2, −<italic>y</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, <italic>z</italic>; (iv) −<italic>x</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, −<italic>y</italic> + 1, <italic>z</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>; (v) <italic>x</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, <italic>y</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, <italic>z</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>; (vi) −<italic>x</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, <italic>y</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, <italic>z</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>; (ix) −<italic>x</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, <italic>y</italic>, −<italic>z</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>; (<italic>x</italic>) <italic>x</italic>, −<italic>y</italic> + 1, −<italic>z</italic>; (xi) −<italic>x</italic> + 1, <italic>y</italic>, <italic>z</italic>; (xii) <italic>x</italic>, −<italic>y</italic> + 1, −<italic>z</italic> + 1; (xiii) −<italic>x</italic> + 1, −<italic>y</italic> + 1, −<italic>z</italic> + 1;(xiv) <italic>x</italic> − <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>, <italic>y</italic>, −<italic>z</italic> + <inline-formula><inline-graphic xlink:href="e-72-01143-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic></inline-formula>.]</p></caption><graphic xlink:href="e-72-01143-fig1"></graphic></fig><fig id="fig2" position="float"><label>Figure 2</label><caption><p>Edge-sharing [CoO<sub>6</sub>] octahedra forming a layer parallel to (100).</p></caption><graphic xlink:href="e-72-01143-fig2"></graphic></fig><fig id="fig3" position="float"><label>Figure 3</label><caption><p>A view along the <italic>a</italic> axis, showing a layer resulting from chains connected <italic>via</italic> vertices of PO<sub>4</sub> tetrahedra and FeO<sub>6</sub> octahedra, alternating with a zigzag chain of Sr atoms.</p></caption><graphic xlink:href="e-72-01143-fig3"></graphic></fig><fig id="fig4" position="float"><label>Figure 4</label><caption><p>Polyhedral representation of SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub>, showing channels running along [100].</p></caption><graphic xlink:href="e-72-01143-fig4"></graphic></fig><fig id="fig5" position="float"><label>Figure 5</label><caption><p>Polyhedral representation of SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub>, showing channels running along [010].</p></caption><graphic xlink:href="e-72-01143-fig5"></graphic></fig><table-wrap id="table1" position="float"><label>Table 1</label><caption><title>Experimental details</title></caption><table frame="hsides" rules="groups"><tbody valign="top"><tr><td rowspan="1" colspan="2" align="left" valign="top">Crystal data</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">Chemical formula</td><td rowspan="1" colspan="1" align="left" valign="top">SrCo<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub></td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>M</italic><sub>r</sub></td><td rowspan="1" colspan="1" align="left" valign="top">546.24</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">Crystal system, space group</td><td rowspan="1" colspan="1" align="left" valign="top">Orthorhombic, <italic>I</italic><italic>m</italic><italic>m</italic><italic>a</italic></td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">Temperature (K)</td><td rowspan="1" colspan="1" align="left" valign="top">296</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>a</italic>, <italic>b</italic>, <italic>c</italic> (Å)</td><td rowspan="1" colspan="1" align="left" valign="top">10.4097 (2), 13.2714 (3), 6.5481 (2)</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>V</italic> (Å<sup>3</sup>)</td><td rowspan="1" colspan="1" align="left" valign="top">904.63 (4)</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>Z</italic></td><td rowspan="1" colspan="1" align="left" valign="top">4</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">Radiation type</td><td rowspan="1" colspan="1" align="left" valign="top">Mo <italic>K</italic>α</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">μ (mm<sup>−1</sup>)</td><td rowspan="1" colspan="1" align="left" valign="top">11.64</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">Crystal size (mm)</td><td rowspan="1" colspan="1" align="left" valign="top">0.30 × 0.27 × 0.21</td></tr><tr><td rowspan="1" colspan="2" align="left" valign="top"> </td></tr><tr><td rowspan="1" colspan="2" align="left" valign="top">Data collection</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">Diffractometer</td><td rowspan="1" colspan="1" align="left" valign="top">Bruker X8 APEX</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">Absorption correction</td><td rowspan="1" colspan="1" align="left" valign="top">Multi-scan (<italic>SADABS</italic>; Krause <italic>et al.</italic>, 2015<xref ref-type="bibr" rid="bb12"> ▸</xref>)</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>T</italic><sub>min</sub>, <italic>T</italic><sub>max</sub></td><td rowspan="1" colspan="1" align="left" valign="top">0.595, 0.747</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">No. of measured, independent and observed [<italic>I</italic> > 2σ(<italic>I</italic>)] reflections</td><td rowspan="1" colspan="1" align="left" valign="top">10008, 1297, 1243</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>R</italic><sub>int</sub></td><td rowspan="1" colspan="1" align="left" valign="top">0.030</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">(sin θ/λ)<sub>max</sub> (Å<sup>−1</sup>)</td><td rowspan="1" colspan="1" align="left" valign="top">0.858</td></tr><tr><td rowspan="1" colspan="2" align="left" valign="top"> </td></tr><tr><td rowspan="1" colspan="2" align="left" valign="top">Refinement</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>R</italic>[<italic>F</italic><sup>2</sup> > 2σ(<italic>F</italic><sup>2</sup>)], <italic>wR</italic>(<italic>F</italic><sup>2</sup>), <italic>S</italic></td><td rowspan="1" colspan="1" align="left" valign="top">0.017, 0.046, 1.16</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">No. of reflections</td><td rowspan="1" colspan="1" align="left" valign="top">1297</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">No. of parameters</td><td rowspan="1" colspan="1" align="left" valign="top">54</td></tr><tr><td rowspan="1" colspan="1" align="left" valign="top">Δρ<sub>max</sub>, Δρ<sub>min</sub> (e Å<sup>−3</sup>)</td><td rowspan="1" colspan="1" align="left" valign="top">1.00, −0.74</td></tr></tbody></table><table-wrap-foot><p>Computer programs: <italic>APEX2</italic> and <italic>SAINT</italic> (Bruker, 2009<xref ref-type="bibr" rid="bb7"> ▸</xref>), <italic>SHELXT2014</italic> (Sheldrick, 2015<italic>a</italic><xref ref-type="bibr" rid="bb15"> ▸</xref>), <italic>SHELXL2014</italic> (Sheldrick, 2015<italic>b</italic><xref ref-type="bibr" rid="bb16"> ▸</xref>), <italic>ORTEP-3 for Windows</italic> (Farrugia, 2012<xref ref-type="bibr" rid="bb8"> ▸</xref>), <italic>DIAMOND</italic> (Brandenburg, 2006<xref ref-type="bibr" rid="bb6"> ▸</xref>) and <italic>publCIF</italic> (Westrip, 2010<xref ref-type="bibr" rid="bb18"> ▸</xref>).</p></table-wrap-foot></table-wrap></floats-group></pmc><affiliations><list><country><li>Gabon</li><li>Maroc</li></country></list><tree><country name="Maroc"><noRegion><name sortKey="Bouraima, Adam" sort="Bouraima, Adam" uniqKey="Bouraima A" first="Adam" last="Bouraima">Adam Bouraima</name></noRegion><name sortKey="Assani, Abderrazzak" sort="Assani, Abderrazzak" uniqKey="Assani A" first="Abderrazzak" last="Assani">Abderrazzak Assani</name><name sortKey="El Ammari, Lahcen" sort="El Ammari, Lahcen" uniqKey="El Ammari L" first="Lahcen" last="El Ammari">Lahcen El Ammari</name><name sortKey="Saadi, Mohamed" sort="Saadi, Mohamed" uniqKey="Saadi M" first="Mohamed" last="Saadi">Mohamed Saadi</name></country><country name="Gabon"><noRegion><name sortKey="Bouraima, Adam" sort="Bouraima, Adam" uniqKey="Bouraima A" first="Adam" last="Bouraima">Adam Bouraima</name></noRegion><name sortKey="Makani, Thomas" sort="Makani, Thomas" uniqKey="Makani T" first="Thomas" last="Makani">Thomas Makani</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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