An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions
Identifieur interne : 001D25 ( Istex/Corpus ); précédent : 001D24; suivant : 001D26An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions
Auteurs : Philip Andrews ; Alan Kennedy ; Robert Mulvey ; Colin Raston ; Brett Roberts ; René RowlingsSource :
- Angewandte Chemie [ 0044-8249 ] ; 2000-06-02.
Abstract
Sechs Aren‐Anionen in einem kationischen [K6Mg6N12]6+‐Ring (siehe Bild, Aren=Benzol) weist das erste gemischte makrocyclische Metallamid mit 24 (!) Ringatomen auf. Der Makrocyclus wurde in einer sehr effizienten Synthese erhalten, bei der die Anionen durch selektive Monodeprotonierung entstehen.
Url:
DOI: 10.1002/1521-3757(20000602)112:11<2036::AID-ANGE2036>3.0.CO;2-2
Links to Exploration step
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Ringatomen auf. Der Makrocyclus wurde in einer sehr effizienten Synthese erhalten, bei der die Anionen durch selektive Monodeprotonierung entstehen.</div></front></TEI><istex><corpusName>wiley</corpusName><author><json:item><name>Philip C. Andrews Dr.</name><affiliations><json:string>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</json:string></affiliations></json:item><json:item><name>Alan R. Kennedy Dr.</name><affiliations><json:string>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</json:string></affiliations></json:item><json:item><name>Robert E. Mulvey Prof.</name><affiliations><json:string>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</json:string><json:string>E-mail: r.e.mulvey@strath.ac.uk</json:string></affiliations></json:item><json:item><name>Colin L. Raston Prof.</name><affiliations><json:string>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</json:string></affiliations></json:item><json:item><name>Brett A. Roberts</name><affiliations><json:string>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</json:string></affiliations></json:item><json:item><name>René B. Rowlings Dr.</name><affiliations><json:string>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</json:string></affiliations></json:item></author><subject><json:item><lang><json:string>eng</json:string></lang><value>Alkalimetalle</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Amide</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Erdalkalimetalle</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Makrocyclen</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Templatsynthesen</value></json:item></subject><articleId><json:string>ANGE2036</json:string></articleId><language><json:string>eng</json:string></language><abstract>Sechs Aren‐Anionen in einem kationischen [K6Mg6N12]6+‐Ring (siehe Bild, Aren=Benzol) weist das erste gemischte makrocyclische Metallamid mit 24 (!) Ringatomen auf. 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Chem.</title><idno type="pISSN">0044-8249</idno><idno type="eISSN">1521-3757</idno><idno type="DOI">10.1002/(ISSN)1521-3757</idno><imprint><publisher>WILEY‐VCH Verlag GmbH</publisher><pubPlace>Weinheim</pubPlace><date type="published" when="2000-06-02"></date><biblScope unit="volume">112</biblScope><biblScope unit="issue">11</biblScope><biblScope unit="page" from="2036">2036</biblScope><biblScope unit="page" to="2038">2038</biblScope></imprint></monogr><idno type="istex">422CF70AD6C619A7537E8EC3BA73B57C480C230F</idno><idno type="DOI">10.1002/1521-3757(20000602)112:11<2036::AID-ANGE2036>3.0.CO;2-2</idno><idno type="ArticleID">ANGE2036</idno></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>2000</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="de" style="short"><p>Sechs Aren‐Anionen in einem kationischen [K6Mg6N12]6+‐Ring (siehe Bild, Aren=Benzol) weist das erste gemischte makrocyclische Metallamid mit 24 (!) Ringatomen auf. Der Makrocyclus wurde in einer sehr effizienten Synthese erhalten, bei der die Anionen durch selektive Monodeprotonierung entstehen.</p></abstract><textClass xml:lang="de"><keywords scheme="keyword"><list><head>keywords</head><item><term>Alkalimetalle</term></item><item><term>Amide</term></item><item><term>Erdalkalimetalle</term></item><item><term>Makrocyclen</term></item><item><term>Templatsynthesen</term></item></list></keywords></textClass><textClass><keywords scheme="Journal Subject"><list><head>article-category</head><item><term>Zuschrift</term></item></list></keywords></textClass></profileDesc><revisionDesc><change when="2000-02-07">Received</change><change when="2000-06-02">Published</change></revisionDesc></teiHeader></istex:fulltextTEI><json:item><original>false</original><mimetype>text/plain</mimetype><extension>txt</extension><uri>https://api.istex.fr/document/422CF70AD6C619A7537E8EC3BA73B57C480C230F/fulltext/txt</uri></json:item></fulltext><metadata><istex:metadataXml wicri:clean="Wiley, elements deleted: body"><istex:xmlDeclaration>version="1.0" encoding="UTF-8" standalone="yes"</istex:xmlDeclaration><istex:document><component version="2.0" type="serialArticle" xml:lang="en"><header><publicationMeta level="product"><publisherInfo><publisherName>WILEY‐VCH Verlag GmbH</publisherName><publisherLoc>Weinheim</publisherLoc></publisherInfo><doi registered="yes">10.1002/(ISSN)1521-3757</doi><issn type="print">0044-8249</issn><issn type="electronic">1521-3757</issn><idGroup><id type="product" value="ANGE"></id></idGroup><titleGroup><title type="main" xml:lang="de" sort="ANGEWANDTE CHEMIE">Angewandte Chemie</title><title type="short">Angew. 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Rep. of Germany</copyright><eventGroup><event type="manuscriptReceived" date="2000-02-07"></event><event type="firstOnline" date="2000-06-14"></event><event type="publishedOnlineFinalForm" date="2000-06-14"></event><event type="xmlConverted" agent="Converter:JWSART34_TO_WML3G version:2.4.7 mode:FullText source:HeaderRef result:HeaderRef" date="2011-02-24"></event><event type="xmlConverted" agent="Converter:WILEY_ML3G_TO_WILEY_ML3GV2 version:3.8.8" date="2014-01-03"></event><event type="xmlConverted" agent="Converter:WML3G_To_WML3G version:4.1.7 mode:FullText,remove_FC" date="2014-10-14"></event></eventGroup><numberingGroup><numbering type="pageFirst">2036</numbering><numbering type="pageLast">2038</numbering></numberingGroup><linkGroup><link type="toTypesetVersion" href="file:ANGE.ANGE2036.pdf"></link></linkGroup></publicationMeta><contentMeta><countGroup><count type="figureTotal" number="12"></count><count type="tableTotal" number="0"></count><count type="referenceTotal" number="14"></count></countGroup><titleGroup><title type="main" xml:lang="en">An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions</title></titleGroup><creators><creator xml:id="au1" creatorRole="author" affiliationRef="#afb"><personName><givenNames>Philip C.</givenNames><familyName>Andrews</familyName><degrees>Dr.</degrees></personName></creator><creator xml:id="au2" creatorRole="author" affiliationRef="#afa"><personName><givenNames>Alan R.</givenNames><familyName>Kennedy</familyName><degrees>Dr.</degrees></personName></creator><creator xml:id="au3" creatorRole="author" affiliationRef="#afa"><personName><givenNames>Robert E.</givenNames><familyName>Mulvey</familyName><degrees>Prof.</degrees></personName><contactDetails><email>r.e.mulvey@strath.ac.uk</email></contactDetails></creator><creator xml:id="au4" creatorRole="author" affiliationRef="#afb"><personName><givenNames>Colin L.</givenNames><familyName>Raston</familyName><degrees>Prof.</degrees></personName></creator><creator xml:id="au5" creatorRole="author" affiliationRef="#afb"><personName><givenNames>Brett A.</givenNames><familyName>Roberts</familyName></personName></creator><creator xml:id="au6" creatorRole="author" affiliationRef="#afa"><personName><givenNames>René B.</givenNames><familyName>Rowlings</familyName><degrees>Dr.</degrees></personName></creator></creators><affiliationGroup><affiliation xml:id="afa" countryCode="GB" type="organization"><unparsedAffiliation>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</unparsedAffiliation></affiliation><affiliation xml:id="afb" countryCode="AU" type="organization"><unparsedAffiliation>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</unparsedAffiliation></affiliation></affiliationGroup><keywordGroup xml:lang="de" type="author"><keyword xml:id="kwd1">Alkalimetalle</keyword><keyword xml:id="kwd2">Amide</keyword><keyword xml:id="kwd3">Erdalkalimetalle</keyword><keyword xml:id="kwd4">Makrocyclen</keyword><keyword xml:id="kwd5">Templatsynthesen</keyword></keywordGroup><abstractGroup><abstract type="short" xml:lang="de"><p><b>Sechs Aren‐Anionen</b> in einem kationischen [K<sub>6</sub>Mg<sub>6</sub>N<sub>12</sub>]<sup>6+</sup>‐Ring (siehe Bild, Aren=Benzol) weist das erste gemischte makrocyclische Metallamid mit 24 (!) Ringatomen auf. Der Makrocyclus wurde in einer sehr effizienten Synthese erhalten, bei der die Anionen durch selektive Monodeprotonierung entstehen.</p></abstract></abstractGroup></contentMeta><noteGroup><note xml:id="fnxx" numbered="no"><p>This work was supported by the UK Engineering and Physical Science Research Council (Grant award No. GR/M78113). Thanks are also extended to Dr. P. J. Nichols for help with the crystallographic work.</p></note></noteGroup></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions</title></titleInfo><name type="personal"><namePart type="given">Philip C.</namePart><namePart type="family">Andrews</namePart><namePart type="termsOfAddress">Dr.</namePart><affiliation>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Alan R.</namePart><namePart type="family">Kennedy</namePart><namePart type="termsOfAddress">Dr.</namePart><affiliation>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Robert E.</namePart><namePart type="family">Mulvey</namePart><namePart type="termsOfAddress">Prof.</namePart><affiliation>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</affiliation><affiliation>E-mail: r.e.mulvey@strath.ac.uk</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Colin L.</namePart><namePart type="family">Raston</namePart><namePart type="termsOfAddress">Prof.</namePart><affiliation>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Brett A.</namePart><namePart type="family">Roberts</namePart><affiliation>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">René B.</namePart><namePart type="family">Rowlings</namePart><namePart type="termsOfAddress">Dr.</namePart><affiliation>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="brief-communication" displayLabel="shortCommunication"></genre><originInfo><publisher>WILEY‐VCH Verlag GmbH</publisher><place><placeTerm type="text">Weinheim</placeTerm></place><dateIssued encoding="w3cdtf">2000-06-02</dateIssued><dateCaptured encoding="w3cdtf">2000-02-07</dateCaptured><copyrightDate encoding="w3cdtf">2000</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType><extent unit="figures">12</extent><extent unit="references">14</extent></physicalDescription><abstract type="short" lang="de">Sechs Aren‐Anionen in einem kationischen [K6Mg6N12]6+‐Ring (siehe Bild, Aren=Benzol) weist das erste gemischte makrocyclische Metallamid mit 24 (!) Ringatomen auf. Der Makrocyclus wurde in einer sehr effizienten Synthese erhalten, bei der die Anionen durch selektive Monodeprotonierung entstehen.</abstract><subject lang="de"><genre>keywords</genre><topic>Alkalimetalle</topic><topic>Amide</topic><topic>Erdalkalimetalle</topic><topic>Makrocyclen</topic><topic>Templatsynthesen</topic></subject><relatedItem type="host"><titleInfo><title>Angewandte Chemie</title></titleInfo><titleInfo type="abbreviated"><title>Angew. Chem.</title></titleInfo><genre type="journal">journal</genre><subject><genre>article-category</genre><topic>Zuschrift</topic></subject><identifier type="ISSN">0044-8249</identifier><identifier type="eISSN">1521-3757</identifier><identifier type="DOI">10.1002/(ISSN)1521-3757</identifier><identifier type="PublisherID">ANGE</identifier><part><date>2000</date><detail type="volume"><caption>vol.</caption><number>112</number></detail><detail type="issue"><caption>no.</caption><number>11</number></detail><extent unit="pages"><start>2036</start><end>2038</end><total>3</total></extent></part></relatedItem><identifier type="istex">422CF70AD6C619A7537E8EC3BA73B57C480C230F</identifier><identifier type="DOI">10.1002/1521-3757(20000602)112:11<2036::AID-ANGE2036>3.0.CO;2-2</identifier><identifier type="ArticleID">ANGE2036</identifier><accessCondition type="use and reproduction" contentType="copyright">Copyright © 2000 WILEY‐VCH Verlag GmbH, Weinheim, Fed. 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