CobaltMaghrebV1, Ncbi, Merge, bibRecord, 000391

Structure cristalline de la triple molybdate Ag0.90Al1.06Co2.94(MoO4)5

Identifieur interne : 000391 ( Ncbi/Merge ); précédent : 000390; suivant : 000392

Structure cristalline de la triple molybdate Ag0.90Al1.06Co2.94(MoO4)5

Auteurs : Rawia Nasri [Tunisie] ; Saïda Fatma Chérif [Tunisie] ; Mohamed Faouzi Zid [Tunisie]

Source :

Acta Crystallographica Section E: Crystallographic Communications [ 2056-9890 ] ; 2015.

RBID : PMC:4438844

Abstract

A new triple hexakis(molybdate), Ag_0.90Al_1.06Co_2.94(MoO₄)₅, was synthesized using a solid-state reaction at 845 K. Dimers M₂O₁₀ (M = Co/Al) and trimers M₃O₁₄ link to the MoO₄ tetrahedra by sharing corners and form a three-dimensional framework with the interstitial sites occupied by Ag⁺ cations.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC4438844

DOI: 10.1107/S2056989015005290
PubMed: 26029398
PubMed Central: 4438844

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Links to Exploration step

PMC:4438844

Le document en format XML

<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Structure cristalline de la triple molybdate Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
</title>
<author><name sortKey="Nasri, Rawia" sort="Nasri, Rawia" uniqKey="Nasri R" first="Rawia" last="Nasri">Rawia Nasri</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis,<country>Tunisia</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Cherif, Saida Fatma" sort="Cherif, Saida Fatma" uniqKey="Cherif S" first="Saïda Fatma" last="Chérif">Saïda Fatma Chérif</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis,<country>Tunisia</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Zid, Mohamed Faouzi" sort="Zid, Mohamed Faouzi" uniqKey="Zid M" first="Mohamed Faouzi" last="Zid">Mohamed Faouzi Zid</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis,<country>Tunisia</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
</titleStmt>
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<idno type="pmid">26029398</idno>
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<idno type="doi">10.1107/S2056989015005290</idno>
<date when="2015">2015</date>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Structure cristalline de la triple molybdate Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
</title>
<author><name sortKey="Nasri, Rawia" sort="Nasri, Rawia" uniqKey="Nasri R" first="Rawia" last="Nasri">Rawia Nasri</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis,<country>Tunisia</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Cherif, Saida Fatma" sort="Cherif, Saida Fatma" uniqKey="Cherif S" first="Saïda Fatma" last="Chérif">Saïda Fatma Chérif</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis,<country>Tunisia</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Zid, Mohamed Faouzi" sort="Zid, Mohamed Faouzi" uniqKey="Zid M" first="Mohamed Faouzi" last="Zid">Mohamed Faouzi Zid</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis,<country>Tunisia</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
</analytic>
<series><title level="j">Acta Crystallographica Section E: Crystallographic Communications</title>
<idno type="eISSN">2056-9890</idno>
<imprint><date when="2015">2015</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
</fileDesc>
<profileDesc><textClass></textClass>
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<front><div type="abstract" xml:lang="en"><p>A new triple hexakis(molybdate), Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
, was synthesized using a solid-state reaction at 845 K. Dimers <italic>M</italic>
<sub>2</sub>
O<sub>10</sub>
 (<italic>M</italic>
 = Co/Al) and trimers <italic>M</italic>
<sub>3</sub>
O<sub>14</sub>
 link to the MoO<sub>4</sub>
 tetrahedra by sharing corners and form a three-dimensional framework with the interstitial sites occupied by Ag<sup>+</sup>
 cations.</p>
</div>
</front>
<back><div1 type="bibliography"><listBibl><biblStruct></biblStruct>
<biblStruct></biblStruct>
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<biblStruct></biblStruct>
<biblStruct></biblStruct>
</listBibl>
</div1>
</back>
</TEI>
<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
  <front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr E Crystallogr Commun</journal-id>
<journal-id journal-id-type="iso-abbrev">Acta Crystallogr E Crystallogr Commun</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Crystallographic Communications</journal-title>
</journal-title-group>
<issn pub-type="epub">2056-9890</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">26029398</article-id>
<article-id pub-id-type="pmc">4438844</article-id>
<article-id pub-id-type="publisher-id">vn2089</article-id>
<article-id pub-id-type="doi">10.1107/S2056989015005290</article-id>
<article-id pub-id-type="coden">ACSECI</article-id>
<article-id pub-id-type="pii">S2056989015005290</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Research Communications</subject>
</subj-group>
</article-categories>
<title-group><article-title>Structure cristalline de la triple molybdate Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
</article-title>
<alt-title><italic>Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Nasri</surname>
<given-names>Rawia</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Chérif</surname>
<given-names>Saïda Fatma</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Zid</surname>
<given-names>Mohamed Faouzi</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<aff id="a"><label>a</label>
Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis,<country>Tunisia</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>c.fatouma@yahoo.fr</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>4</month>
<year>2015</year>
</pub-date>
<pub-date pub-type="epub"><day>21</day>
<month>3</month>
<year>2015</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>21</day>
<month>3</month>
<year>2015</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the 
 							. </pmc-comment>
      <volume>71</volume>
<issue>Pt 4</issue>
<issue-id pub-id-type="publisher-id">e150400</issue-id>
<fpage>388</fpage>
<lpage>391</lpage>
<history><date date-type="received"><day>23</day>
<month>2</month>
<year>2015</year>
</date>
<date date-type="accepted"><day>14</day>
<month>3</month>
<year>2015</year>
</date>
</history>
<permissions><copyright-statement>© Nasri et al. 2015</copyright-statement>
<copyright-year>2015</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits
unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S2056989015005290">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract abstract-type="toc"><p>A new triple hexakis(molybdate), Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
, was synthesized using a solid-state reaction at 845 K. Dimers <italic>M</italic>
<sub>2</sub>
O<sub>10</sub>
 (<italic>M</italic>
 = Co/Al) and trimers <italic>M</italic>
<sub>3</sub>
O<sub>14</sub>
 link to the MoO<sub>4</sub>
 tetrahedra by sharing corners and form a three-dimensional framework with the interstitial sites occupied by Ag<sup>+</sup>
 cations.</p>
</abstract>
<abstract><p>Silver(I) aluminiun tricobalt(II) pentakis[tetraoxidomolybdate(VI)], Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
, was synthesized using a solid-state reaction at 845 K. The structure can be described as a three-dimensional framework formed from dimeric <italic>M</italic>
<sub>2</sub>
O<sub>10</sub>
 (<italic>M</italic>
 = Co/Al) and trimeric <italic>M</italic>
<sub>3</sub>
O<sub>14</sub>
 units linked to MoO<sub>4</sub>
 tetrahedra by sharing corners, with the cavities occupied by disordered Ag<sup>+</sup>
 cations. It is shown that the Co and Al atoms occupy common positions with different occupancies. The Ag<sup>+</sup>
 cations are located at two different sites with occupancies of 0.486 (1) and 0.408 (1). The title coumpond is isotypic with NaMg<sub>3</sub>
Al(MoO<sub>4</sub>
)<sub>5</sub>
 and NaFe<sub>4</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
. Differences and similarities with other related structures are discussed.</p>
</abstract>
<kwd-group><kwd>triple molybdates</kwd>
<kwd>hexakis(molybdate)</kwd>
<kwd>open-framework structure</kwd>
<kwd>crystal structure</kwd>
</kwd-group>
</article-meta>
</front>
<floats-group><fig id="fig1" position="float"><label>Figure 1</label>
<caption><p>Représentation des polyèdres de coordination de l’unité structurale dans Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
. Les éllipsoïdes ont été définis avec 50% de probabilité. [Code de symétrie: (i) <italic>x</italic>
, <italic>y</italic>
 + 1, <italic>z</italic>
; (ii) <italic>x</italic>
, <italic>y</italic>
 − 1, <italic>z</italic>
; (iii) <italic>x</italic>
 + 1, <italic>y</italic>
, <italic>z</italic>
; (iv) −<italic>x</italic>
 + 1, −<italic>y</italic>
 + 1, −<italic>z</italic>
; (v) −<italic>x</italic>
 + 2, −<italic>y</italic>
 + 1, −<italic>z</italic>
 + 1; (vi) −<italic>x</italic>
 + 1, −<italic>y</italic>
 + 1, −<italic>z</italic>
 + 1; (vii) <italic>x</italic>
 − 1, <italic>y</italic>
, <italic>z;</italic>
 M = Co/Al.]</p>
</caption>
<graphic xlink:href="e-71-00388-fig1"></graphic>
</fig>
<fig id="fig2" position="float"><label>Figure 2</label>
<caption><p>Projection: (<italic>a</italic>
) d’une couche de type <italic>A</italic>
 disposée parallèlement au plan (001), (<italic>b</italic>
) d’une couche de type <italic>D</italic>
 dans le plan (001), (<italic>c</italic>
) d’une couche de type <italic>C</italic>
 dans le plan (001), (<italic>d</italic>
) d’une bicouche dans le plan (001).</p>
</caption>
<graphic xlink:href="e-71-00388-fig2"></graphic>
</fig>
<fig id="fig3" position="float"><label>Figure 3</label>
<caption><p>Projection de la structure de Ag<sub>0.90</sub>
Al<sub>1.06</sub>
Co<sub>2.94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
, selon <italic>a</italic>
.</p>
</caption>
<graphic xlink:href="e-71-00388-fig3"></graphic>
</fig>
<fig id="fig4" position="float"><label>Figure 4</label>
<caption><p>Projection de la structure de: (<italic>a</italic>
) <italic>β</italic>
-K<sub>2</sub>
Co<sub>2</sub>
(MoO<sub>4</sub>
)<sub>3</sub>
, selon <italic>b</italic>
, (<italic>b</italic>
) <italic>α</italic>
-K<sub>2</sub>
Co<sub>2</sub>
(MoO<sub>4</sub>
)<sub>3</sub>
, selon <italic>a</italic>
.</p>
</caption>
<graphic xlink:href="e-71-00388-fig4"></graphic>
</fig>
<table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Dtails exprimentaux</title>
</caption>
<table frame="hsides" rules="groups"><tbody valign="top"><tr><td rowspan="1" colspan="2" align="left" valign="top">Donnes crystallines</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Formule chimique</td>
<td rowspan="1" colspan="1" align="left" valign="top">Ag<sub>0,90</sub>
Al<sub>1,06</sub>
Co<sub>2,94</sub>
(MoO<sub>4</sub>
)<sub>5</sub>
</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>M</italic>
<sub>r</sub>
</td>
<td rowspan="1" colspan="1" align="left" valign="top">1098,64</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Systme cristallin, groupe d’espace</td>
<td rowspan="1" colspan="1" align="left" valign="top">Triclinique, <italic>P</italic>
<inline-formula><inline-graphic xlink:href="e-71-00388-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Temprature (K)</td>
<td rowspan="1" colspan="1" align="left" valign="top">298</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>a</italic>
, <italic>b</italic>
, <italic>c</italic>
 ()</td>
<td rowspan="1" colspan="1" align="left" valign="top">6,8547(8), 6,9410(8), 17,597(2)</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">, , ()</td>
<td rowspan="1" colspan="1" align="left" valign="top">87,958(6), 87,462(6), 78,818(4)</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>V</italic>
 (<sup>3</sup>
)</td>
<td rowspan="1" colspan="1" align="left" valign="top">820,20(16)</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>Z</italic>
</td>
<td rowspan="1" colspan="1" align="left" valign="top">2</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Type de rayonnement</td>
<td rowspan="1" colspan="1" align="left" valign="top">Mo <italic>K</italic>
</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"> (mm<sup>1</sup>
)</td>
<td rowspan="1" colspan="1" align="left" valign="top">7,79</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Taille des cristaux (mm)</td>
<td rowspan="1" colspan="1" align="left" valign="top">0,22 0,16 0,12</td>
</tr>
<tr><td rowspan="1" colspan="2" align="left" valign="top"> </td>
</tr>
<tr><td rowspan="1" colspan="2" align="left" valign="top">Collection de donnes</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Diffractomtre</td>
<td rowspan="1" colspan="1" align="left" valign="top">EnrafNonius CAD-4</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Correction d’absorption</td>
<td rowspan="1" colspan="1" align="left" valign="top"> scan (North <italic>et al.</italic>
, 1968<xref ref-type="bibr" rid="bb18"> ▸</xref>
)</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>T</italic>
<sub>min</sub>
, <italic>T</italic>
<sub>max</sub>
</td>
<td rowspan="1" colspan="1" align="left" valign="top">0,233, 0,407</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Nombre de rflexions mesures, indpendantes et observes [<italic>I</italic>
 > 2(<italic>I</italic>
)]</td>
<td rowspan="1" colspan="1" align="left" valign="top">3912, 3527, 3086</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>R</italic>
<sub>int</sub>
</td>
<td rowspan="1" colspan="1" align="left" valign="top">0,029</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">(sin /)<sub>max</sub>
 (<sup>1</sup>
)</td>
<td rowspan="1" colspan="1" align="left" valign="top">0,638</td>
</tr>
<tr><td rowspan="1" colspan="2" align="left" valign="top"> </td>
</tr>
<tr><td rowspan="1" colspan="2" align="left" valign="top">Affinement</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"><italic>R</italic>
[<italic>F</italic>
<sup>2</sup>
 > 2(<italic>F</italic>
<sup>2</sup>
)], <italic>wR</italic>
(<italic>F</italic>
<sup>2</sup>
), <italic>S</italic>
</td>
<td rowspan="1" colspan="1" align="left" valign="top">0,027, 0,070, 1,09</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Nombre de rflexions</td>
<td rowspan="1" colspan="1" align="left" valign="top">3527</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top">Nombre de paramtres</td>
<td rowspan="1" colspan="1" align="left" valign="top">287</td>
</tr>
<tr><td rowspan="1" colspan="1" align="left" valign="top"><sub>max</sub>
, <sub>min</sub>
 (e <sup>3</sup>
)</td>
<td rowspan="1" colspan="1" align="left" valign="top">1,28, 0,77</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Programmes informatiques: <italic>CAD-4 EXPRESS</italic>
 (Duisenberg, 1992<xref ref-type="bibr" rid="bb4"> ▸</xref>
; Macek Yordanov, 1992<xref ref-type="bibr" rid="bb15"> ▸</xref>
), <italic>XCAD4</italic>
 (Harms Wocadlo, 1995<xref ref-type="bibr" rid="bb9"> ▸</xref>
), <italic>SHELXS97</italic>
 et <italic>SHELXL97</italic>
 (Sheldrick, 2008<xref ref-type="bibr" rid="bb20"> ▸</xref>
), <italic>DIAMOND</italic>
 (Brandenburg Putz, 2001<xref ref-type="bibr" rid="bb1"> ▸</xref>
) et <italic>WinGX</italic>
 (Farrugia, 2012<xref ref-type="bibr" rid="bb7"> ▸</xref>
).</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
<affiliations><list><country><li>Tunisie</li>
</country>
</list>
<tree><country name="Tunisie"><noRegion><name sortKey="Nasri, Rawia" sort="Nasri, Rawia" uniqKey="Nasri R" first="Rawia" last="Nasri">Rawia Nasri</name>
</noRegion>
<name sortKey="Cherif, Saida Fatma" sort="Cherif, Saida Fatma" uniqKey="Cherif S" first="Saïda Fatma" last="Chérif">Saïda Fatma Chérif</name>
<name sortKey="Zid, Mohamed Faouzi" sort="Zid, Mohamed Faouzi" uniqKey="Zid M" first="Mohamed Faouzi" last="Zid">Mohamed Faouzi Zid</name>
</country>
</tree>
</affiliations>
</record>

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	Serveur d'exploration sur le cobalt au Maghreb
	Attention, ce site est en cours de développement ! Attention, site généré par des moyens informatiques à partir de corpus bruts. Les informations ne sont donc pas validées.

Serveur d'exploration sur le cobalt au Maghreb

Structure cristalline de la triple molybdate Ag0.90Al1.06Co2.94(MoO4)5

Structure cristalline de la triple molybdate Ag0.90Al1.06Co2.94(MoO4)5

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Abstract

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