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Synthesis and characterisation of nanostructured FeCo alloys

Identifieur interne : 000199 ( PascalFrancis/Corpus ); précédent : 000198; suivant : 000200

Synthesis and characterisation of nanostructured FeCo alloys

Auteurs : H. Moumeni ; S. Alleg ; C. Djebbari ; F. Z. Bentayeb ; J. M. Greneche

Source :

RBID : Pascal:05-0041453

Descripteurs français

English descriptors

Abstract

Nanocrystalline Fe(1-x)Cox (x = 0.12, 0.5, 0.6) mixtures have been prepared by mechanical alloying using a planetary ball mill under several milling conditions. The alloying process between the elemental powders and the microstructure changes of the prepared samples have been investigated using X-ray diffraction (XRD) and 57Fe Mössbauer spectrometry. The XRD patterns refinement on the mechanical alloying products according to the Rietveld method (Maud software) reveals the allotropic transformation of Co from fcc to hcp form and the progressive dissolution of Co into the α-Fe lattice as a function of both Co concentration and milling conditions. The grain size values of the obtained powders reaches a nanometer scale of about 10 nm. Mössbauer results show that the beginning of the solid state reaction between Fe and Co elemental powders depends on the milling conditions. After 24 h of milling, the average hyperfine magnetic fields values of Fe88Co12, Fe50Co50 and Fe40Co60 mixtures are consistent with a disordered and an ordered FeCo solid solution, respectively.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

pA  
A01 01  1    @0 0022-2461
A02 01      @0 JMTSAS
A03   1    @0 J. mater. sci.
A05       @2 39
A06       @2 16-17
A08 01  1  ENG  @1 Synthesis and characterisation of nanostructured FeCo alloys
A11 01  1    @1 MOUMENI (H.)
A11 02  1    @1 ALLEG (S.)
A11 03  1    @1 DJEBBARI (C.)
A11 04  1    @1 BENTAYEB (F. Z.)
A11 05  1    @1 GRENECHE (J. M.)
A14 01      @1 Laboratoire de Magnétisme et de Spectroscopie des Solides LM2S, Département de Physique, Faculté des Sciences, Université de Annaba, B.P. 12 @2 23000 Annaba @3 DZA @Z 1 aut. @Z 2 aut. @Z 3 aut. @Z 4 aut.
A14 02      @1 Laboratoire de Physique de l'Etat Condensé, UMR CNRS 6087, Université du Maine, Faculté des Sciences @2 72085, Le Mans @3 FRA @Z 5 aut.
A20       @1 5441-5443
A21       @1 2004
A23 01      @0 ENG
A43 01      @1 INIST @2 12733 @5 354000120290480880
A44       @0 0000 @1 © 2005 INIST-CNRS. All rights reserved.
A45       @0 10 ref.
A47 01  1    @0 05-0041453
A60       @1 P @2 C
A61       @0 A
A64 01  1    @0 Journal of materials science
A66 01      @0 NLD
C01 01    ENG  @0 Nanocrystalline Fe(1-x)Cox (x = 0.12, 0.5, 0.6) mixtures have been prepared by mechanical alloying using a planetary ball mill under several milling conditions. The alloying process between the elemental powders and the microstructure changes of the prepared samples have been investigated using X-ray diffraction (XRD) and 57Fe Mössbauer spectrometry. The XRD patterns refinement on the mechanical alloying products according to the Rietveld method (Maud software) reveals the allotropic transformation of Co from fcc to hcp form and the progressive dissolution of Co into the α-Fe lattice as a function of both Co concentration and milling conditions. The grain size values of the obtained powders reaches a nanometer scale of about 10 nm. Mössbauer results show that the beginning of the solid state reaction between Fe and Co elemental powders depends on the milling conditions. After 24 h of milling, the average hyperfine magnetic fields values of Fe88Co12, Fe50Co50 and Fe40Co60 mixtures are consistent with a disordered and an ordered FeCo solid solution, respectively.
C02 01  3    @0 001B80A07W
C02 02  3    @0 001B80A20
C02 03  3    @0 001B60A46
C02 04  X    @0 240
C03 01  3  FRE  @0 Etude expérimentale @5 01
C03 01  3  ENG  @0 Experimental study @5 01
C03 02  3  FRE  @0 Fabrication @5 02
C03 02  3  ENG  @0 Fabrication @5 02
C03 03  3  FRE  @0 Alliage binaire @5 03
C03 03  3  ENG  @0 Binary alloys @5 03
C03 04  3  FRE  @0 Alliage base fer @2 NK @5 05
C03 04  3  ENG  @0 Iron base alloys @2 NK @5 05
C03 05  3  FRE  @0 Cobalt alliage @5 06
C03 05  3  ENG  @0 Cobalt alloys @5 06
C03 06  3  FRE  @0 Alliage base cobalt @2 NK @5 07
C03 06  3  ENG  @0 Cobalt base alloys @2 NK @5 07
C03 07  3  FRE  @0 Fer alliage @5 08
C03 07  3  ENG  @0 Iron alloys @5 08
C03 08  3  FRE  @0 Composition chimique @5 09
C03 08  3  ENG  @0 Chemical composition @5 09
C03 09  3  FRE  @0 Alliage mécanique @5 10
C03 09  3  ENG  @0 Mechanical alloying @5 10
C03 10  X  FRE  @0 Nanocristal @5 11
C03 10  X  ENG  @0 Nanocrystal @5 11
C03 10  X  SPA  @0 Nanocristal @5 11
C03 11  3  FRE  @0 Nanostructure @5 12
C03 11  3  ENG  @0 Nanostructures @5 12
C03 12  X  FRE  @0 Poudre métallique @5 13
C03 12  X  ENG  @0 Metal powder @5 13
C03 12  X  GER  @0 Metallpulver @5 13
C03 12  X  SPA  @0 Polvo metálico @5 13
C03 13  X  FRE  @0 Poudre ultrafine @5 14
C03 13  X  ENG  @0 Ultrafine powder @5 14
C03 13  X  SPA  @0 Polvo ultrafino @5 14
C03 14  3  FRE  @0 Concassage @5 15
C03 14  3  ENG  @0 Crushing @5 15
C03 15  X  FRE  @0 Broyeur boulet @5 16
C03 15  X  ENG  @0 Ball mill @5 16
C03 15  X  GER  @0 Kugelmuehle @5 16
C03 15  X  SPA  @0 Molino bolas @5 16
C03 16  X  FRE  @0 Broyeur satellite @5 17
C03 16  X  ENG  @0 Planetary mill @5 17
C03 16  X  SPA  @0 Molino rodillos satelite @5 17
C03 17  3  FRE  @0 Microstructure @5 18
C03 17  3  ENG  @0 Microstructure @5 18
C03 18  3  FRE  @0 Diffraction RX @5 19
C03 18  3  ENG  @0 XRD @5 19
C03 19  3  FRE  @0 Spectrométrie Mössbauer @5 20
C03 19  3  ENG  @0 Moessbauer spectroscopy @5 20
C03 20  3  FRE  @0 Fer 57 @5 21
C03 20  3  ENG  @0 Iron 57 @5 21
C03 21  3  FRE  @0 Transformation phase @5 22
C03 21  3  ENG  @0 Phase transformations @5 22
C03 22  X  FRE  @0 Réaction état solide @5 23
C03 22  X  ENG  @0 Solid state reaction @5 23
C03 22  X  GER  @0 Festkoerperreaktion @5 23
C03 22  X  SPA  @0 Reacción estado sólido @5 23
C03 23  X  FRE  @0 Relation fabrication structure @5 24
C03 23  X  ENG  @0 Fabrication structure relation @5 24
C03 23  X  SPA  @0 Relación fabricación estructura @5 24
C03 24  3  FRE  @0 Alliage Fe87Co13 @2 NK @4 INC @5 32
C03 25  3  FRE  @0 Co Fe @4 INC @5 33
C03 26  3  FRE  @0 Alliage Co51Fe49 @2 NK @4 INC @5 34
C03 27  3  FRE  @0 Alliage Co61Fe39 @2 NK @4 INC @5 35
C03 28  3  FRE  @0 8107W @2 PAC @4 INC @5 92
C03 29  3  FRE  @0 8120E @2 PAC @4 INC @5 93
C03 30  3  FRE  @0 6146 @2 PAC @4 INC @5 94
C03 31  3  FRE  @0 Mécanochimie @4 CD @5 96
C03 31  3  ENG  @0 Mechanochemistry @4 CD @5 96
C07 01  3  FRE  @0 Métal transition alliage @5 04
C07 01  3  ENG  @0 Transition element alloys @5 04
N21       @1 017
N44 01      @1 PSI
N82       @1 PSI
pR  
A30 01  1  ENG  @1 International Conference on Mechanochemistry and Mechanical Alloying (INCOME 2003) @3 Braunschweig DEU @4 2003-09-07

Format Inist (serveur)

NO : PASCAL 05-0041453 INIST
ET : Synthesis and characterisation of nanostructured FeCo alloys
AU : MOUMENI (H.); ALLEG (S.); DJEBBARI (C.); BENTAYEB (F. Z.); GRENECHE (J. M.)
AF : Laboratoire de Magnétisme et de Spectroscopie des Solides LM2S, Département de Physique, Faculté des Sciences, Université de Annaba, B.P. 12/23000 Annaba/Algérie (1 aut., 2 aut., 3 aut., 4 aut.); Laboratoire de Physique de l'Etat Condensé, UMR CNRS 6087, Université du Maine, Faculté des Sciences/72085, Le Mans/France (5 aut.)
DT : Publication en série; Congrès; Niveau analytique
SO : Journal of materials science; ISSN 0022-2461; Coden JMTSAS; Pays-Bas; Da. 2004; Vol. 39; No. 16-17; Pp. 5441-5443; Bibl. 10 ref.
LA : Anglais
EA : Nanocrystalline Fe(1-x)Cox (x = 0.12, 0.5, 0.6) mixtures have been prepared by mechanical alloying using a planetary ball mill under several milling conditions. The alloying process between the elemental powders and the microstructure changes of the prepared samples have been investigated using X-ray diffraction (XRD) and 57Fe Mössbauer spectrometry. The XRD patterns refinement on the mechanical alloying products according to the Rietveld method (Maud software) reveals the allotropic transformation of Co from fcc to hcp form and the progressive dissolution of Co into the α-Fe lattice as a function of both Co concentration and milling conditions. The grain size values of the obtained powders reaches a nanometer scale of about 10 nm. Mössbauer results show that the beginning of the solid state reaction between Fe and Co elemental powders depends on the milling conditions. After 24 h of milling, the average hyperfine magnetic fields values of Fe88Co12, Fe50Co50 and Fe40Co60 mixtures are consistent with a disordered and an ordered FeCo solid solution, respectively.
CC : 001B80A07W; 001B80A20; 001B60A46; 240
FD : Etude expérimentale; Fabrication; Alliage binaire; Alliage base fer; Cobalt alliage; Alliage base cobalt; Fer alliage; Composition chimique; Alliage mécanique; Nanocristal; Nanostructure; Poudre métallique; Poudre ultrafine; Concassage; Broyeur boulet; Broyeur satellite; Microstructure; Diffraction RX; Spectrométrie Mössbauer; Fer 57; Transformation phase; Réaction état solide; Relation fabrication structure; Alliage Fe87Co13; Co Fe; Alliage Co51Fe49; Alliage Co61Fe39; 8107W; 8120E; 6146; Mécanochimie
FG : Métal transition alliage
ED : Experimental study; Fabrication; Binary alloys; Iron base alloys; Cobalt alloys; Cobalt base alloys; Iron alloys; Chemical composition; Mechanical alloying; Nanocrystal; Nanostructures; Metal powder; Ultrafine powder; Crushing; Ball mill; Planetary mill; Microstructure; XRD; Moessbauer spectroscopy; Iron 57; Phase transformations; Solid state reaction; Fabrication structure relation; Mechanochemistry
EG : Transition element alloys
GD : Metallpulver; Kugelmuehle; Festkoerperreaktion
SD : Nanocristal; Polvo metálico; Polvo ultrafino; Molino bolas; Molino rodillos satelite; Reacción estado sólido; Relación fabricación estructura
LO : INIST-12733.354000120290480880
ID : 05-0041453

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Pascal:05-0041453

Le document en format XML

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<term>Crushing</term>
<term>Experimental study</term>
<term>Fabrication</term>
<term>Fabrication structure relation</term>
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<term>Etude expérimentale</term>
<term>Fabrication</term>
<term>Alliage binaire</term>
<term>Alliage base fer</term>
<term>Cobalt alliage</term>
<term>Alliage base cobalt</term>
<term>Fer alliage</term>
<term>Composition chimique</term>
<term>Alliage mécanique</term>
<term>Nanocristal</term>
<term>Nanostructure</term>
<term>Poudre métallique</term>
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<term>Spectrométrie Mössbauer</term>
<term>Fer 57</term>
<term>Transformation phase</term>
<term>Réaction état solide</term>
<term>Relation fabrication structure</term>
<term>Alliage Fe87Co13</term>
<term>Co Fe</term>
<term>Alliage Co51Fe49</term>
<term>Alliage Co61Fe39</term>
<term>8107W</term>
<term>8120E</term>
<term>6146</term>
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<div type="abstract" xml:lang="en">Nanocrystalline Fe
<sub>(1-x)</sub>
Co
<sub>x</sub>
(x = 0.12, 0.5, 0.6) mixtures have been prepared by mechanical alloying using a planetary ball mill under several milling conditions. The alloying process between the elemental powders and the microstructure changes of the prepared samples have been investigated using X-ray diffraction (XRD) and
<sup>57</sup>
Fe Mössbauer spectrometry. The XRD patterns refinement on the mechanical alloying products according to the Rietveld method (Maud software) reveals the allotropic transformation of Co from fcc to hcp form and the progressive dissolution of Co into the α-Fe lattice as a function of both Co concentration and milling conditions. The grain size values of the obtained powders reaches a nanometer scale of about 10 nm. Mössbauer results show that the beginning of the solid state reaction between Fe and Co elemental powders depends on the milling conditions. After 24 h of milling, the average hyperfine magnetic fields values of Fe
<sub>88</sub>
Co
<sub>12</sub>
, Fe
<sub>50</sub>
Co
<sub>50</sub>
and Fe
<sub>40</sub>
Co
<sub>60</sub>
mixtures are consistent with a disordered and an ordered FeCo solid solution, respectively.</div>
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<s3>DZA</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</fA14>
<fA14 i1="02">
<s1>Laboratoire de Physique de l'Etat Condensé, UMR CNRS 6087, Université du Maine, Faculté des Sciences</s1>
<s2>72085, Le Mans</s2>
<s3>FRA</s3>
<sZ>5 aut.</sZ>
</fA14>
<fA20>
<s1>5441-5443</s1>
</fA20>
<fA21>
<s1>2004</s1>
</fA21>
<fA23 i1="01">
<s0>ENG</s0>
</fA23>
<fA43 i1="01">
<s1>INIST</s1>
<s2>12733</s2>
<s5>354000120290480880</s5>
</fA43>
<fA44>
<s0>0000</s0>
<s1>© 2005 INIST-CNRS. All rights reserved.</s1>
</fA44>
<fA45>
<s0>10 ref.</s0>
</fA45>
<fA47 i1="01" i2="1">
<s0>05-0041453</s0>
</fA47>
<fA60>
<s1>P</s1>
<s2>C</s2>
</fA60>
<fA61>
<s0>A</s0>
</fA61>
<fA64 i1="01" i2="1">
<s0>Journal of materials science</s0>
</fA64>
<fA66 i1="01">
<s0>NLD</s0>
</fA66>
<fC01 i1="01" l="ENG">
<s0>Nanocrystalline Fe
<sub>(1-x)</sub>
Co
<sub>x</sub>
(x = 0.12, 0.5, 0.6) mixtures have been prepared by mechanical alloying using a planetary ball mill under several milling conditions. The alloying process between the elemental powders and the microstructure changes of the prepared samples have been investigated using X-ray diffraction (XRD) and
<sup>57</sup>
Fe Mössbauer spectrometry. The XRD patterns refinement on the mechanical alloying products according to the Rietveld method (Maud software) reveals the allotropic transformation of Co from fcc to hcp form and the progressive dissolution of Co into the α-Fe lattice as a function of both Co concentration and milling conditions. The grain size values of the obtained powders reaches a nanometer scale of about 10 nm. Mössbauer results show that the beginning of the solid state reaction between Fe and Co elemental powders depends on the milling conditions. After 24 h of milling, the average hyperfine magnetic fields values of Fe
<sub>88</sub>
Co
<sub>12</sub>
, Fe
<sub>50</sub>
Co
<sub>50</sub>
and Fe
<sub>40</sub>
Co
<sub>60</sub>
mixtures are consistent with a disordered and an ordered FeCo solid solution, respectively.</s0>
</fC01>
<fC02 i1="01" i2="3">
<s0>001B80A07W</s0>
</fC02>
<fC02 i1="02" i2="3">
<s0>001B80A20</s0>
</fC02>
<fC02 i1="03" i2="3">
<s0>001B60A46</s0>
</fC02>
<fC02 i1="04" i2="X">
<s0>240</s0>
</fC02>
<fC03 i1="01" i2="3" l="FRE">
<s0>Etude expérimentale</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="3" l="ENG">
<s0>Experimental study</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="3" l="FRE">
<s0>Fabrication</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="3" l="ENG">
<s0>Fabrication</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="3" l="FRE">
<s0>Alliage binaire</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG">
<s0>Binary alloys</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE">
<s0>Alliage base fer</s0>
<s2>NK</s2>
<s5>05</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG">
<s0>Iron base alloys</s0>
<s2>NK</s2>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE">
<s0>Cobalt alliage</s0>
<s5>06</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG">
<s0>Cobalt alloys</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="3" l="FRE">
<s0>Alliage base cobalt</s0>
<s2>NK</s2>
<s5>07</s5>
</fC03>
<fC03 i1="06" i2="3" l="ENG">
<s0>Cobalt base alloys</s0>
<s2>NK</s2>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE">
<s0>Fer alliage</s0>
<s5>08</s5>
</fC03>
<fC03 i1="07" i2="3" l="ENG">
<s0>Iron alloys</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE">
<s0>Composition chimique</s0>
<s5>09</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG">
<s0>Chemical composition</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE">
<s0>Alliage mécanique</s0>
<s5>10</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG">
<s0>Mechanical alloying</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE">
<s0>Nanocristal</s0>
<s5>11</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG">
<s0>Nanocrystal</s0>
<s5>11</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA">
<s0>Nanocristal</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE">
<s0>Nanostructure</s0>
<s5>12</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG">
<s0>Nanostructures</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE">
<s0>Poudre métallique</s0>
<s5>13</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG">
<s0>Metal powder</s0>
<s5>13</s5>
</fC03>
<fC03 i1="12" i2="X" l="GER">
<s0>Metallpulver</s0>
<s5>13</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA">
<s0>Polvo metálico</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE">
<s0>Poudre ultrafine</s0>
<s5>14</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG">
<s0>Ultrafine powder</s0>
<s5>14</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA">
<s0>Polvo ultrafino</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE">
<s0>Concassage</s0>
<s5>15</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG">
<s0>Crushing</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE">
<s0>Broyeur boulet</s0>
<s5>16</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG">
<s0>Ball mill</s0>
<s5>16</s5>
</fC03>
<fC03 i1="15" i2="X" l="GER">
<s0>Kugelmuehle</s0>
<s5>16</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA">
<s0>Molino bolas</s0>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE">
<s0>Broyeur satellite</s0>
<s5>17</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG">
<s0>Planetary mill</s0>
<s5>17</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA">
<s0>Molino rodillos satelite</s0>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="3" l="FRE">
<s0>Microstructure</s0>
<s5>18</s5>
</fC03>
<fC03 i1="17" i2="3" l="ENG">
<s0>Microstructure</s0>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="3" l="FRE">
<s0>Diffraction RX</s0>
<s5>19</s5>
</fC03>
<fC03 i1="18" i2="3" l="ENG">
<s0>XRD</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="3" l="FRE">
<s0>Spectrométrie Mössbauer</s0>
<s5>20</s5>
</fC03>
<fC03 i1="19" i2="3" l="ENG">
<s0>Moessbauer spectroscopy</s0>
<s5>20</s5>
</fC03>
<fC03 i1="20" i2="3" l="FRE">
<s0>Fer 57</s0>
<s5>21</s5>
</fC03>
<fC03 i1="20" i2="3" l="ENG">
<s0>Iron 57</s0>
<s5>21</s5>
</fC03>
<fC03 i1="21" i2="3" l="FRE">
<s0>Transformation phase</s0>
<s5>22</s5>
</fC03>
<fC03 i1="21" i2="3" l="ENG">
<s0>Phase transformations</s0>
<s5>22</s5>
</fC03>
<fC03 i1="22" i2="X" l="FRE">
<s0>Réaction état solide</s0>
<s5>23</s5>
</fC03>
<fC03 i1="22" i2="X" l="ENG">
<s0>Solid state reaction</s0>
<s5>23</s5>
</fC03>
<fC03 i1="22" i2="X" l="GER">
<s0>Festkoerperreaktion</s0>
<s5>23</s5>
</fC03>
<fC03 i1="22" i2="X" l="SPA">
<s0>Reacción estado sólido</s0>
<s5>23</s5>
</fC03>
<fC03 i1="23" i2="X" l="FRE">
<s0>Relation fabrication structure</s0>
<s5>24</s5>
</fC03>
<fC03 i1="23" i2="X" l="ENG">
<s0>Fabrication structure relation</s0>
<s5>24</s5>
</fC03>
<fC03 i1="23" i2="X" l="SPA">
<s0>Relación fabricación estructura</s0>
<s5>24</s5>
</fC03>
<fC03 i1="24" i2="3" l="FRE">
<s0>Alliage Fe87Co13</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>32</s5>
</fC03>
<fC03 i1="25" i2="3" l="FRE">
<s0>Co Fe</s0>
<s4>INC</s4>
<s5>33</s5>
</fC03>
<fC03 i1="26" i2="3" l="FRE">
<s0>Alliage Co51Fe49</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>34</s5>
</fC03>
<fC03 i1="27" i2="3" l="FRE">
<s0>Alliage Co61Fe39</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>35</s5>
</fC03>
<fC03 i1="28" i2="3" l="FRE">
<s0>8107W</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>92</s5>
</fC03>
<fC03 i1="29" i2="3" l="FRE">
<s0>8120E</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>93</s5>
</fC03>
<fC03 i1="30" i2="3" l="FRE">
<s0>6146</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>94</s5>
</fC03>
<fC03 i1="31" i2="3" l="FRE">
<s0>Mécanochimie</s0>
<s4>CD</s4>
<s5>96</s5>
</fC03>
<fC03 i1="31" i2="3" l="ENG">
<s0>Mechanochemistry</s0>
<s4>CD</s4>
<s5>96</s5>
</fC03>
<fC07 i1="01" i2="3" l="FRE">
<s0>Métal transition alliage</s0>
<s5>04</s5>
</fC07>
<fC07 i1="01" i2="3" l="ENG">
<s0>Transition element alloys</s0>
<s5>04</s5>
</fC07>
<fN21>
<s1>017</s1>
</fN21>
<fN44 i1="01">
<s1>PSI</s1>
</fN44>
<fN82>
<s1>PSI</s1>
</fN82>
</pA>
<pR>
<fA30 i1="01" i2="1" l="ENG">
<s1>International Conference on Mechanochemistry and Mechanical Alloying (INCOME 2003)</s1>
<s3>Braunschweig DEU</s3>
<s4>2003-09-07</s4>
</fA30>
</pR>
</standard>
<server>
<NO>PASCAL 05-0041453 INIST</NO>
<ET>Synthesis and characterisation of nanostructured FeCo alloys</ET>
<AU>MOUMENI (H.); ALLEG (S.); DJEBBARI (C.); BENTAYEB (F. Z.); GRENECHE (J. M.)</AU>
<AF>Laboratoire de Magnétisme et de Spectroscopie des Solides LM2S, Département de Physique, Faculté des Sciences, Université de Annaba, B.P. 12/23000 Annaba/Algérie (1 aut., 2 aut., 3 aut., 4 aut.); Laboratoire de Physique de l'Etat Condensé, UMR CNRS 6087, Université du Maine, Faculté des Sciences/72085, Le Mans/France (5 aut.)</AF>
<DT>Publication en série; Congrès; Niveau analytique</DT>
<SO>Journal of materials science; ISSN 0022-2461; Coden JMTSAS; Pays-Bas; Da. 2004; Vol. 39; No. 16-17; Pp. 5441-5443; Bibl. 10 ref.</SO>
<LA>Anglais</LA>
<EA>Nanocrystalline Fe
<sub>(1-x)</sub>
Co
<sub>x</sub>
(x = 0.12, 0.5, 0.6) mixtures have been prepared by mechanical alloying using a planetary ball mill under several milling conditions. The alloying process between the elemental powders and the microstructure changes of the prepared samples have been investigated using X-ray diffraction (XRD) and
<sup>57</sup>
Fe Mössbauer spectrometry. The XRD patterns refinement on the mechanical alloying products according to the Rietveld method (Maud software) reveals the allotropic transformation of Co from fcc to hcp form and the progressive dissolution of Co into the α-Fe lattice as a function of both Co concentration and milling conditions. The grain size values of the obtained powders reaches a nanometer scale of about 10 nm. Mössbauer results show that the beginning of the solid state reaction between Fe and Co elemental powders depends on the milling conditions. After 24 h of milling, the average hyperfine magnetic fields values of Fe
<sub>88</sub>
Co
<sub>12</sub>
, Fe
<sub>50</sub>
Co
<sub>50</sub>
and Fe
<sub>40</sub>
Co
<sub>60</sub>
mixtures are consistent with a disordered and an ordered FeCo solid solution, respectively.</EA>
<CC>001B80A07W; 001B80A20; 001B60A46; 240</CC>
<FD>Etude expérimentale; Fabrication; Alliage binaire; Alliage base fer; Cobalt alliage; Alliage base cobalt; Fer alliage; Composition chimique; Alliage mécanique; Nanocristal; Nanostructure; Poudre métallique; Poudre ultrafine; Concassage; Broyeur boulet; Broyeur satellite; Microstructure; Diffraction RX; Spectrométrie Mössbauer; Fer 57; Transformation phase; Réaction état solide; Relation fabrication structure; Alliage Fe87Co13; Co Fe; Alliage Co51Fe49; Alliage Co61Fe39; 8107W; 8120E; 6146; Mécanochimie</FD>
<FG>Métal transition alliage</FG>
<ED>Experimental study; Fabrication; Binary alloys; Iron base alloys; Cobalt alloys; Cobalt base alloys; Iron alloys; Chemical composition; Mechanical alloying; Nanocrystal; Nanostructures; Metal powder; Ultrafine powder; Crushing; Ball mill; Planetary mill; Microstructure; XRD; Moessbauer spectroscopy; Iron 57; Phase transformations; Solid state reaction; Fabrication structure relation; Mechanochemistry</ED>
<EG>Transition element alloys</EG>
<GD>Metallpulver; Kugelmuehle; Festkoerperreaktion</GD>
<SD>Nanocristal; Polvo metálico; Polvo ultrafino; Molino bolas; Molino rodillos satelite; Reacción estado sólido; Relación fabricación estructura</SD>
<LO>INIST-12733.354000120290480880</LO>
<ID>05-0041453</ID>
</server>
</inist>
</record>

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