Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)
Identifieur interne : 002643 ( Main/Exploration ); précédent : 002642; suivant : 002644Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)
Auteurs : Berthold Weber [Allemagne] ; Beate Hartmann [Allemagne] ; Detlef Stöckigt [Allemagne] ; Klaus Schreiber [Allemagne] ; Michael Roloff [Allemagne] ; Heinz-Jürcen Bertram [Allemagne] ; Claus O. Schmidt [Allemagne]Source :
- Journal of agricultural and food chemistry : (Print) [ 0021-8561 ] ; 2006.
Descripteurs français
- Pascal (Inist)
- Wicri :
- topic : Distillation.
English descriptors
- KwdEn :
- Chromatography, High Pressure Liquid (methods), Citrus sinensis, Citrus sinensis (chemistry), Distillation, Flavones, Flavones (analysis), Flavones (chemistry), Flavonoid, Fruit (chemistry), Gas Chromatography-Mass Spectrometry, Identification, Liquid chromatography, Magnetic Resonance Spectroscopy, Mass Spectrometry, Mass spectrometry, NMR spectrometry, Oil, Orange, Peel, Plant Oils (chemistry), Residue.
- MESH :
- chemical , analysis : Flavones.
- chemistry : Citrus sinensis, Flavones, Fruit, Plant Oils.
- methods : Chromatography, High Pressure Liquid.
- Gas Chromatography-Mass Spectrometry, Magnetic Resonance Spectroscopy, Mass Spectrometry.
Abstract
Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance techniques with ultraviolet/diode array detection were used as complementary analytical tools for the reliable identification of polymethoxylated flavones in residues from molecular distillation of cold-pressed peel oils of Citrus sinensis. After development of a liquid chromatographic separation procedure, the presence of several polymethoxy flavones such as sinensetin, nobiletin, tangeretin, quercetogetin, heptamethoxyflavone, and other derivatives was unambiguously confirmed. In addition, proceranone, an acetylated tetranortriterpenoid with limonoid structure, was identified for the first time in citrus.
Affiliations:
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KG, Corporate Research Division</s1><s2>37601 Holzminden</s2><s3>DEU</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>Allemagne</country><wicri:noRegion>37601 Holzminden</wicri:noRegion><wicri:noRegion>Corporate Research Division</wicri:noRegion><wicri:noRegion>37601 Holzminden</wicri:noRegion></affiliation></author></analytic><series><title level="j" type="main">Journal of agricultural and food chemistry : (Print)</title><title level="j" type="abbreviated">J. agric. food chem. : (Print)</title><idno type="ISSN">0021-8561</idno><imprint><date when="2006">2006</date></imprint></series></biblStruct></sourceDesc><seriesStmt><title level="j" type="main">Journal of agricultural and food chemistry : (Print)</title><title level="j" type="abbreviated">J. agric. food chem. : (Print)</title><idno type="ISSN">0021-8561</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Chromatography, High Pressure Liquid (methods)</term><term>Citrus sinensis</term><term>Citrus sinensis (chemistry)</term><term>Distillation</term><term>Flavones</term><term>Flavones (analysis)</term><term>Flavones (chemistry)</term><term>Flavonoid</term><term>Fruit (chemistry)</term><term>Gas Chromatography-Mass Spectrometry</term><term>Identification</term><term>Liquid chromatography</term><term>Magnetic Resonance Spectroscopy</term><term>Mass Spectrometry</term><term>Mass spectrometry</term><term>NMR spectrometry</term><term>Oil</term><term>Orange</term><term>Peel</term><term>Plant Oils (chemistry)</term><term>Residue</term></keywords><keywords scheme="MESH" type="chemical" qualifier="analysis" xml:lang="en"><term>Flavones</term></keywords><keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Citrus sinensis</term><term>Flavones</term><term>Fruit</term><term>Plant Oils</term></keywords><keywords scheme="MESH" qualifier="methods" xml:lang="en"><term>Chromatography, High Pressure Liquid</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Gas Chromatography-Mass Spectrometry</term><term>Magnetic Resonance Spectroscopy</term><term>Mass Spectrometry</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Chromatographie phase liquide</term><term>Spectrométrie masse</term><term>Spectrométrie RMN</term><term>Identification</term><term>Flavone</term><term>Résidu</term><term>Distillation</term><term>Flavonoïde</term><term>Orange</term><term>Pelure</term><term>Huile</term><term>Citrus sinensis</term><term>Limonoïde</term></keywords><keywords scheme="Wicri" type="topic" xml:lang="fr"><term>Distillation</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance techniques with ultraviolet/diode array detection were used as complementary analytical tools for the reliable identification of polymethoxylated flavones in residues from molecular distillation of cold-pressed peel oils of Citrus sinensis. After development of a liquid chromatographic separation procedure, the presence of several polymethoxy flavones such as sinensetin, nobiletin, tangeretin, quercetogetin, heptamethoxyflavone, and other derivatives was unambiguously confirmed. In addition, proceranone, an acetylated tetranortriterpenoid with limonoid structure, was identified for the first time in citrus.</div></front></TEI><affiliations><list><country><li>Allemagne</li></country></list><tree><country name="Allemagne"><noRegion><name sortKey="Weber, Berthold" sort="Weber, Berthold" uniqKey="Weber B" first="Berthold" last="Weber">Berthold Weber</name></noRegion><name sortKey="Bertram, Heinz Jurcen" sort="Bertram, Heinz Jurcen" uniqKey="Bertram H" first="Heinz-Jürcen" last="Bertram">Heinz-Jürcen Bertram</name><name sortKey="Hartmann, Beate" sort="Hartmann, Beate" uniqKey="Hartmann B" first="Beate" last="Hartmann">Beate Hartmann</name><name sortKey="Roloff, Michael" sort="Roloff, Michael" uniqKey="Roloff M" first="Michael" last="Roloff">Michael Roloff</name><name sortKey="Schmidt, Claus O" sort="Schmidt, Claus O" uniqKey="Schmidt C" first="Claus O." last="Schmidt">Claus O. Schmidt</name><name sortKey="Schreiber, Klaus" sort="Schreiber, Klaus" uniqKey="Schreiber K" first="Klaus" last="Schreiber">Klaus Schreiber</name><name sortKey="Stockigt, Detlef" sort="Stockigt, Detlef" uniqKey="Stockigt D" first="Detlef" last="Stöckigt">Detlef Stöckigt</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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