OrangerV1, Pmc, Corpus, bibRecord, 000A60

Immunochemical Screening of Pesticides (Simazine and Cypermethrin) in Orange Oil

Identifieur interne : 000A60 ( Pmc/Corpus ); précédent : 000A59; suivant : 000A61

Immunochemical Screening of Pesticides (Simazine and Cypermethrin) in Orange Oil

Auteurs : Mikaela Nichkova ; Xun Fu ; Zheng Yang ; Ping Zhong ; James R. Sanborn ; Dan Chang ; Shirley J. Gee ; Bruce D. Hammock

Source :

Journal of agricultural and food chemistry [ 0021-8561 ] ; 2009.

RBID : PMC:3033343

Abstract

Pesticide residue analysis in citrus oils is very important for their quality and marketing. This study assessed the reliability and sensitivity of enzyme-linked immunosorbent assays (ELISA) for simazine and cypermethrin screening in orange oil. Simazine was analyzed after extraction of the oil with methanolic phosphate buffer with a limit of quantitation (LOQ) of 40 µg/L for 1-fold and ~100 µg/L for 10-fold oils. Due to matrix effects the immunoanalysis of cypermethrin required hexane–acetonitrile partitioning followed by silica solid phase extraction. The method detected levels higher than 0.5 ppm (mg/L). This LOQ is lower than the U.S. EPA tolerance level (0.9 ppm) for cypermethrin in citrus oils. A good correlation (r² 0.99) between ELISA and LC-MS/MS was observed for the analysis of both analytes in 1-fold orange oil. Immunochemical screening can be used to reduce instrumental analysis costs by its use in preliminary orange oil screening.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3033343

DOI: 10.1021/jf900652a
PubMed: 19526986
PubMed Central: 3033343

Links to Exploration step

PMC:3033343

Le document en format XML

<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Immunochemical Screening of Pesticides (Simazine and Cypermethrin) in Orange Oil</title>
<author><name sortKey="Nichkova, Mikaela" sort="Nichkova, Mikaela" uniqKey="Nichkova M" first="Mikaela" last="Nichkova">Mikaela Nichkova</name>
<affiliation><nlm:aff id="A1">Department of Entomology, University of California, One Shields Avenue, Davis, California 95616</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Fu, Xun" sort="Fu, Xun" uniqKey="Fu X" first="Xun" last="Fu">Xun Fu</name>
<affiliation><nlm:aff id="A2">Givaudan Flavors Corp., 1199 Edison Drive, Cincinnati, Ohio 45216</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Yang, Zheng" sort="Yang, Zheng" uniqKey="Yang Z" first="Zheng" last="Yang">Zheng Yang</name>
<affiliation><nlm:aff id="A3">Givaudan Flavors Corp., 4705 U. S. Highway 92 East, Lakeland, Florida 33801</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Zhong, Ping" sort="Zhong, Ping" uniqKey="Zhong P" first="Ping" last="Zhong">Ping Zhong</name>
<affiliation><nlm:aff id="A2">Givaudan Flavors Corp., 1199 Edison Drive, Cincinnati, Ohio 45216</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Sanborn, James R" sort="Sanborn, James R" uniqKey="Sanborn J" first="James R." last="Sanborn">James R. Sanborn</name>
<affiliation><nlm:aff id="A1">Department of Entomology, University of California, One Shields Avenue, Davis, California 95616</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Chang, Dan" sort="Chang, Dan" uniqKey="Chang D" first="Dan" last="Chang">Dan Chang</name>
<affiliation><nlm:aff id="A4">Synthia-LLC, P.O. Box 1238, Gualala, California 95445</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Gee, Shirley J" sort="Gee, Shirley J" uniqKey="Gee S" first="Shirley J." last="Gee">Shirley J. Gee</name>
<affiliation><nlm:aff id="A4">Synthia-LLC, P.O. Box 1238, Gualala, California 95445</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Hammock, Bruce D" sort="Hammock, Bruce D" uniqKey="Hammock B" first="Bruce D." last="Hammock">Bruce D. Hammock</name>
<affiliation><nlm:aff id="A1">Department of Entomology, University of California, One Shields Avenue, Davis, California 95616</nlm:aff>
</affiliation>
</author>
</titleStmt>
<publicationStmt><idno type="wicri:source">PMC</idno>
<idno type="pmid">19526986</idno>
<idno type="pmc">3033343</idno>
<idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3033343</idno>
<idno type="RBID">PMC:3033343</idno>
<idno type="doi">10.1021/jf900652a</idno>
<date when="2009">2009</date>
<idno type="wicri:Area/Pmc/Corpus">000A60</idno>
</publicationStmt>
<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Immunochemical Screening of Pesticides (Simazine and Cypermethrin) in Orange Oil</title>
<author><name sortKey="Nichkova, Mikaela" sort="Nichkova, Mikaela" uniqKey="Nichkova M" first="Mikaela" last="Nichkova">Mikaela Nichkova</name>
<affiliation><nlm:aff id="A1">Department of Entomology, University of California, One Shields Avenue, Davis, California 95616</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Fu, Xun" sort="Fu, Xun" uniqKey="Fu X" first="Xun" last="Fu">Xun Fu</name>
<affiliation><nlm:aff id="A2">Givaudan Flavors Corp., 1199 Edison Drive, Cincinnati, Ohio 45216</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Yang, Zheng" sort="Yang, Zheng" uniqKey="Yang Z" first="Zheng" last="Yang">Zheng Yang</name>
<affiliation><nlm:aff id="A3">Givaudan Flavors Corp., 4705 U. S. Highway 92 East, Lakeland, Florida 33801</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Zhong, Ping" sort="Zhong, Ping" uniqKey="Zhong P" first="Ping" last="Zhong">Ping Zhong</name>
<affiliation><nlm:aff id="A2">Givaudan Flavors Corp., 1199 Edison Drive, Cincinnati, Ohio 45216</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Sanborn, James R" sort="Sanborn, James R" uniqKey="Sanborn J" first="James R." last="Sanborn">James R. Sanborn</name>
<affiliation><nlm:aff id="A1">Department of Entomology, University of California, One Shields Avenue, Davis, California 95616</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Chang, Dan" sort="Chang, Dan" uniqKey="Chang D" first="Dan" last="Chang">Dan Chang</name>
<affiliation><nlm:aff id="A4">Synthia-LLC, P.O. Box 1238, Gualala, California 95445</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Gee, Shirley J" sort="Gee, Shirley J" uniqKey="Gee S" first="Shirley J." last="Gee">Shirley J. Gee</name>
<affiliation><nlm:aff id="A4">Synthia-LLC, P.O. Box 1238, Gualala, California 95445</nlm:aff>
</affiliation>
</author>
<author><name sortKey="Hammock, Bruce D" sort="Hammock, Bruce D" uniqKey="Hammock B" first="Bruce D." last="Hammock">Bruce D. Hammock</name>
<affiliation><nlm:aff id="A1">Department of Entomology, University of California, One Shields Avenue, Davis, California 95616</nlm:aff>
</affiliation>
</author>
</analytic>
<series><title level="j">Journal of agricultural and food chemistry</title>
<idno type="ISSN">0021-8561</idno>
<idno type="eISSN">1520-5118</idno>
<imprint><date when="2009">2009</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
</fileDesc>
<profileDesc><textClass></textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en"><p id="P2">Pesticide residue analysis in citrus oils is very important for their quality and marketing. This study assessed the reliability and sensitivity of enzyme-linked immunosorbent assays (ELISA) for simazine and cypermethrin screening in orange oil. Simazine was analyzed after extraction of the oil with methanolic phosphate buffer with a limit of quantitation (LOQ) of 40 µg/L for 1-fold and ~100 µg/L for 10-fold oils. Due to matrix effects the immunoanalysis of cypermethrin required hexane–acetonitrile partitioning followed by silica solid phase extraction. The method detected levels higher than 0.5 ppm (mg/L). This LOQ is lower than the U.S. EPA tolerance level (0.9 ppm) for cypermethrin in citrus oils. A good correlation (<italic>r</italic>
<sup>2</sup>
 0.99) between ELISA and LC-MS/MS was observed for the analysis of both analytes in 1-fold orange oil. Immunochemical screening can be used to reduce instrumental analysis costs by its use in preliminary orange oil screening.</p>
</div>
</front>
</TEI>
<pmc article-type="research-article" xml:lang="EN"><pmc-comment>The publisher of this article does not allow downloading of the full text in XML form.</pmc-comment>
  <pmc-dir>properties manuscript</pmc-dir>
  <front><journal-meta><journal-id journal-id-type="nlm-journal-id">0374755</journal-id>
<journal-id journal-id-type="pubmed-jr-id">4421</journal-id>
<journal-id journal-id-type="nlm-ta">J Agric Food Chem</journal-id>
<journal-title>Journal of agricultural and food chemistry</journal-title>
<issn pub-type="ppub">0021-8561</issn>
<issn pub-type="epub">1520-5118</issn>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">19526986</article-id>
<article-id pub-id-type="pmc">3033343</article-id>
<article-id pub-id-type="doi">10.1021/jf900652a</article-id>
<article-id pub-id-type="manuscript">NIHMS267615</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Article</subject>
</subj-group>
</article-categories>
<title-group><article-title>Immunochemical Screening of Pesticides (Simazine and Cypermethrin) in Orange Oil</article-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Nichkova</surname>
<given-names>Mikaela</given-names>
</name>
<xref ref-type="aff" rid="A1">†</xref>
<xref ref-type="author-notes" rid="FN1">⊥</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Fu</surname>
<given-names>Xun</given-names>
</name>
<xref ref-type="aff" rid="A2">‡</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Yang</surname>
<given-names>Zheng</given-names>
</name>
<xref ref-type="aff" rid="A3">§</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Zhong</surname>
<given-names>Ping</given-names>
</name>
<xref ref-type="aff" rid="A2">‡</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Sanborn</surname>
<given-names>James R.</given-names>
</name>
<xref ref-type="aff" rid="A1">†</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Chang</surname>
<given-names>Dan</given-names>
</name>
<xref ref-type="aff" rid="A4">#</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Gee</surname>
<given-names>Shirley J.</given-names>
</name>
<xref ref-type="aff" rid="A4">#</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Hammock</surname>
<given-names>Bruce D.</given-names>
</name>
<xref ref-type="aff" rid="A1">†</xref>
<xref ref-type="corresp" rid="cor1">*</xref>
</contrib>
</contrib-group>
<aff id="A1"><label>†</label>
Department of Entomology, University of California, One Shields Avenue, Davis, California 95616</aff>
<aff id="A2"><label>‡</label>
Givaudan Flavors Corp., 1199 Edison Drive, Cincinnati, Ohio 45216</aff>
<aff id="A3"><label>§</label>
Givaudan Flavors Corp., 4705 U. S. Highway 92 East, Lakeland, Florida 33801</aff>
<aff id="A4"><label>#</label>
Synthia-LLC, P.O. Box 1238, Gualala, California 95445</aff>
<author-notes><corresp id="cor1"><label>*</label>
Corresponding author [telephone (530) 752-8465; fax (530) 752-1537; <email>bdhammock@ucdavis.edu</email>
]</corresp>
<fn id="FN1" fn-type="present-address"><label>⊥</label>
<p id="P1">Present address: Pharmasan Laboratories, 373 280th Street, Osceola, Wisconsin 54020</p>
</fn>
</author-notes>
<pub-date pub-type="nihms-submitted"><day>26</day>
<month>1</month>
<year>2011</year>
</pub-date>
<pub-date pub-type="ppub"><day>8</day>
<month>7</month>
<year>2009</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>3</day>
<month>2</month>
<year>2011</year>
</pub-date>
<volume>57</volume>
<issue>13</issue>
<fpage>5673</fpage>
<lpage>5679</lpage>
<permissions><copyright-statement>© 2009 American Chemical Society</copyright-statement>
<copyright-year>2009</copyright-year>
</permissions>
<abstract><p id="P2">Pesticide residue analysis in citrus oils is very important for their quality and marketing. This study assessed the reliability and sensitivity of enzyme-linked immunosorbent assays (ELISA) for simazine and cypermethrin screening in orange oil. Simazine was analyzed after extraction of the oil with methanolic phosphate buffer with a limit of quantitation (LOQ) of 40 µg/L for 1-fold and ~100 µg/L for 10-fold oils. Due to matrix effects the immunoanalysis of cypermethrin required hexane–acetonitrile partitioning followed by silica solid phase extraction. The method detected levels higher than 0.5 ppm (mg/L). This LOQ is lower than the U.S. EPA tolerance level (0.9 ppm) for cypermethrin in citrus oils. A good correlation (<italic>r</italic>
<sup>2</sup>
 0.99) between ELISA and LC-MS/MS was observed for the analysis of both analytes in 1-fold orange oil. Immunochemical screening can be used to reduce instrumental analysis costs by its use in preliminary orange oil screening.</p>
</abstract>
<kwd-group><kwd>Immunoassay</kwd>
<kwd>orange oil</kwd>
<kwd>pyrethroids</kwd>
<kwd>triazines</kwd>
</kwd-group>
<contract-num rid="ES1">P42 ES004699-24
				||ES</contract-num>
<contract-sponsor id="ES1">National Institute of Environmental Health Sciences : NIEHS</contract-sponsor>
</article-meta>
</front>
</pmc>
</record>

Pour manipuler ce document sous Unix (Dilib)

EXPLOR_STEP=$WICRI_ROOT/Wicri/Bois/explor/OrangerV1/Data/Pmc/Corpus

HfdSelect -h $EXPLOR_STEP/biblio.hfd -nk 000A60 | SxmlIndent | more

HfdSelect -h $EXPLOR_AREA/Data/Pmc/Corpus/biblio.hfd -nk 000A60 | SxmlIndent | more

Pour mettre un lien sur cette page dans le réseau Wicri

{{Explor lien
   |wiki=    Wicri/Bois
   |area=    OrangerV1
   |flux=    Pmc
   |étape=   Corpus
   |type=    RBID
   |clé=     PMC:3033343
   |texte=   Immunochemical Screening of Pesticides (Simazine and Cypermethrin) in Orange Oil
}}

Pour générer des pages wiki

HfdIndexSelect -h $EXPLOR_AREA/Data/Pmc/Corpus/RBID.i   -Sk "pubmed:19526986" \
       | HfdSelect -Kh $EXPLOR_AREA/Data/Pmc/Corpus/biblio.hfd   \
       | NlmPubMed2Wicri -a OrangerV1

This area was generated with Dilib version V0.6.25.
Data generation: Sat Dec 3 17:11:04 2016. Site generation: Wed Mar 6 18:18:32 2024

	Serveur d'exploration sur l'oranger
	Attention, ce site est en cours de développement ! Attention, site généré par des moyens informatiques à partir de corpus bruts. Les informations ne sont donc pas validées.

Serveur d'exploration sur l'oranger

Immunochemical Screening of Pesticides (Simazine and Cypermethrin) in Orange Oil

Immunochemical Screening of Pesticides (Simazine and Cypermethrin) in Orange Oil

Source :

Abstract

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri

Pour générer des pages wiki