Electrochemical study of LaNi3.55Mn0.4Al0.3Fe0.75 as negative electrode in alkaline secondary batteries
Identifieur interne : 000053 ( PascalFrancis/Checkpoint ); précédent : 000052; suivant : 000054Electrochemical study of LaNi3.55Mn0.4Al0.3Fe0.75 as negative electrode in alkaline secondary batteries
Auteurs : S. Boussami [Tunisie] ; C. Khaldi [Tunisie] ; Jilani Lamloumi [Tunisie] ; H. Mathlouthi [Tunisie] ; H. Takenouti [France]Source :
- Electrochimica acta [ 0013-4686 ] ; 2012.
Descripteurs français
- Pascal (Inist)
- Electrode poreuse, Accumulateur alcalin, Stockage hydrogène, Diffusion, Spectrométrie impédance électrochimique, Cyclage, Alliage base nickel, Alliage n éléments, Lanthane alliage, Manganèse alliage, Aluminium alliage, Fer alliage, Microscopie électronique balayage, Dimension pore, Accumulateur électrochimique, Phénomène transport, Caractéristique électrique, Structure surface, Morphologie, Porosité.
English descriptors
- KwdEn :
- Alkaline storage battery, Aluminium alloy, Cycling, Diffusion, Electrical characteristic, Electrochemical impedance spectroscopy, Hydrogen storage, Iron alloy, Lanthanum alloy, Manganèse alloy, Morphology, Multi-element alloys, Nickel base alloys, Pore size, Porosity, Porous electrode, Scanning electron microscopy, Secondary cell, Surface structure, Transport process.
Abstract
Cobalt-free AB5-type hydrogen storage alloys have been examined for the purpose of lowering metal hydride raw material costs. For this purpose, the electrochemical behaviour of cobalt-free LaNi3.55Mn0.4Ai0.3Fe0.75 alloy was investigated using chronopotentiometry and electrochemical impedance spectroscopy. It was shown that the discharge capacity decreases by 50% after fifty cycles. To investigate the capacity decrease, the impedance measurements were conducted during charging at different stages of life cycle. The experimental impedance spectroscopy reveals that the metal hydride electrode exhibits a porous behaviour. The results were then analyzed on the basis of equivalent circuit model involving the porous electrode behaviour according to de Levie's model, i.e. equivalent cylindrical pores connected in parallel. The pore texture of electrode material was then estimated namely by the pore number, mean values of cylinder radius and effective length. The loss of discharge capacity is due to that of the reactivity of the electrode material and not the collapsing of pore texture.
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Boussami</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>LMMP, ESSTT, 5 Avenue Taha Hussein</s1><s2>1008 Tunis</s2><s3>TUN</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>Tunisie</country><placeName><settlement type="city">Tunis</settlement><region nuts="2">Gouvernorat de Tunis</region></placeName></affiliation></author><author><name sortKey="Khaldi, C" sort="Khaldi, C" uniqKey="Khaldi C" first="C." last="Khaldi">C. Khaldi</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>LMMP, ESSTT, 5 Avenue Taha Hussein</s1><s2>1008 Tunis</s2><s3>TUN</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>Tunisie</country><placeName><settlement type="city">Tunis</settlement><region nuts="2">Gouvernorat de Tunis</region></placeName></affiliation></author><author><name sortKey="Lamloumi, J" sort="Lamloumi, J" uniqKey="Lamloumi J" first="J." last="Lamloumi">Jilani Lamloumi</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>LMMP, ESSTT, 5 Avenue Taha Hussein</s1><s2>1008 Tunis</s2><s3>TUN</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>Tunisie</country><placeName><settlement type="city">Tunis</settlement><region nuts="2">Gouvernorat de Tunis</region></placeName><placeName><settlement type="city">Tunis</settlement><region type="region" nuts="2">Gouvernorat de Tunis</region></placeName><orgName type="university" n="3">Université de Tunis</orgName></affiliation></author><author><name sortKey="Mathlouthi, H" sort="Mathlouthi, H" uniqKey="Mathlouthi H" first="H." last="Mathlouthi">H. Mathlouthi</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>LMMP, ESSTT, 5 Avenue Taha Hussein</s1><s2>1008 Tunis</s2><s3>TUN</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></inist:fA14><country>Tunisie</country><placeName><settlement type="city">Tunis</settlement><region nuts="2">Gouvernorat de Tunis</region></placeName></affiliation></author><author><name sortKey="Takenouti, H" sort="Takenouti, H" uniqKey="Takenouti H" first="H." last="Takenouti">H. Takenouti</name><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>LISE, CNRS, UPMC Univ Paris06, Case 133, 4 Place Jussieu</s1><s2>75252 Paris</s2><s3>FRA</s3><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author></analytic><series><title level="j" type="main">Electrochimica acta</title><title level="j" type="abbreviated">Electrochim. acta</title><idno type="ISSN">0013-4686</idno><imprint><date when="2012">2012</date></imprint></series></biblStruct></sourceDesc><seriesStmt><title level="j" type="main">Electrochimica acta</title><title level="j" type="abbreviated">Electrochim. acta</title><idno type="ISSN">0013-4686</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Alkaline storage battery</term><term>Aluminium alloy</term><term>Cycling</term><term>Diffusion</term><term>Electrical characteristic</term><term>Electrochemical impedance spectroscopy</term><term>Hydrogen storage</term><term>Iron alloy</term><term>Lanthanum alloy</term><term>Manganèse alloy</term><term>Morphology</term><term>Multi-element alloys</term><term>Nickel base alloys</term><term>Pore size</term><term>Porosity</term><term>Porous electrode</term><term>Scanning electron microscopy</term><term>Secondary cell</term><term>Surface structure</term><term>Transport process</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Electrode poreuse</term><term>Accumulateur alcalin</term><term>Stockage hydrogène</term><term>Diffusion</term><term>Spectrométrie impédance électrochimique</term><term>Cyclage</term><term>Alliage base nickel</term><term>Alliage n éléments</term><term>Lanthane alliage</term><term>Manganèse alliage</term><term>Aluminium alliage</term><term>Fer alliage</term><term>Microscopie électronique balayage</term><term>Dimension pore</term><term>Accumulateur électrochimique</term><term>Phénomène transport</term><term>Caractéristique électrique</term><term>Structure surface</term><term>Morphologie</term><term>Porosité</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Cobalt-free AB5-type hydrogen storage alloys have been examined for the purpose of lowering metal hydride raw material costs. For this purpose, the electrochemical behaviour of cobalt-free LaNi<sub>3.55</sub>Mn<sub>0.4</sub>Ai<sub>0.3</sub>Fe<sub>0.75</sub> alloy was investigated using chronopotentiometry and electrochemical impedance spectroscopy. It was shown that the discharge capacity decreases by 50% after fifty cycles. To investigate the capacity decrease, the impedance measurements were conducted during charging at different stages of life cycle. The experimental impedance spectroscopy reveals that the metal hydride electrode exhibits a porous behaviour. The results were then analyzed on the basis of equivalent circuit model involving the porous electrode behaviour according to de Levie's model, i.e. equivalent cylindrical pores connected in parallel. The pore texture of electrode material was then estimated namely by the pore number, mean values of cylinder radius and effective length. The loss of discharge capacity is due to that of the reactivity of the electrode material and not the collapsing of pore texture.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0013-4686</s0></fA01><fA02 i1="01"><s0>ELCAAV</s0></fA02><fA03 i2="1"><s0>Electrochim. acta</s0></fA03><fA05><s2>69</s2></fA05><fA08 i1="01" i2="1" l="ENG"><s1>Electrochemical study of LaNi<sub>3.55</sub>Mn<sub>0.4</sub>Al<sub>0.3</sub>Fe<sub>0.75</sub> as negative electrode in alkaline secondary batteries</s1></fA08><fA11 i1="01" i2="1"><s1>BOUSSAMI (S.)</s1></fA11><fA11 i1="02" i2="1"><s1>KHALDI (C.)</s1></fA11><fA11 i1="03" i2="1"><s1>LAMLOUMI (J.)</s1></fA11><fA11 i1="04" i2="1"><s1>MATHLOUTHI (H.)</s1></fA11><fA11 i1="05" i2="1"><s1>TAKENOUTI (H.)</s1></fA11><fA14 i1="01"><s1>LMMP, ESSTT, 5 Avenue Taha Hussein</s1><s2>1008 Tunis</s2><s3>TUN</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ></fA14><fA14 i1="02"><s1>LISE, CNRS, UPMC Univ Paris06, Case 133, 4 Place Jussieu</s1><s2>75252 Paris</s2><s3>FRA</s3><sZ>5 aut.</sZ></fA14><fA20><s1>203-208</s1></fA20><fA21><s1>2012</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>1516</s2><s5>354000509856970290</s5></fA43><fA44><s0>0000</s0><s1>© 2012 INIST-CNRS. All rights reserved.</s1></fA44><fA45><s0>35 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>12-0406949</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>Electrochimica acta</s0></fA64><fA66 i1="01"><s0>GBR</s0></fA66><fC01 i1="01" l="ENG"><s0>Cobalt-free AB5-type hydrogen storage alloys have been examined for the purpose of lowering metal hydride raw material costs. For this purpose, the electrochemical behaviour of cobalt-free LaNi<sub>3.55</sub>Mn<sub>0.4</sub>Ai<sub>0.3</sub>Fe<sub>0.75</sub> alloy was investigated using chronopotentiometry and electrochemical impedance spectroscopy. It was shown that the discharge capacity decreases by 50% after fifty cycles. To investigate the capacity decrease, the impedance measurements were conducted during charging at different stages of life cycle. The experimental impedance spectroscopy reveals that the metal hydride electrode exhibits a porous behaviour. The results were then analyzed on the basis of equivalent circuit model involving the porous electrode behaviour according to de Levie's model, i.e. equivalent cylindrical pores connected in parallel. The pore texture of electrode material was then estimated namely by the pore number, mean values of cylinder radius and effective length. The loss of discharge capacity is due to that of the reactivity of the electrode material and not the collapsing of pore texture.</s0></fC01><fC02 i1="01" i2="X"><s0>001D05I03E</s0></fC02><fC03 i1="01" i2="X" l="FRE"><s0>Electrode poreuse</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="ENG"><s0>Porous electrode</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="SPA"><s0>Electrodo poroso</s0><s5>01</s5></fC03><fC03 i1="02" i2="X" l="FRE"><s0>Accumulateur alcalin</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="ENG"><s0>Alkaline storage battery</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="SPA"><s0>Acumulador alcalino</s0><s5>02</s5></fC03><fC03 i1="03" i2="3" l="FRE"><s0>Stockage hydrogène</s0><s5>03</s5></fC03><fC03 i1="03" i2="3" l="ENG"><s0>Hydrogen storage</s0><s5>03</s5></fC03><fC03 i1="04" i2="X" l="FRE"><s0>Diffusion</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="ENG"><s0>Diffusion</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="SPA"><s0>Difusión</s0><s5>04</s5></fC03><fC03 i1="05" i2="3" l="FRE"><s0>Spectrométrie impédance électrochimique</s0><s5>05</s5></fC03><fC03 i1="05" i2="3" l="ENG"><s0>Electrochemical impedance spectroscopy</s0><s5>05</s5></fC03><fC03 i1="06" i2="X" l="FRE"><s0>Cyclage</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="ENG"><s0>Cycling</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="SPA"><s0>Ciclaje</s0><s5>06</s5></fC03><fC03 i1="07" i2="3" l="FRE"><s0>Alliage base nickel</s0><s2>NK</s2><s5>07</s5></fC03><fC03 i1="07" i2="3" l="ENG"><s0>Nickel base alloys</s0><s2>NK</s2><s5>07</s5></fC03><fC03 i1="08" i2="3" l="FRE"><s0>Alliage n éléments</s0><s5>08</s5></fC03><fC03 i1="08" i2="3" l="ENG"><s0>Multi-element alloys</s0><s5>08</s5></fC03><fC03 i1="09" i2="X" l="FRE"><s0>Lanthane alliage</s0><s5>09</s5></fC03><fC03 i1="09" i2="X" l="ENG"><s0>Lanthanum alloy</s0><s5>09</s5></fC03><fC03 i1="09" i2="X" l="SPA"><s0>Lantano aleación</s0><s5>09</s5></fC03><fC03 i1="10" i2="X" l="FRE"><s0>Manganèse alliage</s0><s5>10</s5></fC03><fC03 i1="10" i2="X" l="ENG"><s0>Manganèse alloy</s0><s5>10</s5></fC03><fC03 i1="10" i2="X" l="SPA"><s0>Manganeso aleación</s0><s5>10</s5></fC03><fC03 i1="11" i2="X" l="FRE"><s0>Aluminium alliage</s0><s5>11</s5></fC03><fC03 i1="11" i2="X" l="ENG"><s0>Aluminium alloy</s0><s5>11</s5></fC03><fC03 i1="11" i2="X" l="SPA"><s0>Aluminio aleación</s0><s5>11</s5></fC03><fC03 i1="12" i2="X" l="FRE"><s0>Fer alliage</s0><s5>12</s5></fC03><fC03 i1="12" i2="X" l="ENG"><s0>Iron alloy</s0><s5>12</s5></fC03><fC03 i1="12" i2="X" l="SPA"><s0>Hierro aleación</s0><s5>12</s5></fC03><fC03 i1="13" i2="X" l="FRE"><s0>Microscopie électronique balayage</s0><s5>13</s5></fC03><fC03 i1="13" i2="X" l="ENG"><s0>Scanning electron microscopy</s0><s5>13</s5></fC03><fC03 i1="13" i2="X" l="SPA"><s0>Microscopía electrónica barrido</s0><s5>13</s5></fC03><fC03 i1="14" i2="X" l="FRE"><s0>Dimension pore</s0><s5>14</s5></fC03><fC03 i1="14" i2="X" l="ENG"><s0>Pore size</s0><s5>14</s5></fC03><fC03 i1="14" i2="X" l="SPA"><s0>Dimensión poro</s0><s5>14</s5></fC03><fC03 i1="15" i2="X" l="FRE"><s0>Accumulateur électrochimique</s0><s5>32</s5></fC03><fC03 i1="15" i2="X" l="ENG"><s0>Secondary cell</s0><s5>32</s5></fC03><fC03 i1="15" i2="X" l="SPA"><s0>Acumulador electroquímico</s0><s5>32</s5></fC03><fC03 i1="16" i2="X" l="FRE"><s0>Phénomène transport</s0><s5>33</s5></fC03><fC03 i1="16" i2="X" l="ENG"><s0>Transport process</s0><s5>33</s5></fC03><fC03 i1="16" i2="X" l="SPA"><s0>Fenómeno transporte</s0><s5>33</s5></fC03><fC03 i1="17" i2="X" l="FRE"><s0>Caractéristique électrique</s0><s5>34</s5></fC03><fC03 i1="17" i2="X" l="ENG"><s0>Electrical characteristic</s0><s5>34</s5></fC03><fC03 i1="17" i2="X" l="SPA"><s0>Característica eléctrica</s0><s5>34</s5></fC03><fC03 i1="18" i2="X" l="FRE"><s0>Structure surface</s0><s5>35</s5></fC03><fC03 i1="18" i2="X" l="ENG"><s0>Surface structure</s0><s5>35</s5></fC03><fC03 i1="18" i2="X" l="SPA"><s0>Estructura superficie</s0><s5>35</s5></fC03><fC03 i1="19" i2="X" l="FRE"><s0>Morphologie</s0><s5>36</s5></fC03><fC03 i1="19" i2="X" l="ENG"><s0>Morphology</s0><s5>36</s5></fC03><fC03 i1="19" i2="X" l="SPA"><s0>Morfología</s0><s5>36</s5></fC03><fC03 i1="20" i2="X" l="FRE"><s0>Porosité</s0><s5>37</s5></fC03><fC03 i1="20" i2="X" l="ENG"><s0>Porosity</s0><s5>37</s5></fC03><fC03 i1="20" i2="X" l="SPA"><s0>Porosidad</s0><s5>37</s5></fC03><fN21><s1>317</s1></fN21></pA></standard></inist><affiliations><list><country><li>France</li><li>Tunisie</li></country><region><li>Gouvernorat de Tunis</li><li>Île-de-France</li></region><settlement><li>Paris</li><li>Tunis</li></settlement><orgName><li>Université de Tunis</li></orgName></list><tree><country name="Tunisie"><region name="Gouvernorat de Tunis"><name sortKey="Boussami, S" sort="Boussami, S" uniqKey="Boussami S" first="S." last="Boussami">S. Boussami</name></region><name sortKey="Khaldi, C" sort="Khaldi, C" uniqKey="Khaldi C" first="C." last="Khaldi">C. Khaldi</name><name sortKey="Lamloumi, J" sort="Lamloumi, J" uniqKey="Lamloumi J" first="J." last="Lamloumi">Jilani Lamloumi</name><name sortKey="Mathlouthi, H" sort="Mathlouthi, H" uniqKey="Mathlouthi H" first="H." last="Mathlouthi">H. Mathlouthi</name></country><country name="France"><region name="Île-de-France"><name sortKey="Takenouti, H" sort="Takenouti, H" uniqKey="Takenouti H" first="H." last="Takenouti">H. Takenouti</name></region></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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