Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry
Identifieur interne : 000B85 ( Istex/Corpus ); précédent : 000B84; suivant : 000B86Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry
Auteurs : Sylvia Sander ; Wolfram Wagner ; Günter HenzeSource :
- Analytica Chimica Acta [ 0003-2670 ] ; 1997.
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- KwdEn :
Abstract
The paper describes the development of two different techniques for the automated determination of uranium by adsorptive stripping voltammetry (AdSV). As a complex forming reagent 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone (chloranilic acid) is used. The automation was performed in one case using an auto-batch system and in the second case by means of a flow-through cell. Sensitivities, reproducibilities and the fields of application are evaluated. The auto-batch technique, with the automatic standard addition capability as well as its logical decision-making capacity for selecting the correct type of working electrode makes it highly suitable for the determination of varying uranium concentrations above 1 μg/l. The dilution of the sample, required by the methodology, makes determinations of uranium concentrations less than 1 mg/l unattainable. The flow-through technique is more suited to determine uranium at the ultra trace concentration level (above 70 ng/l). Provided the matrix is reasonably constant, a pre-determined calibration curve can be used and, due to the higher slope of the calibration plot in the flow-through technique, the linear concentration range extends to a lower concentration compared to stationary conditions. Another advantage of the flow-through technique is the possibility of kinetic and mechanistic investigations of AdSV procedures.
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DOI: 10.1016/S0003-2670(96)00591-0
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ISTEX:B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515DLe document en format XML
<record><TEI wicri:istexFullTextTei="biblStruct"><teiHeader><fileDesc><titleStmt><title xml:lang="en">Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry</title><author><name sortKey="Sander, Sylvia" sort="Sander, Sylvia" uniqKey="Sander S" first="Sylvia" last="Sander">Sylvia Sander</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Wagner, Wolfram" sort="Wagner, Wolfram" uniqKey="Wagner W" first="Wolfram" last="Wagner">Wolfram Wagner</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Henze, Gunter" sort="Henze, Gunter" uniqKey="Henze G" first="Günter" last="Henze">Günter Henze</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</mods:affiliation></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D</idno><date when="1997" year="1997">1997</date><idno type="doi">10.1016/S0003-2670(96)00591-0</idno><idno type="url">https://api.istex.fr/document/B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D/fulltext/pdf</idno><idno type="wicri:Area/Istex/Corpus">000B85</idno><idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Corpus" wicri:corpus="ISTEX">000B85</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a" type="main" xml:lang="en">Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry</title><author><name sortKey="Sander, Sylvia" sort="Sander, Sylvia" uniqKey="Sander S" first="Sylvia" last="Sander">Sylvia Sander</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Wagner, Wolfram" sort="Wagner, Wolfram" uniqKey="Wagner W" first="Wolfram" last="Wagner">Wolfram Wagner</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</mods:affiliation></affiliation></author><author><name sortKey="Henze, Gunter" sort="Henze, Gunter" uniqKey="Henze G" first="Günter" last="Henze">Günter Henze</name><affiliation><mods:affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j">Analytica Chimica Acta</title><title level="j" type="abbrev">ACA</title><idno type="ISSN">0003-2670</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1997">1997</date><biblScope unit="volume">349</biblScope><biblScope unit="issue">1–3</biblScope><biblScope unit="page" from="93">93</biblScope><biblScope unit="page" to="99">99</biblScope></imprint><idno type="ISSN">0003-2670</idno></series><idno type="istex">B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D</idno><idno type="DOI">10.1016/S0003-2670(96)00591-0</idno><idno type="PII">S0003-2670(96)00591-0</idno><idno type="ArticleID">96005910</idno></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0003-2670</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Stripping voltammetry</term><term>Uranium traces</term><term>Waters</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The paper describes the development of two different techniques for the automated determination of uranium by adsorptive stripping voltammetry (AdSV). As a complex forming reagent 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone (chloranilic acid) is used. The automation was performed in one case using an auto-batch system and in the second case by means of a flow-through cell. Sensitivities, reproducibilities and the fields of application are evaluated. The auto-batch technique, with the automatic standard addition capability as well as its logical decision-making capacity for selecting the correct type of working electrode makes it highly suitable for the determination of varying uranium concentrations above 1 μg/l. The dilution of the sample, required by the methodology, makes determinations of uranium concentrations less than 1 mg/l unattainable. The flow-through technique is more suited to determine uranium at the ultra trace concentration level (above 70 ng/l). Provided the matrix is reasonably constant, a pre-determined calibration curve can be used and, due to the higher slope of the calibration plot in the flow-through technique, the linear concentration range extends to a lower concentration compared to stationary conditions. Another advantage of the flow-through technique is the possibility of kinetic and mechanistic investigations of AdSV procedures.</div></front></TEI><istex><corpusName>elsevier</corpusName><author><json:item><name>Sylvia Sander</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</json:string></affiliations></json:item><json:item><name>Wolfram Wagner</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</json:string></affiliations></json:item><json:item><name>Günter Henze</name><affiliations><json:string>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</json:string></affiliations></json:item></author><subject><json:item><lang><json:string>eng</json:string></lang><value>Stripping voltammetry</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Uranium traces</value></json:item><json:item><lang><json:string>eng</json:string></lang><value>Waters</value></json:item></subject><articleId><json:string>96005910</json:string></articleId><language><json:string>eng</json:string></language><originalGenre><json:string>Full-length article</json:string></originalGenre><abstract>The paper describes the development of two different techniques for the automated determination of uranium by adsorptive stripping voltammetry (AdSV). As a complex forming reagent 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone (chloranilic acid) is used. The automation was performed in one case using an auto-batch system and in the second case by means of a flow-through cell. Sensitivities, reproducibilities and the fields of application are evaluated. The auto-batch technique, with the automatic standard addition capability as well as its logical decision-making capacity for selecting the correct type of working electrode makes it highly suitable for the determination of varying uranium concentrations above 1 μg/l. The dilution of the sample, required by the methodology, makes determinations of uranium concentrations less than 1 mg/l unattainable. The flow-through technique is more suited to determine uranium at the ultra trace concentration level (above 70 ng/l). Provided the matrix is reasonably constant, a pre-determined calibration curve can be used and, due to the higher slope of the calibration plot in the flow-through technique, the linear concentration range extends to a lower concentration compared to stationary conditions. Another advantage of the flow-through technique is the possibility of kinetic and mechanistic investigations of AdSV procedures.</abstract><qualityIndicators><score>4.722</score><pdfVersion>1.2</pdfVersion><pdfPageSize>540 x 720 pts</pdfPageSize><refBibsNative>true</refBibsNative><keywordCount>3</keywordCount><abstractCharCount>1379</abstractCharCount><pdfWordCount>2406</pdfWordCount><pdfCharCount>15958</pdfCharCount><pdfPageCount>7</pdfPageCount><abstractWordCount>193</abstractWordCount></qualityIndicators><title>Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry</title><pii><json:string>S0003-2670(96)00591-0</json:string></pii><refBibs><json:item><host><volume>349</volume><pages><first>654</first></pages><author></author><title>Fresenius' J. Anal. Chem.</title></host></json:item><json:item><host><volume>305</volume><pages><first>154</first></pages><author></author><title>Anal. Chim. Acta</title></host></json:item></refBibs><genre><json:string>research-article</json:string></genre><host><volume>349</volume><pii><json:string>S0003-2670(00)X0091-8</json:string></pii><pages><last>99</last><first>93</first></pages><issn><json:string>0003-2670</json:string></issn><issue>1–3</issue><genre><json:string>journal</json:string></genre><language><json:string>unknown</json:string></language><title>Analytica Chimica Acta</title><publicationDate>1997</publicationDate></host><categories><wos><json:string>science</json:string><json:string>chemistry, analytical</json:string></wos><scienceMetrix><json:string>natural sciences</json:string><json:string>chemistry</json:string><json:string>analytical chemistry</json:string></scienceMetrix></categories><publicationDate>1997</publicationDate><copyrightDate>1997</copyrightDate><doi><json:string>10.1016/S0003-2670(96)00591-0</json:string></doi><id>B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D</id><score>0.67457557</score><fulltext><json:item><extension>pdf</extension><original>true</original><mimetype>application/pdf</mimetype><uri>https://api.istex.fr/document/B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D/fulltext/pdf</uri></json:item><json:item><extension>zip</extension><original>false</original><mimetype>application/zip</mimetype><uri>https://api.istex.fr/document/B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D/fulltext/zip</uri></json:item><istex:fulltextTEI uri="https://api.istex.fr/document/B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D/fulltext/tei"><teiHeader><fileDesc><titleStmt><title level="a" type="main" xml:lang="en">Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry</title></titleStmt><publicationStmt><authority>ISTEX</authority><publisher>ELSEVIER</publisher><availability><p>ELSEVIER</p></availability><date>1997</date></publicationStmt><notesStmt><note type="content">Section title: Electroanalytical chemistry</note></notesStmt><sourceDesc><biblStruct type="inbook"><analytic><title level="a" type="main" xml:lang="en">Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry</title><author xml:id="author-1"><persName><forename type="first">Sylvia</forename><surname>Sander</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</affiliation></author><author xml:id="author-2"><persName><forename type="first">Wolfram</forename><surname>Wagner</surname></persName><affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</affiliation></author><author xml:id="author-3"><persName><forename type="first">Günter</forename><surname>Henze</surname></persName><note type="correspondence"><p>Corresponding author.</p></note><affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</affiliation></author></analytic><monogr><title level="j">Analytica Chimica Acta</title><title level="j" type="abbrev">ACA</title><idno type="pISSN">0003-2670</idno><idno type="PII">S0003-2670(00)X0091-8</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1997"></date><biblScope unit="volume">349</biblScope><biblScope unit="issue">1–3</biblScope><biblScope unit="page" from="93">93</biblScope><biblScope unit="page" to="99">99</biblScope></imprint></monogr><idno type="istex">B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D</idno><idno type="DOI">10.1016/S0003-2670(96)00591-0</idno><idno type="PII">S0003-2670(96)00591-0</idno><idno type="ArticleID">96005910</idno></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>1997</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="en"><p>The paper describes the development of two different techniques for the automated determination of uranium by adsorptive stripping voltammetry (AdSV). As a complex forming reagent 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone (chloranilic acid) is used. The automation was performed in one case using an auto-batch system and in the second case by means of a flow-through cell. Sensitivities, reproducibilities and the fields of application are evaluated. The auto-batch technique, with the automatic standard addition capability as well as its logical decision-making capacity for selecting the correct type of working electrode makes it highly suitable for the determination of varying uranium concentrations above 1 μg/l. The dilution of the sample, required by the methodology, makes determinations of uranium concentrations less than 1 mg/l unattainable. The flow-through technique is more suited to determine uranium at the ultra trace concentration level (above 70 ng/l). Provided the matrix is reasonably constant, a pre-determined calibration curve can be used and, due to the higher slope of the calibration plot in the flow-through technique, the linear concentration range extends to a lower concentration compared to stationary conditions. Another advantage of the flow-through technique is the possibility of kinetic and mechanistic investigations of AdSV procedures.</p></abstract><textClass xml:lang="en"><keywords scheme="keyword"><list><head>Keywords</head><item><term>Stripping voltammetry</term></item><item><term>Uranium traces</term></item><item><term>Waters</term></item></list></keywords></textClass></profileDesc><revisionDesc><change when="1996-11-20">Modified</change><change when="1997">Published</change></revisionDesc></teiHeader></istex:fulltextTEI><json:item><extension>txt</extension><original>false</original><mimetype>text/plain</mimetype><uri>https://api.istex.fr/document/B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D/fulltext/txt</uri></json:item></fulltext><metadata><istex:metadataXml wicri:clean="Elsevier, elements deleted: tail"><istex:xmlDeclaration>version="1.0" encoding="UTF-8"</istex:xmlDeclaration><istex:docType PUBLIC="-//ES//DTD journal article DTD version 4.5.2//EN//XML" URI="art452.dtd" name="istex:docType"></istex:docType><istex:document><converted-article version="4.5.2" docsubtype="fla" xml:lang="en"><item-info><jid>ACA</jid><aid>96005910</aid><ce:pii>S0003-2670(96)00591-0</ce:pii><ce:doi>10.1016/S0003-2670(96)00591-0</ce:doi><ce:copyright type="unknown" year="1997"></ce:copyright></item-info><head><ce:dochead><ce:textfn>Electroanalytical chemistry</ce:textfn></ce:dochead><ce:title>Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry</ce:title><ce:author-group><ce:author><ce:given-name>Sylvia</ce:given-name><ce:surname>Sander</ce:surname></ce:author><ce:author><ce:given-name>Wolfram</ce:given-name><ce:surname>Wagner</ce:surname></ce:author><ce:author><ce:given-name>Günter</ce:given-name><ce:surname>Henze</ce:surname><ce:cross-ref refid="COR1"><ce:sup loc="post">∗</ce:sup></ce:cross-ref></ce:author><ce:affiliation><ce:textfn>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</ce:textfn></ce:affiliation><ce:correspondence id="COR1"><ce:label>∗</ce:label><ce:text>Corresponding author.</ce:text></ce:correspondence></ce:author-group><ce:date-received day="12" month="8" year="1996"></ce:date-received><ce:date-revised day="20" month="11" year="1996"></ce:date-revised><ce:date-accepted day="30" month="11" year="1996"></ce:date-accepted><ce:abstract class="author"><ce:section-title>Abstract</ce:section-title><ce:abstract-sec><ce:simple-para view="all" id="simple-para.0010">The paper describes the development of two different techniques for the automated determination of uranium by adsorptive stripping voltammetry (AdSV). As a complex forming reagent 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone (chloranilic acid) is used. The automation was performed in one case using an auto-batch system and in the second case by means of a flow-through cell. Sensitivities, reproducibilities and the fields of application are evaluated. The auto-batch technique, with the automatic standard addition capability as well as its logical decision-making capacity for selecting the correct type of working electrode makes it highly suitable for the determination of varying uranium concentrations above 1 μg/l. The dilution of the sample, required by the methodology, makes determinations of uranium concentrations less than 1 mg/l unattainable. The flow-through technique is more suited to determine uranium at the ultra trace concentration level (above 70 ng/l). Provided the matrix is reasonably constant, a pre-determined calibration curve can be used and, due to the higher slope of the calibration plot in the flow-through technique, the linear concentration range extends to a lower concentration compared to stationary conditions. Another advantage of the flow-through technique is the possibility of kinetic and mechanistic investigations of AdSV procedures.</ce:simple-para></ce:abstract-sec></ce:abstract><ce:keywords class="keyword"><ce:section-title>Keywords</ce:section-title><ce:keyword><ce:text>Stripping voltammetry</ce:text></ce:keyword><ce:keyword><ce:text>Uranium traces</ce:text></ce:keyword><ce:keyword><ce:text>Waters</ce:text></ce:keyword></ce:keywords></head></converted-article></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry</title></titleInfo><titleInfo type="alternative" lang="en" contentType="CDATA"><title>Possibilities for the automated determination of trace concentrations of uranium in water samples by adsorptive stripping voltammetry</title></titleInfo><name type="personal"><namePart type="given">Sylvia</namePart><namePart type="family">Sander</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Wolfram</namePart><namePart type="family">Wagner</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Günter</namePart><namePart type="family">Henze</namePart><affiliation>Fachbereich Chemie, Universität Kaiserslautem und Abteilung für Anorganische und Analytische Chemie, Universität Trier, Postfach 3825, D-54286 Trier, Germany</affiliation><description>Corresponding author.</description><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="research-article" displayLabel="Full-length article"></genre><originInfo><publisher>ELSEVIER</publisher><dateIssued encoding="w3cdtf">1997</dateIssued><dateModified encoding="w3cdtf">1996-11-20</dateModified><copyrightDate encoding="w3cdtf">1997</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">eng</languageTerm><languageTerm type="code" authority="rfc3066">en</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="en">The paper describes the development of two different techniques for the automated determination of uranium by adsorptive stripping voltammetry (AdSV). As a complex forming reagent 2,5-dichloro-3,6-dihydroxy-1,4-benzoquinone (chloranilic acid) is used. The automation was performed in one case using an auto-batch system and in the second case by means of a flow-through cell. Sensitivities, reproducibilities and the fields of application are evaluated. The auto-batch technique, with the automatic standard addition capability as well as its logical decision-making capacity for selecting the correct type of working electrode makes it highly suitable for the determination of varying uranium concentrations above 1 μg/l. The dilution of the sample, required by the methodology, makes determinations of uranium concentrations less than 1 mg/l unattainable. The flow-through technique is more suited to determine uranium at the ultra trace concentration level (above 70 ng/l). Provided the matrix is reasonably constant, a pre-determined calibration curve can be used and, due to the higher slope of the calibration plot in the flow-through technique, the linear concentration range extends to a lower concentration compared to stationary conditions. Another advantage of the flow-through technique is the possibility of kinetic and mechanistic investigations of AdSV procedures.</abstract><note type="content">Section title: Electroanalytical chemistry</note><subject lang="en"><genre>Keywords</genre><topic>Stripping voltammetry</topic><topic>Uranium traces</topic><topic>Waters</topic></subject><relatedItem type="host"><titleInfo><title>Analytica Chimica Acta</title></titleInfo><titleInfo type="abbreviated"><title>ACA</title></titleInfo><genre type="journal">journal</genre><originInfo><dateIssued encoding="w3cdtf">19970829</dateIssued></originInfo><identifier type="ISSN">0003-2670</identifier><identifier type="PII">S0003-2670(00)X0091-8</identifier><part><date>19970829</date><detail type="volume"><number>349</number><caption>vol.</caption></detail><detail type="issue"><number>1–3</number><caption>no.</caption></detail><extent unit="issue pages"><start>1</start><end>388</end></extent><extent unit="pages"><start>93</start><end>99</end></extent></part></relatedItem><identifier type="istex">B23ACD6759AEEEFFBBC03E5AA587D9DC4B10515D</identifier><identifier type="DOI">10.1016/S0003-2670(96)00591-0</identifier><identifier type="PII">S0003-2670(96)00591-0</identifier><identifier type="ArticleID">96005910</identifier><recordInfo><recordContentSource>ELSEVIER</recordContentSource></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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