Preparation and characterization of the spinel series Co6+xNi4-xMn8O24 (0≤x≤4)
Identifieur interne : 000E44 ( Main/Merge ); précédent : 000E43; suivant : 000E45Preparation and characterization of the spinel series Co6+xNi4-xMn8O24 (0≤x≤4)
Auteurs : C. Boudaya [Tunisie] ; L. Laroussi [Tunisie] ; E. Dhahri [Tunisie] ; J. C. Joubert [France] ; A. Cheikh-Rouhou [Tunisie]Source :
- Phase transitions : (Print) [ 0141-1594 ] ; 1999.
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- Pascal (Inist)
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- KwdEn :
Abstract
Samples of the spinel series, Co6+xNi4-xMn8O24 (0≤x≤4), prepared by traditional ceramic procedures, are characterized by X-ray diffraction, SEM techniques and magnetization measurements. In the whole concentration range, a single-phase cubic spinels are obtained at a sintering temperature of 1050°C for a period of time of 72 h. SEM analysis showed that the ceramics are well densified and consisted of well individualized grains of a narrow size distribution. Magnetization measurements revealed the existence of a Yafet-Kittel configuration at low temperature and a ferrimagnetic-paramagnetic transition with increasing temperature. The Curie temperature decreased from 250 K for x = 2.5 to 200 K for x = 4.
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Ni<sub>4-x</sub>
Mn<sub>8</sub>
O<sub>24</sub>
(0≤x≤4)</title>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Preparation and characterization of the spinel series Co<sub>6+x</sub>
Ni<sub>4-x</sub>
Mn<sub>8</sub>
O<sub>24</sub>
(0≤x≤4)</title>
<author><name sortKey="Boudaya, C" sort="Boudaya, C" uniqKey="Boudaya C" first="C." last="Boudaya">C. Boudaya</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Laboratoire de Physique des matériaux, Faculté des Sciences de Sfax, BP 763</s1>
<s2>3038 Sfax</s2>
<s3>TUN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>5 aut.</sZ>
</inist:fA14>
<country>Tunisie</country>
<wicri:noRegion>3038 Sfax</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Laroussi, L" sort="Laroussi, L" uniqKey="Laroussi L" first="L." last="Laroussi">L. Laroussi</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Laboratoire de Physique des matériaux, Faculté des Sciences de Sfax, BP 763</s1>
<s2>3038 Sfax</s2>
<s3>TUN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>5 aut.</sZ>
</inist:fA14>
<country>Tunisie</country>
<wicri:noRegion>3038 Sfax</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Dhahri, E" sort="Dhahri, E" uniqKey="Dhahri E" first="E." last="Dhahri">E. Dhahri</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Laboratoire de Physique des matériaux, Faculté des Sciences de Sfax, BP 763</s1>
<s2>3038 Sfax</s2>
<s3>TUN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>5 aut.</sZ>
</inist:fA14>
<country>Tunisie</country>
<wicri:noRegion>3038 Sfax</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Joubert, J C" sort="Joubert, J C" uniqKey="Joubert J" first="J. C." last="Joubert">J. C. Joubert</name>
<affiliation wicri:level="3"><inist:fA14 i1="02"><s1>Laboratoire des Matériaux et de Génie Physique, CNRS UMR 5628, ENSPG, BP 46</s1>
<s2>38402 Saint Martin d'Hères</s2>
<s3>FRA</s3>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>France</country>
<placeName><region type="region" nuts="2">Auvergne-Rhône-Alpes</region>
<region type="old region" nuts="2">Rhône-Alpes</region>
<settlement type="city">Saint Martin d'Hères</settlement>
</placeName>
</affiliation>
</author>
<author><name sortKey="Cheikh Rouhou, A" sort="Cheikh Rouhou, A" uniqKey="Cheikh Rouhou A" first="A." last="Cheikh-Rouhou">A. Cheikh-Rouhou</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Laboratoire de Physique des matériaux, Faculté des Sciences de Sfax, BP 763</s1>
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</analytic>
<series><title level="j" type="main">Phase transitions : (Print)</title>
<title level="j" type="abbreviated">Phase transit. : (Print)</title>
<idno type="ISSN">0141-1594</idno>
<imprint><date when="1999">1999</date>
</imprint>
</series>
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<seriesStmt><title level="j" type="main">Phase transitions : (Print)</title>
<title level="j" type="abbreviated">Phase transit. : (Print)</title>
<idno type="ISSN">0141-1594</idno>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Cobalt oxides</term>
<term>Crystal structure</term>
<term>Curie point</term>
<term>Experimental study</term>
<term>Magnetic transitions</term>
<term>Magnetization</term>
<term>Manganese oxides</term>
<term>Microstructure</term>
<term>Nickel oxides</term>
<term>Preparation</term>
<term>Quantity ratio</term>
<term>Quaternary compounds</term>
<term>SEM</term>
<term>Sintering</term>
<term>Spinels</term>
<term>XRD</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Etude expérimentale</term>
<term>Préparation</term>
<term>Frittage</term>
<term>Microstructure</term>
<term>Structure cristalline</term>
<term>Aimantation</term>
<term>Point Curie</term>
<term>Transition magnétique</term>
<term>Effet concentration</term>
<term>Diffraction RX</term>
<term>SEM</term>
<term>Spinelles</term>
<term>Cobalt oxyde</term>
<term>Nickel oxyde</term>
<term>Manganèse oxyde</term>
<term>Composé quaternaire</term>
<term>Co6+xNi4-xMn8O24</term>
<term>Co Mn Ni O</term>
<term>6166F</term>
<term>7530K</term>
</keywords>
</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">Samples of the spinel series, Co<sub>6+x</sub>
Ni<sub>4-x</sub>
Mn<sub>8</sub>
O<sub>24</sub>
(0≤x≤4), prepared by traditional ceramic procedures, are characterized by X-ray diffraction, SEM techniques and magnetization measurements. In the whole concentration range, a single-phase cubic spinels are obtained at a sintering temperature of 1050°C for a period of time of 72 h. SEM analysis showed that the ceramics are well densified and consisted of well individualized grains of a narrow size distribution. Magnetization measurements revealed the existence of a Yafet-Kittel configuration at low temperature and a ferrimagnetic-paramagnetic transition with increasing temperature. The Curie temperature decreased from 250 K for x = 2.5 to 200 K for x = 4.</div>
</front>
</TEI>
<affiliations><list><country><li>France</li>
<li>Tunisie</li>
</country>
<region><li>Auvergne-Rhône-Alpes</li>
<li>Rhône-Alpes</li>
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<settlement><li>Saint Martin d'Hères</li>
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<tree><country name="Tunisie"><noRegion><name sortKey="Boudaya, C" sort="Boudaya, C" uniqKey="Boudaya C" first="C." last="Boudaya">C. Boudaya</name>
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<name sortKey="Cheikh Rouhou, A" sort="Cheikh Rouhou, A" uniqKey="Cheikh Rouhou A" first="A." last="Cheikh-Rouhou">A. Cheikh-Rouhou</name>
<name sortKey="Dhahri, E" sort="Dhahri, E" uniqKey="Dhahri E" first="E." last="Dhahri">E. Dhahri</name>
<name sortKey="Laroussi, L" sort="Laroussi, L" uniqKey="Laroussi L" first="L." last="Laroussi">L. Laroussi</name>
</country>
<country name="France"><region name="Auvergne-Rhône-Alpes"><name sortKey="Joubert, J C" sort="Joubert, J C" uniqKey="Joubert J" first="J. C." last="Joubert">J. C. Joubert</name>
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