Determination of ten pyrethroids in various fruit juices: comparison of dispersive liquid-liquid microextraction sample preparation and QuEChERS method combined with dispersive liquid-liquid microextraction.
Identifieur interne : 000359 ( PubMed/Checkpoint ); précédent : 000358; suivant : 000360Determination of ten pyrethroids in various fruit juices: comparison of dispersive liquid-liquid microextraction sample preparation and QuEChERS method combined with dispersive liquid-liquid microextraction.
Auteurs : Yaohai Zhang [République populaire de Chine] ; Xuelian Zhang [République populaire de Chine] ; Bining Jiao [République populaire de Chine]Source :
- Food chemistry [ 0308-8146 ] ; 2014.
English descriptors
- KwdEn :
- Beverages (analysis), Chemical Fractionation (methods), Citrus (chemistry), Citrus sinensis (chemistry), Food Contamination (analysis), Fruit (chemistry), Gas Chromatography-Mass Spectrometry, Insecticides (chemistry), Insecticides (isolation & purification), Liquid Phase Microextraction (methods), Malus (chemistry), Pesticide Residues (chemistry), Pesticide Residues (isolation & purification), Prunus (chemistry), Pyrethrins (chemistry), Pyrethrins (isolation & purification).
- MESH :
- chemical , chemistry : Insecticides, Pesticide Residues, Pyrethrins.
- analysis : Beverages, Food Contamination.
- chemistry : Citrus, Citrus sinensis, Fruit, Malus, Prunus.
- chemical , isolation & purification : Insecticides, Pesticide Residues, Pyrethrins.
- methods : Chemical Fractionation, Liquid Phase Microextraction.
- Gas Chromatography-Mass Spectrometry.
Abstract
Dispersive liquid-liquid microextraction (DLLME) sample preparation and the quick, easy, cheap, effective, rugged and safe (QuEChERS) method combined with DLLME were developed and compared for the analysis of ten pyrethroids in various fruit juices using gas chromatography-electron capture detection (GC-ECD). QuEChERS-DLLME method has found its widespread applications to all the fruit juices including those samples with more complex matrices (orange, lemon, kiwi and mango) while DLLME was confined to the fruit juices with simpler matrices (apple, pear, grape and peach). The two methods provided acceptable recoveries and repeatability. In addition, the applicabilities of two methods were demonstrated with the real samples and further confirmed by gas chromatography-mass spectrometry (GC-MS).
DOI: 10.1016/j.foodchem.2014.03.028
PubMed: 24767068
Affiliations:
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pubmed:24767068Le document en format XML
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<term>Food Contamination (analysis)</term>
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<term>Gas Chromatography-Mass Spectrometry</term>
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<front><div type="abstract" xml:lang="en">Dispersive liquid-liquid microextraction (DLLME) sample preparation and the quick, easy, cheap, effective, rugged and safe (QuEChERS) method combined with DLLME were developed and compared for the analysis of ten pyrethroids in various fruit juices using gas chromatography-electron capture detection (GC-ECD). QuEChERS-DLLME method has found its widespread applications to all the fruit juices including those samples with more complex matrices (orange, lemon, kiwi and mango) while DLLME was confined to the fruit juices with simpler matrices (apple, pear, grape and peach). The two methods provided acceptable recoveries and repeatability. In addition, the applicabilities of two methods were demonstrated with the real samples and further confirmed by gas chromatography-mass spectrometry (GC-MS).</div>
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<Abstract><AbstractText>Dispersive liquid-liquid microextraction (DLLME) sample preparation and the quick, easy, cheap, effective, rugged and safe (QuEChERS) method combined with DLLME were developed and compared for the analysis of ten pyrethroids in various fruit juices using gas chromatography-electron capture detection (GC-ECD). QuEChERS-DLLME method has found its widespread applications to all the fruit juices including those samples with more complex matrices (orange, lemon, kiwi and mango) while DLLME was confined to the fruit juices with simpler matrices (apple, pear, grape and peach). The two methods provided acceptable recoveries and repeatability. In addition, the applicabilities of two methods were demonstrated with the real samples and further confirmed by gas chromatography-mass spectrometry (GC-MS).</AbstractText>
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