CobaltMaghrebV1, PascalFrancis, Corpus, bibRecord, 000288

Layered LiNi0.5Co0.5O2 cathode materials grown by soft-chemistry via various solution methods

Identifieur interne : 000288 ( PascalFrancis/Corpus ); précédent : 000287; suivant : 000289

Layered LiNi0.5Co0.5O2 cathode materials grown by soft-chemistry via various solution methods

Auteurs : C. Julien ; C. Letranchant ; S. Rangan ; M. Lemal ; S. Ziolkiewicz ; S. Castro-Garcia ; L. El-Farh ; M. Benkaddour

Source :

Materials science & engineering. B, Solid-state materials for advanced technology [ 0921-5107 ] ; 2000.

RBID : Pascal:00-0300818

Descripteurs français

Pascal (Inist)
- Batterie, Lithium Ion, Matériau électrode, Lithium Oxyde, Nickel Oxyde, Cobalt Oxyde, Structure lamellaire, Fabrication électrode, Solution aqueuse, Acide carboxylique, Séquestrant, Analyse thermique, Analyse thermique différentielle, Thermogravimétrie, Structure surface, Morphologie, Diffraction RX, Spectrométrie IR, Transformation Fourier, Caractéristique électrique, Cycle charge décharge, LiNi0,5Co0,5O2, Co Li Ni O.

English descriptors

KwdEn :
- Aqueous solution, Battery, Carboxylic acid, Cobalt Oxides, Complexing agent, Differential thermal analysis, Discharge charge cycle, Electrical characteristic, Electrode material, Electrode production, Fourier transformation, Infrared spectrometry, Lamellar structure, Lithium Ions, Lithium Oxides, Morphology, Nickel Oxides, Surface structure, Thermal analysis, Thermogravimetry, X ray diffraction.

Abstract

The lithiated nickel-cobalt oxide LiNi_0.5Co_0.5O₂ used as cathode material was grown at low-temperature using different aqueous solution methods. The wet chemistry involved the mixture of metal salts (acetates or nitrates) with various carboxylic acid-based aqueous solutions. Physicochemical and electrochemical properties of LiNi_0.5Co_0.5O₂ products calcined at 400-600°C were extensively investigated. The four methods used involved complexing agents such as either citric, oxalic, aminoacetic (glycine), or succinic acid in aqueous medium which functioned as a fuel, decomposed the metal complexes at low temperature, and yielded the free impurity LiNi_0.5Co_0.5O₂ compounds. Thermal (TG-DTA) analyses and XRD data show that powders grown with a layered structure (R3m space group) have been obtained at temperatures below 400°C by the acidification reaction of the aqueous solutions. The local structure of synthesized products was characterized by Fourier transform infrared (FTIR) spectroscopy. The electrochemical properties of the synthesized products were evaluated in rechargeable Li cells using a non-aqueous organic electrolyte (1 M LiClO₄ in propylene carbonate, PC). The LiNi_0.5Co_0.5O₂ positive electrodes fired at 600°C exhibited good cycling behavior.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

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A03		`1`		`@0 Mater. sci. eng., B, Solid-state mater. adv. technol.`
A05				`@2 76`
A06				`@2 2`
A08	`01`	`1`	`ENG`	`@1 Layered LiNi_0.5Co_0.5O₂ cathode materials grown by soft-chemistry via various solution methods`
A11	`01`	`1`		`@1 JULIEN (C.)`
A11	`02`	`1`		`@1 LETRANCHANT (C.)`
A11	`03`	`1`		`@1 RANGAN (S.)`
A11	`04`	`1`		`@1 LEMAL (M.)`
A11	`05`	`1`		`@1 ZIOLKIEWICZ (S.)`
A11	`06`	`1`		`@1 CASTRO-GARCIA (S.)`
A11	`07`	`1`		`@1 EL-FARH (L.)`
A11	`08`	`1`		`@1 BENKADDOUR (M.)`
A14	`01`			`@1 Laboratoire des Milieux Désordonnés et Hétérogènes, UMR7603, Université Pierre et Marie Curie, 4 place Jussieu @2 75252 Paris @3 FRA @Z 1 aut. @Z 2 aut. @Z 3 aut. @Z 4 aut. @Z 5 aut.`
A14	`02`			`@1 Departamento Quimica Fundamental e Industrial, Universidade A Coruna @2 15071 A Coruna @3 ESP @Z 6 aut.`
A14	`03`			`@1 Laboratoire d'Analyse et Caractérisation des Matériaux, Université Mohamed 1er, Faculté des Sciences @2 Oujda @3 MAR @Z 7 aut. @Z 8 aut.`
A20				`@1 145-155`
A21				`@1 2000`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 12899B @5 354000088714780110`
A44				`@0 0000 @1 © 2000 INIST-CNRS. All rights reserved.`
A45				`@0 40 ref.`
A47	`01`	`1`		`@0 00-0300818`
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A61				`@0 A`
A64	`01`	`1`		`@0 Materials science & engineering. B, Solid-state materials for advanced technology`
A66	`01`			`@0 CHE`
C01	`01`		`ENG`	@0 The lithiated nickel-cobalt oxide LiNi_0.5Co_0.5O₂ used as cathode material was grown at low-temperature using different aqueous solution methods. The wet chemistry involved the mixture of metal salts (acetates or nitrates) with various carboxylic acid-based aqueous solutions. Physicochemical and electrochemical properties of LiNi_0.5Co_0.5O₂ products calcined at 400-600°C were extensively investigated. The four methods used involved complexing agents such as either citric, oxalic, aminoacetic (glycine), or succinic acid in aqueous medium which functioned as a fuel, decomposed the metal complexes at low temperature, and yielded the free impurity LiNi_0.5Co_0.5O₂ compounds. Thermal (TG-DTA) analyses and XRD data show that powders grown with a layered structure (R3m space group) have been obtained at temperatures below 400°C by the acidification reaction of the aqueous solutions. The local structure of synthesized products was characterized by Fourier transform infrared (FTIR) spectroscopy. The electrochemical properties of the synthesized products were evaluated in rechargeable Li cells using a non-aqueous organic electrolyte (1 M LiClO₄ in propylene carbonate, PC). The LiNi_0.5Co_0.5O₂ positive electrodes fired at 600°C exhibited good cycling behavior.
C02	`01`	`X`		`@0 001D05I03E`
C03	`01`	`X`	`FRE`	`@0 Batterie @5 01`
C03	`01`	`X`	`ENG`	`@0 Battery @5 01`
C03	`01`	`X`	`SPA`	`@0 Batería @5 01`
C03	`02`	`X`	`FRE`	`@0 Lithium Ion @2 NC @2 NA @5 02`
C03	`02`	`X`	`ENG`	`@0 Lithium Ions @2 NC @2 NA @5 02`
C03	`02`	`X`	`SPA`	`@0 Litio Ión @2 NC @2 NA @5 02`
C03	`03`	`X`	`FRE`	`@0 Matériau électrode @5 03`
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C03	`03`	`X`	`SPA`	`@0 Material electrodo @5 03`
C03	`04`	`X`	`FRE`	`@0 Lithium Oxyde @2 NC @2 NA @5 04`
C03	`04`	`X`	`ENG`	`@0 Lithium Oxides @2 NC @2 NA @5 04`
C03	`04`	`X`	`SPA`	`@0 Litio Óxido @2 NC @2 NA @5 04`
C03	`05`	`X`	`FRE`	`@0 Nickel Oxyde @2 NC @2 FX @2 NA @5 05`
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C03	`06`	`X`	`FRE`	`@0 Cobalt Oxyde @2 NC @2 NA @5 06`
C03	`06`	`X`	`ENG`	`@0 Cobalt Oxides @2 NC @2 NA @5 06`
C03	`06`	`X`	`SPA`	`@0 Cobalto Óxido @2 NC @2 NA @5 06`
C03	`07`	`X`	`FRE`	`@0 Structure lamellaire @5 07`
C03	`07`	`X`	`ENG`	`@0 Lamellar structure @5 07`
C03	`07`	`X`	`SPA`	`@0 Estructura lamelar @5 07`
C03	`08`	`X`	`FRE`	`@0 Fabrication électrode @5 08`
C03	`08`	`X`	`ENG`	`@0 Electrode production @5 08`
C03	`08`	`X`	`SPA`	`@0 Fabricación electrodo @5 08`
C03	`09`	`X`	`FRE`	`@0 Solution aqueuse @5 09`
C03	`09`	`X`	`ENG`	`@0 Aqueous solution @5 09`
C03	`09`	`X`	`SPA`	`@0 Solución acuosa @5 09`
C03	`10`	`X`	`FRE`	`@0 Acide carboxylique @5 10`
C03	`10`	`X`	`ENG`	`@0 Carboxylic acid @5 10`
C03	`10`	`X`	`SPA`	`@0 Acido carboxílico @5 10`
C03	`11`	`X`	`FRE`	`@0 Séquestrant @5 11`
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C03	`15`	`X`	`FRE`	`@0 Structure surface @5 19`
C03	`15`	`X`	`ENG`	`@0 Surface structure @5 19`
C03	`15`	`X`	`SPA`	`@0 Estructura superficie @5 19`
C03	`16`	`X`	`FRE`	`@0 Morphologie @5 20`
C03	`16`	`X`	`ENG`	`@0 Morphology @5 20`
C03	`16`	`X`	`SPA`	`@0 Morfología @5 20`
C03	`17`	`X`	`FRE`	`@0 Diffraction RX @5 21`
C03	`17`	`X`	`ENG`	`@0 X ray diffraction @5 21`
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C03	`19`	`X`	`FRE`	`@0 Transformation Fourier @5 24`
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N21				`@1 206`

Format Inist (serveur)

NO :	PASCAL 00-0300818 INIST
ET :	Layered LiNi_0.5Co_0.5O₂ cathode materials grown by soft-chemistry via various solution methods
AU :	JULIEN (C.); LETRANCHANT (C.); RANGAN (S.); LEMAL (M.); ZIOLKIEWICZ (S.); CASTRO-GARCIA (S.); EL-FARH (L.); BENKADDOUR (M.)
AF :	Laboratoire des Milieux Désordonnés et Hétérogènes, UMR7603, Université Pierre et Marie Curie, 4 place Jussieu/75252 Paris/France (1 aut., 2 aut., 3 aut., 4 aut., 5 aut.); Departamento Quimica Fundamental e Industrial, Universidade A Coruna/15071 A Coruna/Espagne (6 aut.); Laboratoire d'Analyse et Caractérisation des Matériaux, Université Mohamed 1er, Faculté des Sciences/Oujda/Maroc (7 aut., 8 aut.)
DT :	Publication en série; Niveau analytique
SO :	Materials science & engineering. B, Solid-state materials for advanced technology; ISSN 0921-5107; Suisse; Da. 2000; Vol. 76; No. 2; Pp. 145-155; Bibl. 40 ref.
LA :	Anglais
EA :	The lithiated nickel-cobalt oxide LiNi_0.5Co_0.5O₂ used as cathode material was grown at low-temperature using different aqueous solution methods. The wet chemistry involved the mixture of metal salts (acetates or nitrates) with various carboxylic acid-based aqueous solutions. Physicochemical and electrochemical properties of LiNi_0.5Co_0.5O₂ products calcined at 400-600°C were extensively investigated. The four methods used involved complexing agents such as either citric, oxalic, aminoacetic (glycine), or succinic acid in aqueous medium which functioned as a fuel, decomposed the metal complexes at low temperature, and yielded the free impurity LiNi_0.5Co_0.5O₂ compounds. Thermal (TG-DTA) analyses and XRD data show that powders grown with a layered structure (R3m space group) have been obtained at temperatures below 400°C by the acidification reaction of the aqueous solutions. The local structure of synthesized products was characterized by Fourier transform infrared (FTIR) spectroscopy. The electrochemical properties of the synthesized products were evaluated in rechargeable Li cells using a non-aqueous organic electrolyte (1 M LiClO₄ in propylene carbonate, PC). The LiNi_0.5Co_0.5O₂ positive electrodes fired at 600°C exhibited good cycling behavior.
CC :	001D05I03E
FD :	Batterie; Lithium Ion; Matériau électrode; Lithium Oxyde; Nickel Oxyde; Cobalt Oxyde; Structure lamellaire; Fabrication électrode; Solution aqueuse; Acide carboxylique; Séquestrant; Analyse thermique; Analyse thermique différentielle; Thermogravimétrie; Structure surface; Morphologie; Diffraction RX; Spectrométrie IR; Transformation Fourier; Caractéristique électrique; Cycle charge décharge; LiNi0,5Co0,5O2; Co Li Ni O
ED :	Battery; Lithium Ions; Electrode material; Lithium Oxides; Nickel Oxides; Cobalt Oxides; Lamellar structure; Electrode production; Aqueous solution; Carboxylic acid; Complexing agent; Thermal analysis; Differential thermal analysis; Thermogravimetry; Surface structure; Morphology; X ray diffraction; Infrared spectrometry; Fourier transformation; Electrical characteristic; Discharge charge cycle
SD :	Batería; Litio Ión; Material electrodo; Litio Óxido; Niquel Óxido; Cobalto Óxido; Estructura lamelar; Fabricación electrodo; Solución acuosa; Acido carboxílico; Secuestrante; Análisis térmico; Análisis térmico diferencial; Termogravimetría; Estructura superficie; Morfología; Difracción RX; Espectrometría IR; Transformación Fourier; Característica eléctrica; Ciclo carga descarga
LO :	INIST-12899B.354000088714780110
ID :	00-0300818

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Pascal:00-0300818

Le document en format XML

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 cathode materials grown by soft-chemistry via various solution methods</title>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Layered LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 cathode materials grown by soft-chemistry via various solution methods</title>
<author><name sortKey="Julien, C" sort="Julien, C" uniqKey="Julien C" first="C." last="Julien">C. Julien</name>
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<author><name sortKey="Lemal, M" sort="Lemal, M" uniqKey="Lemal M" first="M." last="Lemal">M. Lemal</name>
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<author><name sortKey="Ziolkiewicz, S" sort="Ziolkiewicz, S" uniqKey="Ziolkiewicz S" first="S." last="Ziolkiewicz">S. Ziolkiewicz</name>
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<s3>MAR</s3>
<sZ>7 aut.</sZ>
<sZ>8 aut.</sZ>
</inist:fA14>
</affiliation>
</author>
<author><name sortKey="Benkaddour, M" sort="Benkaddour, M" uniqKey="Benkaddour M" first="M." last="Benkaddour">M. Benkaddour</name>
<affiliation><inist:fA14 i1="03"><s1>Laboratoire d'Analyse et Caractérisation des Matériaux, Université Mohamed 1er, Faculté des Sciences</s1>
<s2>Oujda</s2>
<s3>MAR</s3>
<sZ>7 aut.</sZ>
<sZ>8 aut.</sZ>
</inist:fA14>
</affiliation>
</author>
</analytic>
<series><title level="j" type="main">Materials science & engineering. B, Solid-state materials for advanced technology</title>
<title level="j" type="abbreviated">Mater. sci. eng., B, Solid-state mater. adv. technol.</title>
<idno type="ISSN">0921-5107</idno>
<imprint><date when="2000">2000</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
<seriesStmt><title level="j" type="main">Materials science & engineering. B, Solid-state materials for advanced technology</title>
<title level="j" type="abbreviated">Mater. sci. eng., B, Solid-state mater. adv. technol.</title>
<idno type="ISSN">0921-5107</idno>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Aqueous solution</term>
<term>Battery</term>
<term>Carboxylic acid</term>
<term>Cobalt Oxides</term>
<term>Complexing agent</term>
<term>Differential thermal analysis</term>
<term>Discharge charge cycle</term>
<term>Electrical characteristic</term>
<term>Electrode material</term>
<term>Electrode production</term>
<term>Fourier transformation</term>
<term>Infrared spectrometry</term>
<term>Lamellar structure</term>
<term>Lithium Ions</term>
<term>Lithium Oxides</term>
<term>Morphology</term>
<term>Nickel Oxides</term>
<term>Surface structure</term>
<term>Thermal analysis</term>
<term>Thermogravimetry</term>
<term>X ray diffraction</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Batterie</term>
<term>Lithium Ion</term>
<term>Matériau électrode</term>
<term>Lithium Oxyde</term>
<term>Nickel Oxyde</term>
<term>Cobalt Oxyde</term>
<term>Structure lamellaire</term>
<term>Fabrication électrode</term>
<term>Solution aqueuse</term>
<term>Acide carboxylique</term>
<term>Séquestrant</term>
<term>Analyse thermique</term>
<term>Analyse thermique différentielle</term>
<term>Thermogravimétrie</term>
<term>Structure surface</term>
<term>Morphologie</term>
<term>Diffraction RX</term>
<term>Spectrométrie IR</term>
<term>Transformation Fourier</term>
<term>Caractéristique électrique</term>
<term>Cycle charge décharge</term>
<term>LiNi0,5Co0,5O2</term>
<term>Co Li Ni O</term>
</keywords>
</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">The lithiated nickel-cobalt oxide LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 used as cathode material was grown at low-temperature using different aqueous solution methods. The wet chemistry involved the mixture of metal salts (acetates or nitrates) with various carboxylic acid-based aqueous solutions. Physicochemical and electrochemical properties of LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 products calcined at 400-600°C were extensively investigated. The four methods used involved complexing agents such as either citric, oxalic, aminoacetic (glycine), or succinic acid in aqueous medium which functioned as a fuel, decomposed the metal complexes at low temperature, and yielded the free impurity LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 compounds. Thermal (TG-DTA) analyses and XRD data show that powders grown with a layered structure (R3m space group) have been obtained at temperatures below 400°C by the acidification reaction of the aqueous solutions. The local structure of synthesized products was characterized by Fourier transform infrared (FTIR) spectroscopy. The electrochemical properties of the synthesized products were evaluated in rechargeable Li cells using a non-aqueous organic electrolyte (1 M LiClO<sub>4</sub>
 in propylene carbonate, PC). The LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 positive electrodes fired at 600°C exhibited good cycling behavior.</div>
</front>
</TEI>
<inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0921-5107</s0>
</fA01>
<fA03 i2="1"><s0>Mater. sci. eng., B, Solid-state mater. adv. technol.</s0>
</fA03>
<fA05><s2>76</s2>
</fA05>
<fA06><s2>2</s2>
</fA06>
<fA08 i1="01" i2="1" l="ENG"><s1>Layered LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 cathode materials grown by soft-chemistry via various solution methods</s1>
</fA08>
<fA11 i1="01" i2="1"><s1>JULIEN (C.)</s1>
</fA11>
<fA11 i1="02" i2="1"><s1>LETRANCHANT (C.)</s1>
</fA11>
<fA11 i1="03" i2="1"><s1>RANGAN (S.)</s1>
</fA11>
<fA11 i1="04" i2="1"><s1>LEMAL (M.)</s1>
</fA11>
<fA11 i1="05" i2="1"><s1>ZIOLKIEWICZ (S.)</s1>
</fA11>
<fA11 i1="06" i2="1"><s1>CASTRO-GARCIA (S.)</s1>
</fA11>
<fA11 i1="07" i2="1"><s1>EL-FARH (L.)</s1>
</fA11>
<fA11 i1="08" i2="1"><s1>BENKADDOUR (M.)</s1>
</fA11>
<fA14 i1="01"><s1>Laboratoire des Milieux Désordonnés et Hétérogènes, UMR7603, Université Pierre et Marie Curie, 4 place Jussieu</s1>
<s2>75252 Paris</s2>
<s3>FRA</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>Departamento Quimica Fundamental e Industrial, Universidade A Coruna</s1>
<s2>15071 A Coruna</s2>
<s3>ESP</s3>
<sZ>6 aut.</sZ>
</fA14>
<fA14 i1="03"><s1>Laboratoire d'Analyse et Caractérisation des Matériaux, Université Mohamed 1er, Faculté des Sciences</s1>
<s2>Oujda</s2>
<s3>MAR</s3>
<sZ>7 aut.</sZ>
<sZ>8 aut.</sZ>
</fA14>
<fA20><s1>145-155</s1>
</fA20>
<fA21><s1>2000</s1>
</fA21>
<fA23 i1="01"><s0>ENG</s0>
</fA23>
<fA43 i1="01"><s1>INIST</s1>
<s2>12899B</s2>
<s5>354000088714780110</s5>
</fA43>
<fA44><s0>0000</s0>
<s1>© 2000 INIST-CNRS. All rights reserved.</s1>
</fA44>
<fA45><s0>40 ref.</s0>
</fA45>
<fA47 i1="01" i2="1"><s0>00-0300818</s0>
</fA47>
<fA60><s1>P</s1>
</fA60>
<fA61><s0>A</s0>
</fA61>
<fA64 i1="01" i2="1"><s0>Materials science & engineering. B, Solid-state materials for advanced technology</s0>
</fA64>
<fA66 i1="01"><s0>CHE</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>The lithiated nickel-cobalt oxide LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 used as cathode material was grown at low-temperature using different aqueous solution methods. The wet chemistry involved the mixture of metal salts (acetates or nitrates) with various carboxylic acid-based aqueous solutions. Physicochemical and electrochemical properties of LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 products calcined at 400-600°C were extensively investigated. The four methods used involved complexing agents such as either citric, oxalic, aminoacetic (glycine), or succinic acid in aqueous medium which functioned as a fuel, decomposed the metal complexes at low temperature, and yielded the free impurity LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 compounds. Thermal (TG-DTA) analyses and XRD data show that powders grown with a layered structure (R3m space group) have been obtained at temperatures below 400°C by the acidification reaction of the aqueous solutions. The local structure of synthesized products was characterized by Fourier transform infrared (FTIR) spectroscopy. The electrochemical properties of the synthesized products were evaluated in rechargeable Li cells using a non-aqueous organic electrolyte (1 M LiClO<sub>4</sub>
 in propylene carbonate, PC). The LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 positive electrodes fired at 600°C exhibited good cycling behavior.</s0>
</fC01>
<fC02 i1="01" i2="X"><s0>001D05I03E</s0>
</fC02>
<fC03 i1="01" i2="X" l="FRE"><s0>Batterie</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="ENG"><s0>Battery</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="SPA"><s0>Batería</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="X" l="FRE"><s0>Lithium Ion</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="ENG"><s0>Lithium Ions</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="SPA"><s0>Litio Ión</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="X" l="FRE"><s0>Matériau électrode</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG"><s0>Electrode material</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA"><s0>Material electrodo</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE"><s0>Lithium Oxyde</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG"><s0>Lithium Oxides</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA"><s0>Litio Óxido</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE"><s0>Nickel Oxyde</s0>
<s2>NC</s2>
<s2>FX</s2>
<s2>NA</s2>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="ENG"><s0>Nickel Oxides</s0>
<s2>NC</s2>
<s2>FX</s2>
<s2>NA</s2>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="SPA"><s0>Niquel Óxido</s0>
<s2>NC</s2>
<s2>FX</s2>
<s2>NA</s2>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Cobalt Oxyde</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Cobalt Oxides</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Cobalto Óxido</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE"><s0>Structure lamellaire</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG"><s0>Lamellar structure</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA"><s0>Estructura lamelar</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Fabrication électrode</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG"><s0>Electrode production</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Fabricación electrodo</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE"><s0>Solution aqueuse</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Aqueous solution</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Solución acuosa</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Acide carboxylique</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Carboxylic acid</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Acido carboxílico</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Séquestrant</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Complexing agent</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Secuestrante</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Analyse thermique</s0>
<s5>14</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Thermal analysis</s0>
<s5>14</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Análisis térmico</s0>
<s5>14</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Analyse thermique différentielle</s0>
<s5>15</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Differential thermal analysis</s0>
<s5>15</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Análisis térmico diferencial</s0>
<s5>15</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>Thermogravimétrie</s0>
<s5>16</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>Thermogravimetry</s0>
<s5>16</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Termogravimetría</s0>
<s5>16</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Structure surface</s0>
<s5>19</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG"><s0>Surface structure</s0>
<s5>19</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA"><s0>Estructura superficie</s0>
<s5>19</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>Morphologie</s0>
<s5>20</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG"><s0>Morphology</s0>
<s5>20</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA"><s0>Morfología</s0>
<s5>20</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Diffraction RX</s0>
<s5>21</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG"><s0>X ray diffraction</s0>
<s5>21</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA"><s0>Difracción RX</s0>
<s5>21</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Spectrométrie IR</s0>
<s5>23</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Infrared spectrometry</s0>
<s5>23</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Espectrometría IR</s0>
<s5>23</s5>
</fC03>
<fC03 i1="19" i2="X" l="FRE"><s0>Transformation Fourier</s0>
<s5>24</s5>
</fC03>
<fC03 i1="19" i2="X" l="ENG"><s0>Fourier transformation</s0>
<s5>24</s5>
</fC03>
<fC03 i1="19" i2="X" l="SPA"><s0>Transformación Fourier</s0>
<s5>24</s5>
</fC03>
<fC03 i1="20" i2="X" l="FRE"><s0>Caractéristique électrique</s0>
<s5>26</s5>
</fC03>
<fC03 i1="20" i2="X" l="ENG"><s0>Electrical characteristic</s0>
<s5>26</s5>
</fC03>
<fC03 i1="20" i2="X" l="SPA"><s0>Característica eléctrica</s0>
<s5>26</s5>
</fC03>
<fC03 i1="21" i2="X" l="FRE"><s0>Cycle charge décharge</s0>
<s5>27</s5>
</fC03>
<fC03 i1="21" i2="X" l="ENG"><s0>Discharge charge cycle</s0>
<s5>27</s5>
</fC03>
<fC03 i1="21" i2="X" l="SPA"><s0>Ciclo carga descarga</s0>
<s5>27</s5>
</fC03>
<fC03 i1="22" i2="X" l="FRE"><s0>LiNi0,5Co0,5O2</s0>
<s4>INC</s4>
<s5>62</s5>
</fC03>
<fC03 i1="23" i2="X" l="FRE"><s0>Co Li Ni O</s0>
<s4>INC</s4>
<s5>63</s5>
</fC03>
<fN21><s1>206</s1>
</fN21>
</pA>
</standard>
<server><NO>PASCAL 00-0300818 INIST</NO>
<ET>Layered LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 cathode materials grown by soft-chemistry via various solution methods</ET>
<AU>JULIEN (C.); LETRANCHANT (C.); RANGAN (S.); LEMAL (M.); ZIOLKIEWICZ (S.); CASTRO-GARCIA (S.); EL-FARH (L.); BENKADDOUR (M.)</AU>
<AF>Laboratoire des Milieux Désordonnés et Hétérogènes, UMR7603, Université Pierre et Marie Curie, 4 place Jussieu/75252 Paris/France (1 aut., 2 aut., 3 aut., 4 aut., 5 aut.); Departamento Quimica Fundamental e Industrial, Universidade A Coruna/15071 A Coruna/Espagne (6 aut.); Laboratoire d'Analyse et Caractérisation des Matériaux, Université Mohamed 1er, Faculté des Sciences/Oujda/Maroc (7 aut., 8 aut.)</AF>
<DT>Publication en série; Niveau analytique</DT>
<SO>Materials science & engineering. B, Solid-state materials for advanced technology; ISSN 0921-5107; Suisse; Da. 2000; Vol. 76; No. 2; Pp. 145-155; Bibl. 40 ref.</SO>
<LA>Anglais</LA>
<EA>The lithiated nickel-cobalt oxide LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 used as cathode material was grown at low-temperature using different aqueous solution methods. The wet chemistry involved the mixture of metal salts (acetates or nitrates) with various carboxylic acid-based aqueous solutions. Physicochemical and electrochemical properties of LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 products calcined at 400-600°C were extensively investigated. The four methods used involved complexing agents such as either citric, oxalic, aminoacetic (glycine), or succinic acid in aqueous medium which functioned as a fuel, decomposed the metal complexes at low temperature, and yielded the free impurity LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 compounds. Thermal (TG-DTA) analyses and XRD data show that powders grown with a layered structure (R3m space group) have been obtained at temperatures below 400°C by the acidification reaction of the aqueous solutions. The local structure of synthesized products was characterized by Fourier transform infrared (FTIR) spectroscopy. The electrochemical properties of the synthesized products were evaluated in rechargeable Li cells using a non-aqueous organic electrolyte (1 M LiClO<sub>4</sub>
 in propylene carbonate, PC). The LiNi<sub>0.5</sub>
Co<sub>0.5</sub>
O<sub>2</sub>
 positive electrodes fired at 600°C exhibited good cycling behavior.</EA>
<CC>001D05I03E</CC>
<FD>Batterie; Lithium Ion; Matériau électrode; Lithium Oxyde; Nickel Oxyde; Cobalt Oxyde; Structure lamellaire; Fabrication électrode; Solution aqueuse; Acide carboxylique; Séquestrant; Analyse thermique; Analyse thermique différentielle; Thermogravimétrie; Structure surface; Morphologie; Diffraction RX; Spectrométrie IR; Transformation Fourier; Caractéristique électrique; Cycle charge décharge; LiNi0,5Co0,5O2; Co Li Ni O</FD>
<ED>Battery; Lithium Ions; Electrode material; Lithium Oxides; Nickel Oxides; Cobalt Oxides; Lamellar structure; Electrode production; Aqueous solution; Carboxylic acid; Complexing agent; Thermal analysis; Differential thermal analysis; Thermogravimetry; Surface structure; Morphology; X ray diffraction; Infrared spectrometry; Fourier transformation; Electrical characteristic; Discharge charge cycle</ED>
<SD>Batería; Litio Ión; Material electrodo; Litio Óxido; Niquel Óxido; Cobalto Óxido; Estructura lamelar; Fabricación electrodo; Solución acuosa; Acido carboxílico; Secuestrante; Análisis térmico; Análisis térmico diferencial; Termogravimetría; Estructura superficie; Morfología; Difracción RX; Espectrometría IR; Transformación Fourier; Característica eléctrica; Ciclo carga descarga</SD>
<LO>INIST-12899B.354000088714780110</LO>
<ID>00-0300818</ID>
</server>
</inist>
</record>

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   |texte=   Layered LiNi0.5Co0.5O2 cathode materials grown by soft-chemistry via various solution methods
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	Serveur d'exploration sur le cobalt au Maghreb
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Serveur d'exploration sur le cobalt au Maghreb

Layered LiNi0.5Co0.5O2 cathode materials grown by soft-chemistry via various solution methods

Layered LiNi0.5Co0.5O2 cathode materials grown by soft-chemistry via various solution methods

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