Femtosecond Laser-Controlled Tip-to-Tip Assembly and Welding of Gold Nanorods.
Identifieur interne : 001397 ( PubMed/Curation ); précédent : 001396; suivant : 001398Femtosecond Laser-Controlled Tip-to-Tip Assembly and Welding of Gold Nanorods.
Auteurs : Guillermo González-Rubio [Espagne] ; Jesús González-Izquierdo [Espagne] ; Luis Ba Ares [Espagne] ; Gloria Tardajos [Espagne] ; Antonio Rivera [Espagne] ; Thomas Altantzis [Belgique] ; Sara Bals [Belgique] ; Ovidio Pe A-Rodríguez [Espagne] ; Andrés Guerrero-Martínez [Espagne] ; Luis M. Liz-Marzán [Espagne]Source :
- Nano letters [ 1530-6992 ] ; 2015.
Abstract
Directed assembly of gold nanorods through the use of dithiolated molecular linkers is one of the most efficient methodologies for the morphologically controlled tip-to-tip assembly of this type of anisotropic nanocrystals. However, in a direct analogy to molecular polymerization synthesis, this process is characterized by difficulties in chain-growth control over nanoparticle oligomers. In particular, it is nearly impossible to favor the formation of one type of oligomer, making the methodology hard to use for actual applications in nanoplasmonics. We propose here a light-controlled synthetic procedure that allows obtaining selected plasmonic oligomers in high yield and with reaction times in the scale of minutes by irradiation with low fluence near-infrared (NIR) femtosecond laser pulses. Selective inhibition of the formation of gold nanorod n-mers (trimers) with a longitudinal localized surface plasmon in resonance with a 800 nm Ti:sapphire laser, allowed efficient trapping of the (n - 1)-mers (dimers) by hot spot mediated photothermal decomposition of the interparticle molecular linkers. Laser irradiation at higher energies produced near-field enhancement at the interparticle gaps, which is large enough to melt gold nanorod tips, offering a new pathway toward tip-to-tip welding of gold nanorod oligomers with a plasmonic response at the NIR. Thorough optical and electron microscopy characterization indicates that plasmonic oligomers can be selectively trapped and welded, which has been analyzed in terms of a model that predicts with reasonable accuracy the relative concentrations of the main plasmonic species.
DOI: 10.1021/acs.nanolett.5b03844
PubMed: 26551469
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Complutense s/n, 28040, Madrid, Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid</wicri:regionArea></affiliation></author><author><name sortKey="Gonzalez Izquierdo, Jesus" sort="Gonzalez Izquierdo, Jesus" uniqKey="Gonzalez Izquierdo J" first="Jesús" last="González-Izquierdo">Jesús González-Izquierdo</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid, Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. 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Complutense s/n, 28040, Madrid, Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid</wicri:regionArea></affiliation></author><author><name sortKey="Rivera, Antonio" sort="Rivera, Antonio" uniqKey="Rivera A" first="Antonio" last="Rivera">Antonio Rivera</name><affiliation wicri:level="1"><nlm:affiliation>Instituto de Fusión Nuclear, Universidad Politécnica de Madrid , José Gutiérrez Abascal 2, E-28006 Madrid, Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Instituto de Fusión Nuclear, Universidad Politécnica de Madrid , José Gutiérrez Abascal 2, E-28006 Madrid</wicri:regionArea></affiliation></author><author><name sortKey="Altantzis, Thomas" sort="Altantzis, Thomas" uniqKey="Altantzis T" first="Thomas" last="Altantzis">Thomas Altantzis</name><affiliation wicri:level="1"><nlm:affiliation>EMAT-University of Antwerp , Groenenborgerlaan 171, B-2020 Antwerp, Belgium.</nlm:affiliation><country xml:lang="fr">Belgique</country><wicri:regionArea>EMAT-University of Antwerp , Groenenborgerlaan 171, B-2020 Antwerp</wicri:regionArea></affiliation></author><author><name sortKey="Bals, Sara" sort="Bals, Sara" uniqKey="Bals S" first="Sara" last="Bals">Sara Bals</name><affiliation wicri:level="1"><nlm:affiliation>EMAT-University of Antwerp , Groenenborgerlaan 171, B-2020 Antwerp, Belgium.</nlm:affiliation><country xml:lang="fr">Belgique</country><wicri:regionArea>EMAT-University of Antwerp , Groenenborgerlaan 171, B-2020 Antwerp</wicri:regionArea></affiliation></author><author><name sortKey="Pe A Rodriguez, Ovidio" sort="Pe A Rodriguez, Ovidio" uniqKey="Pe A Rodriguez O" first="Ovidio" last="Pe A-Rodríguez">Ovidio Pe A-Rodríguez</name><affiliation wicri:level="1"><nlm:affiliation>Instituto de Fusión Nuclear, Universidad Politécnica de Madrid , José Gutiérrez Abascal 2, E-28006 Madrid, Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Instituto de Fusión Nuclear, Universidad Politécnica de Madrid , José Gutiérrez Abascal 2, E-28006 Madrid</wicri:regionArea></affiliation></author><author><name sortKey="Guerrero Martinez, Andres" sort="Guerrero Martinez, Andres" uniqKey="Guerrero Martinez A" first="Andrés" last="Guerrero-Martínez">Andrés Guerrero-Martínez</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid, Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid</wicri:regionArea></affiliation></author><author><name sortKey="Liz Marzan, Luis M" sort="Liz Marzan, Luis M" uniqKey="Liz Marzan L" first="Luis M" last="Liz-Marzán">Luis M. Liz-Marzán</name><affiliation wicri:level="1"><nlm:affiliation>BioNanoPlasmonics Laboratory, CIC biomaGUNE , Paseo de Miramón 182, 20009 Donostia - San Sebastián, Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>BioNanoPlasmonics Laboratory, CIC biomaGUNE , Paseo de Miramón 182, 20009 Donostia - San Sebastián</wicri:regionArea></affiliation></author></analytic><series><title level="j">Nano letters</title><idno type="eISSN">1530-6992</idno><imprint><date when="2015" type="published">2015</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Directed assembly of gold nanorods through the use of dithiolated molecular linkers is one of the most efficient methodologies for the morphologically controlled tip-to-tip assembly of this type of anisotropic nanocrystals. However, in a direct analogy to molecular polymerization synthesis, this process is characterized by difficulties in chain-growth control over nanoparticle oligomers. In particular, it is nearly impossible to favor the formation of one type of oligomer, making the methodology hard to use for actual applications in nanoplasmonics. We propose here a light-controlled synthetic procedure that allows obtaining selected plasmonic oligomers in high yield and with reaction times in the scale of minutes by irradiation with low fluence near-infrared (NIR) femtosecond laser pulses. Selective inhibition of the formation of gold nanorod n-mers (trimers) with a longitudinal localized surface plasmon in resonance with a 800 nm Ti:sapphire laser, allowed efficient trapping of the (n - 1)-mers (dimers) by hot spot mediated photothermal decomposition of the interparticle molecular linkers. Laser irradiation at higher energies produced near-field enhancement at the interparticle gaps, which is large enough to melt gold nanorod tips, offering a new pathway toward tip-to-tip welding of gold nanorod oligomers with a plasmonic response at the NIR. Thorough optical and electron microscopy characterization indicates that plasmonic oligomers can be selectively trapped and welded, which has been analyzed in terms of a model that predicts with reasonable accuracy the relative concentrations of the main plasmonic species. </div></front></TEI><pubmed><MedlineCitation Status="PubMed-not-MEDLINE" Owner="NLM"><PMID Version="1">26551469</PMID><DateCompleted><Year>2016</Year><Month>04</Month><Day>20</Day></DateCompleted><DateRevised><Year>2019</Year><Month>01</Month><Day>11</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1530-6992</ISSN><JournalIssue CitedMedium="Internet"><Volume>15</Volume><Issue>12</Issue><PubDate><Year>2015</Year><Month>Dec</Month><Day>09</Day></PubDate></JournalIssue><Title>Nano letters</Title><ISOAbbreviation>Nano Lett.</ISOAbbreviation></Journal><ArticleTitle>Femtosecond Laser-Controlled Tip-to-Tip Assembly and Welding of Gold Nanorods.</ArticleTitle><Pagination><MedlinePgn>8282-8</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1021/acs.nanolett.5b03844</ELocationID><Abstract><AbstractText>Directed assembly of gold nanorods through the use of dithiolated molecular linkers is one of the most efficient methodologies for the morphologically controlled tip-to-tip assembly of this type of anisotropic nanocrystals. However, in a direct analogy to molecular polymerization synthesis, this process is characterized by difficulties in chain-growth control over nanoparticle oligomers. In particular, it is nearly impossible to favor the formation of one type of oligomer, making the methodology hard to use for actual applications in nanoplasmonics. We propose here a light-controlled synthetic procedure that allows obtaining selected plasmonic oligomers in high yield and with reaction times in the scale of minutes by irradiation with low fluence near-infrared (NIR) femtosecond laser pulses. Selective inhibition of the formation of gold nanorod n-mers (trimers) with a longitudinal localized surface plasmon in resonance with a 800 nm Ti:sapphire laser, allowed efficient trapping of the (n - 1)-mers (dimers) by hot spot mediated photothermal decomposition of the interparticle molecular linkers. Laser irradiation at higher energies produced near-field enhancement at the interparticle gaps, which is large enough to melt gold nanorod tips, offering a new pathway toward tip-to-tip welding of gold nanorod oligomers with a plasmonic response at the NIR. Thorough optical and electron microscopy characterization indicates that plasmonic oligomers can be selectively trapped and welded, which has been analyzed in terms of a model that predicts with reasonable accuracy the relative concentrations of the main plasmonic species. </AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>González-Rubio</LastName><ForeName>Guillermo</ForeName><Initials>G</Initials><AffiliationInfo><Affiliation>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid, Spain.</Affiliation></AffiliationInfo><AffiliationInfo><Affiliation>BioNanoPlasmonics Laboratory, CIC biomaGUNE , Paseo de Miramón 182, 20009 Donostia - San Sebastián, Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>González-Izquierdo</LastName><ForeName>Jesús</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid, Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Bañares</LastName><ForeName>Luis</ForeName><Initials>L</Initials><AffiliationInfo><Affiliation>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid, Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Tardajos</LastName><ForeName>Gloria</ForeName><Initials>G</Initials><AffiliationInfo><Affiliation>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid, Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Rivera</LastName><ForeName>Antonio</ForeName><Initials>A</Initials><AffiliationInfo><Affiliation>Instituto de Fusión Nuclear, Universidad Politécnica de Madrid , José Gutiérrez Abascal 2, E-28006 Madrid, Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Altantzis</LastName><ForeName>Thomas</ForeName><Initials>T</Initials><AffiliationInfo><Affiliation>EMAT-University of Antwerp , Groenenborgerlaan 171, B-2020 Antwerp, Belgium.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Bals</LastName><ForeName>Sara</ForeName><Initials>S</Initials><AffiliationInfo><Affiliation>EMAT-University of Antwerp , Groenenborgerlaan 171, B-2020 Antwerp, Belgium.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Peña-Rodríguez</LastName><ForeName>Ovidio</ForeName><Initials>O</Initials><AffiliationInfo><Affiliation>Instituto de Fusión Nuclear, Universidad Politécnica de Madrid , José Gutiérrez Abascal 2, E-28006 Madrid, Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Guerrero-Martínez</LastName><ForeName>Andrés</ForeName><Initials>A</Initials><AffiliationInfo><Affiliation>Departamento de Química Física I, Universidad Complutense de Madrid , Avda. Complutense s/n, 28040, Madrid, Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Liz-Marzán</LastName><ForeName>Luis M</ForeName><Initials>LM</Initials><AffiliationInfo><Affiliation>BioNanoPlasmonics Laboratory, CIC biomaGUNE , Paseo de Miramón 182, 20009 Donostia - San Sebastián, Spain.</Affiliation></AffiliationInfo><AffiliationInfo><Affiliation>Ikerbasque, Basque Foundation for Science , 48013 Bilbao, Spain.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType><PublicationType UI="D013485">Research Support, Non-U.S. Gov't</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2015</Year><Month>11</Month><Day>13</Day></ArticleDate></Article><MedlineJournalInfo><Country>United States</Country><MedlineTA>Nano Lett</MedlineTA><NlmUniqueID>101088070</NlmUniqueID><ISSNLinking>1530-6984</ISSNLinking></MedlineJournalInfo><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">Gold nanorod</Keyword><Keyword MajorTopicYN="N">dimer</Keyword><Keyword MajorTopicYN="N">femtosecond laser</Keyword><Keyword MajorTopicYN="N">nanoparticle assembly</Keyword><Keyword MajorTopicYN="N">welded nanoparticles</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="entrez"><Year>2015</Year><Month>11</Month><Day>10</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2015</Year><Month>11</Month><Day>10</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2015</Year><Month>11</Month><Day>10</Day><Hour>6</Hour><Minute>1</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">26551469</ArticleId><ArticleId 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