AustralieFrV1, Main, Exploration, bibRecord, 006A64

Growth of nanotubes on zirconium in glycerol/fluoride electrolytes

Identifieur interne : 006A64 ( Main/Exploration ); précédent : 006A63; suivant : 006A65

Growth of nanotubes on zirconium in glycerol/fluoride electrolytes

Auteurs : F. Muratore [Royaume-Uni] ; A. Baron-Wiechec [Royaume-Uni] ; T. Hashimoto [Royaume-Uni] ; A. Gholinia [Royaume-Uni] ; P. Skeldon [Royaume-Uni] ; G. E. Thompson [Royaume-Uni]

Source :

Electrochimica acta [ 0013-4686 ] ; 2011.

RBID : Pascal:12-0325080

Descripteurs français

Pascal (Inist)
- Ammonium Fluorure, Nanotube, Zirconium, Glycérol, Anodisation, Microscopie électronique transmission, Oxyde anodique, Faisceau ionique, Microscopie électronique balayage, Microscopie électronique, RBS, Analyse réaction nucléaire, Morphologie, Structure surface, 8107D.

English descriptors

KwdEn :
- Ammonium Fluorides, Anodic oxide, Anodizing, Electron microscopy, Glycerol, Ion beam, Morphology, Nanotubes, Nuclear reaction analysis, RBS, Scanning electron microscopy, Surface structure, Transmission electron microscopy, Zirconium.

Abstract

The study examines anodic films formed on bulk and sputtered zirconium in ammonium fluoride/glycerol electrolyte with up to 5 vol.% added water, using film cross-sections prepared by focused ion beam and ultramicrotomy. The findings indicate porous films consisting of zirconium fluoride surrounding zirconia-based nanotubes. The fluoride arises due to faster migration of F^- ions relative to O^2- ions; its dissolution exposes the nanotubes. Ion beam analyses revealed the highest amount of fluorine for films formed in electrolyte with no water addition. ¹⁸O tracer indicated that water was the primary source of oxygen in the films, which grew at an efficiency of ∼80%.

Affiliations:

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Le document en format XML

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<series><title level="j" type="main">Electrochimica acta</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Ammonium Fluorides</term>
<term>Anodic oxide</term>
<term>Anodizing</term>
<term>Electron microscopy</term>
<term>Glycerol</term>
<term>Ion beam</term>
<term>Morphology</term>
<term>Nanotubes</term>
<term>Nuclear reaction analysis</term>
<term>RBS</term>
<term>Scanning electron microscopy</term>
<term>Surface structure</term>
<term>Transmission electron microscopy</term>
<term>Zirconium</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Ammonium Fluorure</term>
<term>Nanotube</term>
<term>Zirconium</term>
<term>Glycérol</term>
<term>Anodisation</term>
<term>Microscopie électronique transmission</term>
<term>Oxyde anodique</term>
<term>Faisceau ionique</term>
<term>Microscopie électronique balayage</term>
<term>Microscopie électronique</term>
<term>RBS</term>
<term>Analyse réaction nucléaire</term>
<term>Morphologie</term>
<term>Structure surface</term>
<term>8107D</term>
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</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">The study examines anodic films formed on bulk and sputtered zirconium in ammonium fluoride/glycerol electrolyte with up to 5 vol.% added water, using film cross-sections prepared by focused ion beam and ultramicrotomy. The findings indicate porous films consisting of zirconium fluoride surrounding zirconia-based nanotubes. The fluoride arises due to faster migration of F<sup>-</sup>
 ions relative to O<sup>2-</sup>
 ions; its dissolution exposes the nanotubes. Ion beam analyses revealed the highest amount of fluorine for films formed in electrolyte with no water addition. <sup>18</sup>
O tracer indicated that water was the primary source of oxygen in the films, which grew at an efficiency of ∼80%.</div>
</front>
</TEI>
<affiliations><list><country><li>Royaume-Uni</li>
</country>
<region><li>Angleterre</li>
<li>Grand Manchester</li>
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<tree><country name="Royaume-Uni"><region name="Angleterre"><name sortKey="Muratore, F" sort="Muratore, F" uniqKey="Muratore F" first="F." last="Muratore">F. Muratore</name>
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<name sortKey="Baron Wiechec, A" sort="Baron Wiechec, A" uniqKey="Baron Wiechec A" first="A." last="Baron-Wiechec">A. Baron-Wiechec</name>
<name sortKey="Gholinia, A" sort="Gholinia, A" uniqKey="Gholinia A" first="A." last="Gholinia">A. Gholinia</name>
<name sortKey="Hashimoto, T" sort="Hashimoto, T" uniqKey="Hashimoto T" first="T." last="Hashimoto">T. Hashimoto</name>
<name sortKey="Skeldon, P" sort="Skeldon, P" uniqKey="Skeldon P" first="P." last="Skeldon">P. Skeldon</name>
<name sortKey="Thompson, G E" sort="Thompson, G E" uniqKey="Thompson G" first="G. E." last="Thompson">G. E. Thompson</name>
</country>
</tree>
</affiliations>
</record>

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Growth of nanotubes on zirconium in glycerol/fluoride electrolytes

Growth of nanotubes on zirconium in glycerol/fluoride electrolytes

Source :

Descripteurs français

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri