Femtosecond Laser-Controlled Tip-to-Tip Assembly and Welding of Gold Nanorods
Identifieur interne : 001342 ( Ncbi/Checkpoint ); précédent : 001341; suivant : 001343Femtosecond Laser-Controlled Tip-to-Tip Assembly and Welding of Gold Nanorods
Auteurs : Guillermo González-Rubio [Espagne] ; Jesús González-Izquierdo [Espagne] ; Luis Ba Ares [Espagne] ; Gloria Tardajos [Espagne] ; Antonio Rivera [Espagne] ; Thomas Altantzis [Belgique] ; Sara Bals [Belgique] ; Ovidio Pe A-Rodríguez [Espagne] ; Andrés Guerrero-Martínez [Espagne] ; Luis M. Liz-Marzán [Espagne]Source :
- Nano Letters [ 1530-6984 ] ; 2015.
Abstract
Directed assembly of gold nanorods
through the use of dithiolated molecular linkers is one of the most
efficient methodologies for the morphologically controlled tip-to-tip
assembly of this type of anisotropic nanocrystals. However, in a direct
analogy to molecular polymerization synthesis, this process is characterized
by difficulties in chain-growth control over nanoparticle oligomers.
In particular, it is nearly impossible to favor the formation of one
type of oligomer, making the methodology hard to use for actual applications
in nanoplasmonics. We propose here a light-controlled synthetic procedure
that allows obtaining selected plasmonic oligomers in high yield and
with reaction times in the scale of minutes by irradiation with low
fluence near-infrared (NIR) femtosecond laser pulses. Selective inhibition
of the formation of gold nanorod
Url:
DOI: 10.1021/acs.nanolett.5b03844
PubMed: 26551469
PubMed Central: 4898861
Affiliations:
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PMC:4898861Le document en format XML
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<author><name sortKey="Gonzalez Izquierdo, Jesus" sort="Gonzalez Izquierdo, Jesus" uniqKey="Gonzalez Izquierdo J" first="Jesús" last="González-Izquierdo">Jesús González-Izquierdo</name>
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<author><name sortKey="Rivera, Antonio" sort="Rivera, Antonio" uniqKey="Rivera A" first="Antonio" last="Rivera">Antonio Rivera</name>
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, José Gutiérrez Abascal 2, E-28006 Madrid,<country>Spain</country>
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<country xml:lang="fr">Espagne</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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, Groenenborgerlaan 171, B-2020 Antwerp,<country>Belgium</country>
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<country xml:lang="fr">Belgique</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<author><name sortKey="Pe A Rodriguez, Ovidio" sort="Pe A Rodriguez, Ovidio" uniqKey="Pe A Rodriguez O" first="Ovidio" last="Pe A-Rodríguez">Ovidio Pe A-Rodríguez</name>
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, José Gutiérrez Abascal 2, E-28006 Madrid,<country>Spain</country>
</nlm:aff>
<country xml:lang="fr">Espagne</country>
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<author><name sortKey="Guerrero Martinez, Andres" sort="Guerrero Martinez, Andres" uniqKey="Guerrero Martinez A" first="Andrés" last="Guerrero-Martínez">Andrés Guerrero-Martínez</name>
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, Avda. Complutense s/n, 28040, Madrid,<country>Spain</country>
</nlm:aff>
<country xml:lang="fr">Espagne</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<author><name sortKey="Liz Marzan, Luis M" sort="Liz Marzan, Luis M" uniqKey="Liz Marzan L" first="Luis M." last="Liz-Marzán">Luis M. Liz-Marzán</name>
<affiliation wicri:level="1"><nlm:aff id="aff2">BioNanoPlasmonics Laboratory,<institution>CIC biomaGUNE</institution>
, Paseo de Miramón 182, 20009 Donostia - San Sebastián,<country>Spain</country>
</nlm:aff>
<country xml:lang="fr">Espagne</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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, 48013 Bilbao,<country>Spain</country>
</nlm:aff>
<country xml:lang="fr">Espagne</country>
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<series><title level="j">Nano Letters</title>
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<front><div type="abstract" xml:lang="en"><p content-type="toc-graphic"><graphic xlink:href="nl-2015-03844e_0006" id="ab-tgr1"></graphic>
</p>
<p>Directed assembly of gold nanorods
through the use of dithiolated molecular linkers is one of the most
efficient methodologies for the morphologically controlled tip-to-tip
assembly of this type of anisotropic nanocrystals. However, in a direct
analogy to molecular polymerization synthesis, this process is characterized
by difficulties in chain-growth control over nanoparticle oligomers.
In particular, it is nearly impossible to favor the formation of one
type of oligomer, making the methodology hard to use for actual applications
in nanoplasmonics. We propose here a light-controlled synthetic procedure
that allows obtaining selected plasmonic oligomers in high yield and
with reaction times in the scale of minutes by irradiation with low
fluence near-infrared (NIR) femtosecond laser pulses. Selective inhibition
of the formation of gold nanorod <italic>n</italic>
-mers (trimers)
with a longitudinal localized surface plasmon in resonance with a
800 nm Ti:sapphire laser, allowed efficient trapping of the (<italic>n</italic>
– 1)-mers (dimers) by hot spot mediated photothermal
decomposition of the interparticle molecular linkers. Laser irradiation
at higher energies produced near-field enhancement at the interparticle
gaps, which is large enough to melt gold nanorod tips, offering a
new pathway toward tip-to-tip welding of gold nanorod oligomers with
a plasmonic response at the NIR. Thorough optical and electron microscopy
characterization indicates that plasmonic oligomers can be selectively
trapped and welded, which has been analyzed in terms of a model that
predicts with reasonable accuracy the relative concentrations of the
main plasmonic species.</p>
</div>
</front>
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