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Isolation of antioxidant compounds from orange juice by using countercurrent supercritical fluid extraction (CC-SFE)

Identifieur interne : 000148 ( PascalFrancis/Curation ); précédent : 000147; suivant : 000149

Isolation of antioxidant compounds from orange juice by using countercurrent supercritical fluid extraction (CC-SFE)

Auteurs : Francisco J. Senorans [Espagne] ; Alejandro Ruiz-Rodriguez [Espagne] ; Sofia Cavero [Espagne] ; Alejandro Cifuentes [Espagne] ; Elena Ibanez [Espagne] ; Guillermo Reglero [Espagne]

Source :

RBID : Pascal:02-0115226

Descripteurs français

English descriptors

Abstract

Antioxidants from orange juice are isolated by the use of countercurrent supercritical fluid extraction (CC-SFE) and characterized by reversed-phase liquid chromatography (RPLC) coupled to mass spectrometry (MS) and diode-array detection (DAD). A pilot-scale SFE plant equipped with a packed column has been employed for countercurrent extraction and fractionation of raw orange juice with carbon dioxide. Several experiments have been performed in order to study the effect of the countercurrent conditions on the content of antioxidative compounds. In this study, the main variable that has been considered is the solvent-to-feed ratio (S/F) because it plays an essential role in the extraction efficiency. The values tested covered a wide range of sample and solvent (CO2) flow rates. In each experimental run, two different extracted fractions and the residual nonextracted juice were obtained and characterized. Different flavonoids have been identified in the fractions obtained after CC-SFE. The possibility of using this process for antioxidant compounds enrichment is discussed.
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A03   1    @0 J. agric. food chem. : (Print)
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A06       @2 12
A08 01  1  ENG  @1 Isolation of antioxidant compounds from orange juice by using countercurrent supercritical fluid extraction (CC-SFE)
A11 01  1    @1 SENORANS (Francisco J.)
A11 02  1    @1 RUIZ-RODRIGUEZ (Alejandro)
A11 03  1    @1 CAVERO (Sofia)
A11 04  1    @1 CIFUENTES (Alejandro)
A11 05  1    @1 IBANEZ (Elena)
A11 06  1    @1 REGLERO (Guillermo)
A14 01      @1 Área de Tecnologia de Alimentos, Facultad de Ciencias, Universidad Autónoma de Madrid @2 28049 Cantoblanco, Madrid @3 ESP @Z 1 aut. @Z 2 aut. @Z 3 aut. @Z 5 aut. @Z 6 aut.
A14 02      @1 Departamento de Caracterización de Alimentos, Instituto de Fermentaciones Industriales (CSIC), Juan de la Cierva 3 @2 28006 Madrid @3 ESP @Z 4 aut.
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A21       @1 2001
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C01 01    ENG  @0 Antioxidants from orange juice are isolated by the use of countercurrent supercritical fluid extraction (CC-SFE) and characterized by reversed-phase liquid chromatography (RPLC) coupled to mass spectrometry (MS) and diode-array detection (DAD). A pilot-scale SFE plant equipped with a packed column has been employed for countercurrent extraction and fractionation of raw orange juice with carbon dioxide. Several experiments have been performed in order to study the effect of the countercurrent conditions on the content of antioxidative compounds. In this study, the main variable that has been considered is the solvent-to-feed ratio (S/F) because it plays an essential role in the extraction efficiency. The values tested covered a wide range of sample and solvent (CO2) flow rates. In each experimental run, two different extracted fractions and the residual nonextracted juice were obtained and characterized. Different flavonoids have been identified in the fractions obtained after CC-SFE. The possibility of using this process for antioxidant compounds enrichment is discussed.
C02 01  X    @0 002A35B09
C03 01  X  FRE  @0 Isolement @5 01
C03 01  X  ENG  @0 Isolation @5 01
C03 01  X  SPA  @0 Aislamiento @5 01
C03 02  X  FRE  @0 Jus d'orange @5 02
C03 02  X  ENG  @0 Orange juice @5 02
C03 02  X  SPA  @0 Zugo naranja @5 02
C03 03  X  FRE  @0 Antioxydant @5 03
C03 03  X  ENG  @0 Antioxidant @5 03
C03 03  X  SPA  @0 Antioxidante @5 03
C03 04  X  FRE  @0 Extraction SFE @5 04
C03 04  X  ENG  @0 Supercritical fluid extraction @5 04
C03 04  X  SPA  @0 Extracción fluido supercrítico @5 04
C03 05  X  FRE  @0 Procédé extraction @5 05
C03 05  X  ENG  @0 Extraction process @5 05
C03 05  X  SPA  @0 Procedimiento extracción @5 05
C03 06  X  FRE  @0 Ecoulement contre courant @5 06
C03 06  X  ENG  @0 Countercurrent flow @5 06
C03 06  X  SPA  @0 Flujo contra corriente @5 06
C03 07  X  FRE  @0 Produit alimentaire enrichi @5 07
C03 07  X  ENG  @0 Fortified product @5 07
C03 07  X  SPA  @0 Producto alimenticio enriquecido @5 07
C03 08  X  FRE  @0 Aliment santé @5 08
C03 08  X  ENG  @0 Health food @5 08
C03 08  X  SPA  @0 Alimentos sanos @5 08
C03 09  X  FRE  @0 Citrus sinensis @2 NS @5 10
C03 09  X  ENG  @0 Citrus sinensis @2 NS @5 10
C03 09  X  SPA  @0 Citrus sinensis @2 NS @5 10
C03 10  X  FRE  @0 Carbone dioxyde @2 NK @2 FX @5 15
C03 10  X  ENG  @0 Carbon dioxide @2 NK @2 FX @5 15
C03 10  X  SPA  @0 Carbono dióxido @2 NK @2 FX @5 15
C03 11  X  FRE  @0 Flavonoïde @5 16
C03 11  X  ENG  @0 Flavonoid @5 16
C03 11  X  SPA  @0 Flavonoide @5 16
C07 01  X  FRE  @0 Rutaceae @2 NS
C07 01  X  ENG  @0 Rutaceae @2 NS
C07 01  X  SPA  @0 Rutaceae @2 NS
C07 02  X  FRE  @0 Dicotyledones @2 NS
C07 02  X  ENG  @0 Dicotyledones @2 NS
C07 02  X  SPA  @0 Dicotyledones @2 NS
C07 03  X  FRE  @0 Angiospermae @2 NS
C07 03  X  ENG  @0 Angiospermae @2 NS
C07 03  X  SPA  @0 Angiospermae @2 NS
C07 04  X  FRE  @0 Spermatophyta @2 NS
C07 04  X  ENG  @0 Spermatophyta @2 NS
C07 04  X  SPA  @0 Spermatophyta @2 NS
C07 05  X  FRE  @0 Agrume @5 39
C07 05  X  ENG  @0 Citrus fruit @5 39
C07 05  X  SPA  @0 Agrios @5 39
C07 06  X  FRE  @0 Solvant @5 50
C07 06  X  ENG  @0 Solvent @5 50
C07 06  X  SPA  @0 Solvente @5 50
C07 07  X  FRE  @0 Polyphénol @5 51
C07 07  X  ENG  @0 Polyphenol @5 51
C07 07  X  SPA  @0 Polifenol @5 51
N21       @1 063
N82       @1 PSI

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Pascal:02-0115226

Le document en format XML

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<term>Extraction process</term>
<term>Flavonoid</term>
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<term>Orange juice</term>
<term>Supercritical fluid extraction</term>
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<term>Produit alimentaire enrichi</term>
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<div type="abstract" xml:lang="en">Antioxidants from orange juice are isolated by the use of countercurrent supercritical fluid extraction (CC-SFE) and characterized by reversed-phase liquid chromatography (RPLC) coupled to mass spectrometry (MS) and diode-array detection (DAD). A pilot-scale SFE plant equipped with a packed column has been employed for countercurrent extraction and fractionation of raw orange juice with carbon dioxide. Several experiments have been performed in order to study the effect of the countercurrent conditions on the content of antioxidative compounds. In this study, the main variable that has been considered is the solvent-to-feed ratio (S/F) because it plays an essential role in the extraction efficiency. The values tested covered a wide range of sample and solvent (CO
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<sub>2</sub>
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</fC03>
<fC03 i1="02" i2="X" l="SPA">
<s0>Zugo naranja</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="X" l="FRE">
<s0>Antioxydant</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG">
<s0>Antioxidant</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA">
<s0>Antioxidante</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE">
<s0>Extraction SFE</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG">
<s0>Supercritical fluid extraction</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA">
<s0>Extracción fluido supercrítico</s0>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE">
<s0>Procédé extraction</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="ENG">
<s0>Extraction process</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="SPA">
<s0>Procedimiento extracción</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE">
<s0>Ecoulement contre courant</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG">
<s0>Countercurrent flow</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA">
<s0>Flujo contra corriente</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE">
<s0>Produit alimentaire enrichi</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG">
<s0>Fortified product</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA">
<s0>Producto alimenticio enriquecido</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE">
<s0>Aliment santé</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG">
<s0>Health food</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA">
<s0>Alimentos sanos</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE">
<s0>Citrus sinensis</s0>
<s2>NS</s2>
<s5>10</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG">
<s0>Citrus sinensis</s0>
<s2>NS</s2>
<s5>10</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA">
<s0>Citrus sinensis</s0>
<s2>NS</s2>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE">
<s0>Carbone dioxyde</s0>
<s2>NK</s2>
<s2>FX</s2>
<s5>15</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG">
<s0>Carbon dioxide</s0>
<s2>NK</s2>
<s2>FX</s2>
<s5>15</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA">
<s0>Carbono dióxido</s0>
<s2>NK</s2>
<s2>FX</s2>
<s5>15</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE">
<s0>Flavonoïde</s0>
<s5>16</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG">
<s0>Flavonoid</s0>
<s5>16</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA">
<s0>Flavonoide</s0>
<s5>16</s5>
</fC03>
<fC07 i1="01" i2="X" l="FRE">
<s0>Rutaceae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="01" i2="X" l="ENG">
<s0>Rutaceae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="01" i2="X" l="SPA">
<s0>Rutaceae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="02" i2="X" l="FRE">
<s0>Dicotyledones</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="02" i2="X" l="ENG">
<s0>Dicotyledones</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="02" i2="X" l="SPA">
<s0>Dicotyledones</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="03" i2="X" l="FRE">
<s0>Angiospermae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="03" i2="X" l="ENG">
<s0>Angiospermae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="03" i2="X" l="SPA">
<s0>Angiospermae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="04" i2="X" l="FRE">
<s0>Spermatophyta</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="04" i2="X" l="ENG">
<s0>Spermatophyta</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="04" i2="X" l="SPA">
<s0>Spermatophyta</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="05" i2="X" l="FRE">
<s0>Agrume</s0>
<s5>39</s5>
</fC07>
<fC07 i1="05" i2="X" l="ENG">
<s0>Citrus fruit</s0>
<s5>39</s5>
</fC07>
<fC07 i1="05" i2="X" l="SPA">
<s0>Agrios</s0>
<s5>39</s5>
</fC07>
<fC07 i1="06" i2="X" l="FRE">
<s0>Solvant</s0>
<s5>50</s5>
</fC07>
<fC07 i1="06" i2="X" l="ENG">
<s0>Solvent</s0>
<s5>50</s5>
</fC07>
<fC07 i1="06" i2="X" l="SPA">
<s0>Solvente</s0>
<s5>50</s5>
</fC07>
<fC07 i1="07" i2="X" l="FRE">
<s0>Polyphénol</s0>
<s5>51</s5>
</fC07>
<fC07 i1="07" i2="X" l="ENG">
<s0>Polyphenol</s0>
<s5>51</s5>
</fC07>
<fC07 i1="07" i2="X" l="SPA">
<s0>Polifenol</s0>
<s5>51</s5>
</fC07>
<fN21>
<s1>063</s1>
</fN21>
<fN82>
<s1>PSI</s1>
</fN82>
</pA>
</standard>
</inist>
</record>

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   |texte=   Isolation of antioxidant compounds from orange juice by using countercurrent supercritical fluid extraction (CC-SFE)
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