Study of the peak effect in pure, Pb and Pb + Y doped Bi-2212 single crystals
Identifieur interne : 00CA22 ( Main/Merge ); précédent : 00CA21; suivant : 00CA23Study of the peak effect in pure, Pb and Pb + Y doped Bi-2212 single crystals
Auteurs : X. L. Wang [Australie] ; H. K. Liu [Australie] ; S. X. Dou [Australie]Source :
- Physica. C. Superconductivity and its applications
Descripteurs français
- Pascal (Inist)
English descriptors
- KwdEn :
Abstract
The peak effect (PE) in pure, Pb and Pb + Y doped Bi2212 single crystals with different oxygen doping levels was studied by measuring M-H loops over a wide temperature range. The PE in pure Bi2212 crystals was obtained only for crystals with optimal oxygen doping and over-doping but not observed for oxygen under-doped crystals. For Pb doped Bi2212 crystals, the PE appeared at a higher field than in the pure crystals and persisted up to Tc. For (Bi1.64Pb0.36)Sr2Ca1-xYxCu2O8+y (x = 0, 0.05, 0.11, 0.33) single crystals, results show that at low temperatures, the peak field is smaller than in solely Pb doped crystals and decreases as x increases (x > 0.1). However, the peak field at high temperature for the x = 0.05 sample is higher than for heavily Pb doped Bi2212 crystals, indicative of strong pinning due to the co-doping. The formation of Bi5+ rich clusters, which cause the reduction of the c-axis lattice parameter and ρc, is proposed to be responsible for the appearance of the PE in the undoped crystals. The co-existence of Pb4+- and Bi5+-rich clusters causes the strong PE in Pb doped Bi2212 crystals. Y3+ is proposed to be an effective dopant at low doping levels for flux pinning at high temperatures. The PE for all the crystals was characterised by plotting (Hmax -Hmin)/Hmax vs T/Tc, where Hmin and Hmax represent the fields at which the magnetisation starts to increase (Hmin) and reaches a maximum (Hmax) at the peak position. Results showed that the evolution of the peak effect with temperature in the Pb and Pb + Y doped crystals was similar to that seen in Y123.
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Study of the peak effect in pure, Pb and Pb + Y doped Bi-2212 single crystals</title>
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<term>Calcium oxides</term>
<term>Composition effect</term>
<term>Copper oxides</term>
<term>Experimental study</term>
<term>Flux pinning</term>
<term>High-Tc superconductors</term>
<term>Lead oxides</term>
<term>Magnetic hysteresis</term>
<term>Magnetization</term>
<term>Monocrystals</term>
<term>Nonstoichiometry</term>
<term>Peak effect</term>
<term>Strontium oxides</term>
<term>Temperature dependence</term>
<term>Yttrium oxides</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Effet pic</term>
<term>Non stoechiométrie</term>
<term>Hystérésis magnétique</term>
<term>Dépendance température</term>
<term>Aimantation</term>
<term>Effet composition</term>
<term>Ancrage flux</term>
<term>Supraconducteur haute température</term>
<term>Monocristal</term>
<term>Bismuth oxyde</term>
<term>Calcium oxyde</term>
<term>Plomb oxyde</term>
<term>Cuivre oxyde</term>
<term>Strontium oxyde</term>
<term>Yttrium oxyde</term>
<term>Etude expérimentale</term>
<term>7425H</term>
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<front><div type="abstract" xml:lang="en">The peak effect (PE) in pure, Pb and Pb + Y doped Bi2212 single crystals with different oxygen doping levels was studied by measuring M-H loops over a wide temperature range. The PE in pure Bi2212 crystals was obtained only for crystals with optimal oxygen doping and over-doping but not observed for oxygen under-doped crystals. For Pb doped Bi2212 crystals, the PE appeared at a higher field than in the pure crystals and persisted up to T<sub>c</sub>
. For (Bi<sub>1.64</sub>
Pb<sub>0.36</sub>
)Sr<sub>2</sub>
Ca<sub>1-x</sub>
Y<sub>x</sub>
Cu<sub>2</sub>
O<sub>8+y</sub>
(x = 0, 0.05, 0.11, 0.33) single crystals, results show that at low temperatures, the peak field is smaller than in solely Pb doped crystals and decreases as x increases (x > 0.1). However, the peak field at high temperature for the x = 0.05 sample is higher than for heavily Pb doped Bi2212 crystals, indicative of strong pinning due to the co-doping. The formation of Bi<sup>5+</sup>
rich clusters, which cause the reduction of the c-axis lattice parameter and ρ<sub>c</sub>
, is proposed to be responsible for the appearance of the PE in the undoped crystals. The co-existence of Pb<sup>4+</sup>
- and Bi<sup>5+</sup>
-rich clusters causes the strong PE in Pb doped Bi2212 crystals. Y<sup>3+</sup>
is proposed to be an effective dopant at low doping levels for flux pinning at high temperatures. The PE for all the crystals was characterised by plotting (H<sub>max</sub>
-H<sub>min</sub>
)/H<sub>max</sub>
vs T/T<sub>c</sub>
, where H<sub>min</sub>
and H<sub>max</sub>
represent the fields at which the magnetisation starts to increase (H<sub>min</sub>
) and reaches a maximum (H<sub>max</sub>
) at the peak position. Results showed that the evolution of the peak effect with temperature in the Pb and Pb + Y doped crystals was similar to that seen in Y123.</div>
</front>
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<affiliations><list><country><li>Australie</li>
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<name sortKey="Dou, S X" sort="Dou, S X" uniqKey="Dou S" first="S. X." last="Dou">S. X. Dou</name>
<name sortKey="Liu, H K" sort="Liu, H K" uniqKey="Liu H" first="H. K." last="Liu">H. K. Liu</name>
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