AustralieFrV1, PascalFrancis, Corpus, bibRecord, 001172

Growth of nanotubes on zirconium in glycerol/fluoride electrolytes

Identifieur interne : 001172 ( PascalFrancis/Corpus ); précédent : 001171; suivant : 001173

Growth of nanotubes on zirconium in glycerol/fluoride electrolytes

Auteurs : F. Muratore ; A. Baron-Wiechec ; T. Hashimoto ; A. Gholinia ; P. Skeldon ; G. E. Thompson

Source :

Electrochimica acta [ 0013-4686 ] ; 2011.

RBID : Pascal:12-0325080

Descripteurs français

Pascal (Inist)
- Ammonium Fluorure, Nanotube, Zirconium, Glycérol, Anodisation, Microscopie électronique transmission, Oxyde anodique, Faisceau ionique, Microscopie électronique balayage, Microscopie électronique, RBS, Analyse réaction nucléaire, Morphologie, Structure surface, 8107D.

English descriptors

KwdEn :
- Ammonium Fluorides, Anodic oxide, Anodizing, Electron microscopy, Glycerol, Ion beam, Morphology, Nanotubes, Nuclear reaction analysis, RBS, Scanning electron microscopy, Surface structure, Transmission electron microscopy, Zirconium.

Abstract

The study examines anodic films formed on bulk and sputtered zirconium in ammonium fluoride/glycerol electrolyte with up to 5 vol.% added water, using film cross-sections prepared by focused ion beam and ultramicrotomy. The findings indicate porous films consisting of zirconium fluoride surrounding zirconia-based nanotubes. The fluoride arises due to faster migration of F^- ions relative to O^2- ions; its dissolution exposes the nanotubes. Ion beam analyses revealed the highest amount of fluorine for films formed in electrolyte with no water addition. ¹⁸O tracer indicated that water was the primary source of oxygen in the films, which grew at an efficiency of ∼80%.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

A01	`01`	`1`		`@0 0013-4686`
A02	`01`			`@0 ELCAAV`
A03		`1`		`@0 Electrochim. acta`
A05				`@2 56`
A06				`@2 28`
A08	`01`	`1`	`ENG`	`@1 Growth of nanotubes on zirconium in glycerol/fluoride electrolytes`
A09	`01`	`1`	`ENG`	`@1 Electrochemistry from Biology to Physics`
A11	`01`	`1`		`@1 MURATORE (F.)`
A11	`02`	`1`		`@1 BARON-WIECHEC (A.)`
A11	`03`	`1`		`@1 HASHIMOTO (T.)`
A11	`04`	`1`		`@1 GHOLINIA (A.)`
A11	`05`	`1`		`@1 SKELDON (P.)`
A11	`06`	`1`		`@1 THOMPSON (G. E.)`
A12	`01`	`1`		`@1 BERGEL (A.) @9 ed.`
A12	`02`	`1`		`@1 BOND (A. M.) @9 ed.`
A12	`03`	`1`		`@1 BRANKOVIC (S.) @9 ed.`
A12	`04`	`1`		`@1 BULTEL (Y.) @9 ed.`
A12	`05`	`1`		`@1 DI QUARTO (F.) @9 ed.`
A12	`06`	`1`		`@1 GORTON (L.) @9 ed.`
A12	`07`	`1`		`@1 INZELT (G.) @9 ed.`
A12	`08`	`1`		`@1 LAPICQUE (F.) @9 ed.`
A12	`09`	`1`		`@1 LISDAT (F.) @9 ed.`
A12	`10`	`1`		`@1 OPALLO (M.) @9 ed.`
A12	`11`	`1`		`@1 SAVINOVA (E. R.) @9 ed.`
A12	`12`	`1`		`@1 TOH (C.S.) @9 ed.`
A12	`13`	`1`		`@1 TSIRLINA (G. A.) @9 ed.`
A12	`14`	`1`		`@1 VIVIER (V.) @9 ed.`
A12	`15`	`1`		`@1 WINTER (M.) @9 ed.`
A14	`01`			`@1 Corrosion and Protection Centre, School of Materials, The University of Manchester, Sackville St. @2 Manchester M13 9PL @3 GBR @Z 1 aut. @Z 2 aut. @Z 3 aut. @Z 4 aut. @Z 5 aut. @Z 6 aut.`
A15	`01`			`@1 CNRS @2 Toulouse @3 FRA @Z 1 aut.`
A15	`02`			`@1 Monash University @2 Clayton, Vic. @3 AUS @Z 2 aut.`
A15	`03`			`@1 University of Houston @2 Houston, TX @3 USA @Z 3 aut.`
A15	`04`			`@1 LEPMI @2 Grenoble @3 FRA @Z 4 aut.`
A15	`05`			`@1 University of Palermo @3 ITA @Z 5 aut.`
A15	`06`			`@1 Lund University @3 SWE @Z 6 aut.`
A15	`07`			`@1 Eotvos Lorand University @2 Budapest @3 HUN @Z 7 aut.`
A15	`08`			`@1 CNRS @2 Nancy @3 FRA @Z 8 aut.`
A15	`09`			`@1 Wildau University @3 DEU @Z 9 aut.`
A15	`10`			`@1 Polish Academy of Sciences @2 Warsaw @3 POL @Z 10 aut.`
A15	`11`			`@1 Université de Strasbourg @3 FRA @Z 11 aut.`
A15	`12`			`@1 Nanyang Technological University @3 SGP @Z 12 aut.`
A15	`13`			`@1 Moscow State University @3 RUS @Z 13 aut.`
A15	`14`			`@1 Université Pierre et Marie Curie @2 Paris @3 FRA @Z 14 aut.`
A15	`15`			`@1 University of Münster @3 DEU @Z 15 aut.`
A18	`01`	`1`		`@1 International Society of Electrochemistry (ISE) @2 1004 Lausanne @3 CHE @9 org-cong.`
A20				`@1 10500-10506`
A21				`@1 2011`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 1516 @5 354000505919820250`
A44				`@0 0000 @1 © 2012 INIST-CNRS. All rights reserved.`
A45				`@0 34 ref.`
A47	`01`	`1`		`@0 12-0325080`
A60				`@1 P @2 C`
A61				`@0 A`
A64	`01`	`1`		`@0 Electrochimica acta`
A66	`01`			`@0 GBR`
C01	`01`		`ENG`	@0 The study examines anodic films formed on bulk and sputtered zirconium in ammonium fluoride/glycerol electrolyte with up to 5 vol.% added water, using film cross-sections prepared by focused ion beam and ultramicrotomy. The findings indicate porous films consisting of zirconium fluoride surrounding zirconia-based nanotubes. The fluoride arises due to faster migration of F^- ions relative to O^2- ions; its dissolution exposes the nanotubes. Ion beam analyses revealed the highest amount of fluorine for films formed in electrolyte with no water addition. ¹⁸O tracer indicated that water was the primary source of oxygen in the films, which grew at an efficiency of ∼80%.
C02	`01`	`3`		`@0 001B80A07D`
C03	`01`	`X`	`FRE`	`@0 Ammonium Fluorure @1 SOL @2 NC @2 NA @2 FX @5 01`
C03	`01`	`X`	`ENG`	`@0 Ammonium Fluorides @1 SOL @2 NC @2 NA @2 FX @5 01`
C03	`01`	`X`	`SPA`	`@0 Amonio Fluoruro @1 SOL @2 NC @2 NA @2 FX @5 01`
C03	`02`	`3`	`FRE`	`@0 Nanotube @5 02`
C03	`02`	`3`	`ENG`	`@0 Nanotubes @5 02`
C03	`03`	`3`	`FRE`	`@0 Zirconium @2 NC @5 03`
C03	`03`	`3`	`ENG`	`@0 Zirconium @2 NC @5 03`
C03	`04`	`3`	`FRE`	`@0 Glycérol @1 SOL @2 NK @5 04`
C03	`04`	`3`	`ENG`	`@0 Glycerol @1 SOL @2 NK @5 04`
C03	`05`	`3`	`FRE`	`@0 Anodisation @5 05`
C03	`05`	`3`	`ENG`	`@0 Anodizing @5 05`
C03	`06`	`3`	`FRE`	`@0 Microscopie électronique transmission @5 06`
C03	`06`	`3`	`ENG`	`@0 Transmission electron microscopy @5 06`
C03	`07`	`3`	`FRE`	`@0 Oxyde anodique @5 07`
C03	`07`	`3`	`ENG`	`@0 Anodic oxide @5 07`
C03	`08`	`X`	`FRE`	`@0 Faisceau ionique @5 08`
C03	`08`	`X`	`ENG`	`@0 Ion beam @5 08`
C03	`08`	`X`	`SPA`	`@0 Haz iónico @5 08`
C03	`09`	`3`	`FRE`	`@0 Microscopie électronique balayage @5 09`
C03	`09`	`3`	`ENG`	`@0 Scanning electron microscopy @5 09`
C03	`10`	`3`	`FRE`	`@0 Microscopie électronique @5 10`
C03	`10`	`3`	`ENG`	`@0 Electron microscopy @5 10`
C03	`11`	`3`	`FRE`	`@0 RBS @5 11`
C03	`11`	`3`	`ENG`	`@0 RBS @5 11`
C03	`12`	`3`	`FRE`	`@0 Analyse réaction nucléaire @5 12`
C03	`12`	`3`	`ENG`	`@0 Nuclear reaction analysis @5 12`
C03	`13`	`3`	`FRE`	`@0 Morphologie @5 32`
C03	`13`	`3`	`ENG`	`@0 Morphology @5 32`
C03	`14`	`3`	`FRE`	`@0 Structure surface @5 33`
C03	`14`	`3`	`ENG`	`@0 Surface structure @5 33`
C03	`15`	`3`	`FRE`	`@0 8107D @2 PAC @4 INC @5 76`
C07	`01`	`3`	`FRE`	`@0 Métal transition @5 53`
C07	`01`	`3`	`ENG`	`@0 Transition elements @5 53`
N21				`@1 247`

A30	`01`	`1`	`ENG`	`@1 International Society of Electrochemistry (ISE) Meeting @2 61 @3 Nice FRA @4 2010-09-26`

Format Inist (serveur)

NO :	PASCAL 12-0325080 INIST
ET :	Growth of nanotubes on zirconium in glycerol/fluoride electrolytes
AU :	MURATORE (F.); BARON-WIECHEC (A.); HASHIMOTO (T.); GHOLINIA (A.); SKELDON (P.); THOMPSON (G. E.); BERGEL (A.); BOND (A. M.); BRANKOVIC (S.); BULTEL (Y.); DI QUARTO (F.); GORTON (L.); INZELT (G.); LAPICQUE (F.); LISDAT (F.); OPALLO (M.); SAVINOVA (E. R.); TOH (C.S.); TSIRLINA (G. A.); VIVIER (V.); WINTER (M.)
AF :	Corrosion and Protection Centre, School of Materials, The University of Manchester, Sackville St./Manchester M13 9PL/Royaume-Uni (1 aut., 2 aut., 3 aut., 4 aut., 5 aut., 6 aut.); CNRS/Toulouse/France (1 aut.); Monash University/Clayton, Vic./Australie (2 aut.); University of Houston/Houston, TX/Etats-Unis (3 aut.); LEPMI/Grenoble/France (4 aut.); University of Palermo/Italie (5 aut.); Lund University/Suède (6 aut.); Eotvos Lorand University/Budapest/Hongrie (7 aut.); CNRS/Nancy/France (8 aut.); Wildau University/Allemagne (9 aut.); Polish Academy of Sciences/Warsaw/Pologne (10 aut.); Université de Strasbourg/France (11 aut.); Nanyang Technological University/Singapour (12 aut.); Moscow State University/Russie (13 aut.); Université Pierre et Marie Curie/Paris/France (14 aut.); University of Münster/Allemagne (15 aut.)
DT :	Publication en série; Congrès; Niveau analytique
SO :	Electrochimica acta; ISSN 0013-4686; Coden ELCAAV; Royaume-Uni; Da. 2011; Vol. 56; No. 28; Pp. 10500-10506; Bibl. 34 ref.
LA :	Anglais
EA :	The study examines anodic films formed on bulk and sputtered zirconium in ammonium fluoride/glycerol electrolyte with up to 5 vol.% added water, using film cross-sections prepared by focused ion beam and ultramicrotomy. The findings indicate porous films consisting of zirconium fluoride surrounding zirconia-based nanotubes. The fluoride arises due to faster migration of F^- ions relative to O^2- ions; its dissolution exposes the nanotubes. Ion beam analyses revealed the highest amount of fluorine for films formed in electrolyte with no water addition. ¹⁸O tracer indicated that water was the primary source of oxygen in the films, which grew at an efficiency of ∼80%.
CC :	001B80A07D
FD :	Ammonium Fluorure; Nanotube; Zirconium; Glycérol; Anodisation; Microscopie électronique transmission; Oxyde anodique; Faisceau ionique; Microscopie électronique balayage; Microscopie électronique; RBS; Analyse réaction nucléaire; Morphologie; Structure surface; 8107D
FG :	Métal transition
ED :	Ammonium Fluorides; Nanotubes; Zirconium; Glycerol; Anodizing; Transmission electron microscopy; Anodic oxide; Ion beam; Scanning electron microscopy; Electron microscopy; RBS; Nuclear reaction analysis; Morphology; Surface structure
EG :	Transition elements
SD :	Amonio Fluoruro; Haz iónico
LO :	INIST-1516.354000505919820250
ID :	12-0325080

Links to Exploration step

Pascal:12-0325080

Le document en format XML

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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Ammonium Fluorides</term>
<term>Anodic oxide</term>
<term>Anodizing</term>
<term>Electron microscopy</term>
<term>Glycerol</term>
<term>Ion beam</term>
<term>Morphology</term>
<term>Nanotubes</term>
<term>Nuclear reaction analysis</term>
<term>RBS</term>
<term>Scanning electron microscopy</term>
<term>Surface structure</term>
<term>Transmission electron microscopy</term>
<term>Zirconium</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Ammonium Fluorure</term>
<term>Nanotube</term>
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<term>Microscopie électronique transmission</term>
<term>Oxyde anodique</term>
<term>Faisceau ionique</term>
<term>Microscopie électronique balayage</term>
<term>Microscopie électronique</term>
<term>RBS</term>
<term>Analyse réaction nucléaire</term>
<term>Morphologie</term>
<term>Structure surface</term>
<term>8107D</term>
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<front><div type="abstract" xml:lang="en">The study examines anodic films formed on bulk and sputtered zirconium in ammonium fluoride/glycerol electrolyte with up to 5 vol.% added water, using film cross-sections prepared by focused ion beam and ultramicrotomy. The findings indicate porous films consisting of zirconium fluoride surrounding zirconia-based nanotubes. The fluoride arises due to faster migration of F<sup>-</sup>
 ions relative to O<sup>2-</sup>
 ions; its dissolution exposes the nanotubes. Ion beam analyses revealed the highest amount of fluorine for films formed in electrolyte with no water addition. <sup>18</sup>
O tracer indicated that water was the primary source of oxygen in the films, which grew at an efficiency of ∼80%.</div>
</front>
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<fA08 i1="01" i2="1" l="ENG"><s1>Growth of nanotubes on zirconium in glycerol/fluoride electrolytes</s1>
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</fA11>
<fA11 i1="04" i2="1"><s1>GHOLINIA (A.)</s1>
</fA11>
<fA11 i1="05" i2="1"><s1>SKELDON (P.)</s1>
</fA11>
<fA11 i1="06" i2="1"><s1>THOMPSON (G. E.)</s1>
</fA11>
<fA12 i1="01" i2="1"><s1>BERGEL (A.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="02" i2="1"><s1>BOND (A. M.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="03" i2="1"><s1>BRANKOVIC (S.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="04" i2="1"><s1>BULTEL (Y.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="05" i2="1"><s1>DI QUARTO (F.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="06" i2="1"><s1>GORTON (L.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="07" i2="1"><s1>INZELT (G.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="08" i2="1"><s1>LAPICQUE (F.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="09" i2="1"><s1>LISDAT (F.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="10" i2="1"><s1>OPALLO (M.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="11" i2="1"><s1>SAVINOVA (E. R.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="12" i2="1"><s1>TOH (C.S.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="13" i2="1"><s1>TSIRLINA (G. A.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="14" i2="1"><s1>VIVIER (V.)</s1>
<s9>ed.</s9>
</fA12>
<fA12 i1="15" i2="1"><s1>WINTER (M.)</s1>
<s9>ed.</s9>
</fA12>
<fA14 i1="01"><s1>Corrosion and Protection Centre, School of Materials, The University of Manchester, Sackville St.</s1>
<s2>Manchester M13 9PL</s2>
<s3>GBR</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
<sZ>6 aut.</sZ>
</fA14>
<fA15 i1="01"><s1>CNRS</s1>
<s2>Toulouse</s2>
<s3>FRA</s3>
<sZ>1 aut.</sZ>
</fA15>
<fA15 i1="02"><s1>Monash University</s1>
<s2>Clayton, Vic.</s2>
<s3>AUS</s3>
<sZ>2 aut.</sZ>
</fA15>
<fA15 i1="03"><s1>University of Houston</s1>
<s2>Houston, TX</s2>
<s3>USA</s3>
<sZ>3 aut.</sZ>
</fA15>
<fA15 i1="04"><s1>LEPMI</s1>
<s2>Grenoble</s2>
<s3>FRA</s3>
<sZ>4 aut.</sZ>
</fA15>
<fA15 i1="05"><s1>University of Palermo</s1>
<s3>ITA</s3>
<sZ>5 aut.</sZ>
</fA15>
<fA15 i1="06"><s1>Lund University</s1>
<s3>SWE</s3>
<sZ>6 aut.</sZ>
</fA15>
<fA15 i1="07"><s1>Eotvos Lorand University</s1>
<s2>Budapest</s2>
<s3>HUN</s3>
<sZ>7 aut.</sZ>
</fA15>
<fA15 i1="08"><s1>CNRS</s1>
<s2>Nancy</s2>
<s3>FRA</s3>
<sZ>8 aut.</sZ>
</fA15>
<fA15 i1="09"><s1>Wildau University</s1>
<s3>DEU</s3>
<sZ>9 aut.</sZ>
</fA15>
<fA15 i1="10"><s1>Polish Academy of Sciences</s1>
<s2>Warsaw</s2>
<s3>POL</s3>
<sZ>10 aut.</sZ>
</fA15>
<fA15 i1="11"><s1>Université de Strasbourg</s1>
<s3>FRA</s3>
<sZ>11 aut.</sZ>
</fA15>
<fA15 i1="12"><s1>Nanyang Technological University</s1>
<s3>SGP</s3>
<sZ>12 aut.</sZ>
</fA15>
<fA15 i1="13"><s1>Moscow State University</s1>
<s3>RUS</s3>
<sZ>13 aut.</sZ>
</fA15>
<fA15 i1="14"><s1>Université Pierre et Marie Curie</s1>
<s2>Paris</s2>
<s3>FRA</s3>
<sZ>14 aut.</sZ>
</fA15>
<fA15 i1="15"><s1>University of Münster</s1>
<s3>DEU</s3>
<sZ>15 aut.</sZ>
</fA15>
<fA18 i1="01" i2="1"><s1>International Society of Electrochemistry (ISE)</s1>
<s2>1004 Lausanne</s2>
<s3>CHE</s3>
<s9>org-cong.</s9>
</fA18>
<fA20><s1>10500-10506</s1>
</fA20>
<fA21><s1>2011</s1>
</fA21>
<fA23 i1="01"><s0>ENG</s0>
</fA23>
<fA43 i1="01"><s1>INIST</s1>
<s2>1516</s2>
<s5>354000505919820250</s5>
</fA43>
<fA44><s0>0000</s0>
<s1>© 2012 INIST-CNRS. All rights reserved.</s1>
</fA44>
<fA45><s0>34 ref.</s0>
</fA45>
<fA47 i1="01" i2="1"><s0>12-0325080</s0>
</fA47>
<fA60><s1>P</s1>
<s2>C</s2>
</fA60>
<fA61><s0>A</s0>
</fA61>
<fA64 i1="01" i2="1"><s0>Electrochimica acta</s0>
</fA64>
<fA66 i1="01"><s0>GBR</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>The study examines anodic films formed on bulk and sputtered zirconium in ammonium fluoride/glycerol electrolyte with up to 5 vol.% added water, using film cross-sections prepared by focused ion beam and ultramicrotomy. The findings indicate porous films consisting of zirconium fluoride surrounding zirconia-based nanotubes. The fluoride arises due to faster migration of F<sup>-</sup>
 ions relative to O<sup>2-</sup>
 ions; its dissolution exposes the nanotubes. Ion beam analyses revealed the highest amount of fluorine for films formed in electrolyte with no water addition. <sup>18</sup>
O tracer indicated that water was the primary source of oxygen in the films, which grew at an efficiency of ∼80%.</s0>
</fC01>
<fC02 i1="01" i2="3"><s0>001B80A07D</s0>
</fC02>
<fC03 i1="01" i2="X" l="FRE"><s0>Ammonium Fluorure</s0>
<s1>SOL</s1>
<s2>NC</s2>
<s2>NA</s2>
<s2>FX</s2>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="ENG"><s0>Ammonium Fluorides</s0>
<s1>SOL</s1>
<s2>NC</s2>
<s2>NA</s2>
<s2>FX</s2>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="SPA"><s0>Amonio Fluoruro</s0>
<s1>SOL</s1>
<s2>NC</s2>
<s2>NA</s2>
<s2>FX</s2>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="3" l="FRE"><s0>Nanotube</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="3" l="ENG"><s0>Nanotubes</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="3" l="FRE"><s0>Zirconium</s0>
<s2>NC</s2>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG"><s0>Zirconium</s0>
<s2>NC</s2>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE"><s0>Glycérol</s0>
<s1>SOL</s1>
<s2>NK</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG"><s0>Glycerol</s0>
<s1>SOL</s1>
<s2>NK</s2>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE"><s0>Anodisation</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG"><s0>Anodizing</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="3" l="FRE"><s0>Microscopie électronique transmission</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="3" l="ENG"><s0>Transmission electron microscopy</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE"><s0>Oxyde anodique</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="3" l="ENG"><s0>Anodic oxide</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Faisceau ionique</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG"><s0>Ion beam</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Haz iónico</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>Microscopie électronique balayage</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG"><s0>Scanning electron microscopy</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE"><s0>Microscopie électronique</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG"><s0>Electron microscopy</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>RBS</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>RBS</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE"><s0>Analyse réaction nucléaire</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG"><s0>Nuclear reaction analysis</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE"><s0>Morphologie</s0>
<s5>32</s5>
</fC03>
<fC03 i1="13" i2="3" l="ENG"><s0>Morphology</s0>
<s5>32</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE"><s0>Structure surface</s0>
<s5>33</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG"><s0>Surface structure</s0>
<s5>33</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE"><s0>8107D</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>76</s5>
</fC03>
<fC07 i1="01" i2="3" l="FRE"><s0>Métal transition</s0>
<s5>53</s5>
</fC07>
<fC07 i1="01" i2="3" l="ENG"><s0>Transition elements</s0>
<s5>53</s5>
</fC07>
<fN21><s1>247</s1>
</fN21>
</pA>
<pR><fA30 i1="01" i2="1" l="ENG"><s1>International Society of Electrochemistry (ISE) Meeting</s1>
<s2>61</s2>
<s3>Nice FRA</s3>
<s4>2010-09-26</s4>
</fA30>
</pR>
</standard>
<server><NO>PASCAL 12-0325080 INIST</NO>
<ET>Growth of nanotubes on zirconium in glycerol/fluoride electrolytes</ET>
<AU>MURATORE (F.); BARON-WIECHEC (A.); HASHIMOTO (T.); GHOLINIA (A.); SKELDON (P.); THOMPSON (G. E.); BERGEL (A.); BOND (A. M.); BRANKOVIC (S.); BULTEL (Y.); DI QUARTO (F.); GORTON (L.); INZELT (G.); LAPICQUE (F.); LISDAT (F.); OPALLO (M.); SAVINOVA (E. R.); TOH (C.S.); TSIRLINA (G. A.); VIVIER (V.); WINTER (M.)</AU>
<AF>Corrosion and Protection Centre, School of Materials, The University of Manchester, Sackville St./Manchester M13 9PL/Royaume-Uni (1 aut., 2 aut., 3 aut., 4 aut., 5 aut., 6 aut.); CNRS/Toulouse/France (1 aut.); Monash University/Clayton, Vic./Australie (2 aut.); University of Houston/Houston, TX/Etats-Unis (3 aut.); LEPMI/Grenoble/France (4 aut.); University of Palermo/Italie (5 aut.); Lund University/Suède (6 aut.); Eotvos Lorand University/Budapest/Hongrie (7 aut.); CNRS/Nancy/France (8 aut.); Wildau University/Allemagne (9 aut.); Polish Academy of Sciences/Warsaw/Pologne (10 aut.); Université de Strasbourg/France (11 aut.); Nanyang Technological University/Singapour (12 aut.); Moscow State University/Russie (13 aut.); Université Pierre et Marie Curie/Paris/France (14 aut.); University of Münster/Allemagne (15 aut.)</AF>
<DT>Publication en série; Congrès; Niveau analytique</DT>
<SO>Electrochimica acta; ISSN 0013-4686; Coden ELCAAV; Royaume-Uni; Da. 2011; Vol. 56; No. 28; Pp. 10500-10506; Bibl. 34 ref.</SO>
<LA>Anglais</LA>
<EA>The study examines anodic films formed on bulk and sputtered zirconium in ammonium fluoride/glycerol electrolyte with up to 5 vol.% added water, using film cross-sections prepared by focused ion beam and ultramicrotomy. The findings indicate porous films consisting of zirconium fluoride surrounding zirconia-based nanotubes. The fluoride arises due to faster migration of F<sup>-</sup>
 ions relative to O<sup>2-</sup>
 ions; its dissolution exposes the nanotubes. Ion beam analyses revealed the highest amount of fluorine for films formed in electrolyte with no water addition. <sup>18</sup>
O tracer indicated that water was the primary source of oxygen in the films, which grew at an efficiency of ∼80%.</EA>
<CC>001B80A07D</CC>
<FD>Ammonium Fluorure; Nanotube; Zirconium; Glycérol; Anodisation; Microscopie électronique transmission; Oxyde anodique; Faisceau ionique; Microscopie électronique balayage; Microscopie électronique; RBS; Analyse réaction nucléaire; Morphologie; Structure surface; 8107D</FD>
<FG>Métal transition</FG>
<ED>Ammonium Fluorides; Nanotubes; Zirconium; Glycerol; Anodizing; Transmission electron microscopy; Anodic oxide; Ion beam; Scanning electron microscopy; Electron microscopy; RBS; Nuclear reaction analysis; Morphology; Surface structure</ED>
<EG>Transition elements</EG>
<SD>Amonio Fluoruro; Haz iónico</SD>
<LO>INIST-1516.354000505919820250</LO>
<ID>12-0325080</ID>
</server>
</inist>
</record>

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Growth of nanotubes on zirconium in glycerol/fluoride electrolytes

Growth of nanotubes on zirconium in glycerol/fluoride electrolytes

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