OrangerV1, PascalFrancis, Corpus, bibRecord, 000589

Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)

Identifieur interne : 000589 ( PascalFrancis/Corpus ); précédent : 000588; suivant : 000590

Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)

Auteurs : Berthold Weber ; Beate Hartmann ; Detlef Stöckigt ; Klaus Schreiber ; Michael Roloff ; Heinz-Jürcen Bertram ; Claus O. Schmidt

Source :

Journal of agricultural and food chemistry : (Print) [ 0021-8561 ] ; 2006.

RBID : Pascal:06-0098010

Descripteurs français

Pascal (Inist)
- Chromatographie phase liquide, Spectrométrie masse, Spectrométrie RMN, Identification, Flavone, Résidu, Distillation, Flavonoïde, Orange, Pelure, Huile, Citrus sinensis, Limonoïde.

English descriptors

KwdEn :
- Citrus sinensis, Distillation, Flavones, Flavonoid, Identification, Liquid chromatography, Mass spectrometry, NMR spectrometry, Oil, Orange, Peel, Residue.

Abstract

Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance techniques with ultraviolet/diode array detection were used as complementary analytical tools for the reliable identification of polymethoxylated flavones in residues from molecular distillation of cold-pressed peel oils of Citrus sinensis. After development of a liquid chromatographic separation procedure, the presence of several polymethoxy flavones such as sinensetin, nobiletin, tangeretin, quercetogetin, heptamethoxyflavone, and other derivatives was unambiguously confirmed. In addition, proceranone, an acetylated tetranortriterpenoid with limonoid structure, was identified for the first time in citrus.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

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A02	`01`			`@0 JAFCAU`
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A06				`@2 2`
A08	`01`	`1`	`ENG`	`@1 Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)`
A11	`01`	`1`		`@1 WEBER (Berthold)`
A11	`02`	`1`		`@1 HARTMANN (Beate)`
A11	`03`	`1`		`@1 STÖCKIGT (Detlef)`
A11	`04`	`1`		`@1 SCHREIBER (Klaus)`
A11	`05`	`1`		`@1 ROLOFF (Michael)`
A11	`06`	`1`		`@1 BERTRAM (Heinz-Jürcen)`
A11	`07`	`1`		`@1 SCHMIDT (Claus O.)`
A14	`01`			`@1 Symrise GmbH & Co. KG, Corporate Research Division @2 37601 Holzminden @3 DEU @Z 1 aut. @Z 2 aut. @Z 3 aut. @Z 4 aut. @Z 5 aut. @Z 6 aut. @Z 7 aut.`
A20				`@1 274-278`
A21				`@1 2006`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 7332 @5 354000133227560020`
A44				`@0 0000 @1 © 2006 INIST-CNRS. All rights reserved.`
A45				`@0 27 ref.`
A47	`01`	`1`		`@0 06-0098010`
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A61				`@0 A`
A64	`01`	`1`		`@0 Journal of agricultural and food chemistry : (Print)`
A66	`01`			`@0 USA`
C01	`01`		`ENG`	@0 Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance techniques with ultraviolet/diode array detection were used as complementary analytical tools for the reliable identification of polymethoxylated flavones in residues from molecular distillation of cold-pressed peel oils of Citrus sinensis. After development of a liquid chromatographic separation procedure, the presence of several polymethoxy flavones such as sinensetin, nobiletin, tangeretin, quercetogetin, heptamethoxyflavone, and other derivatives was unambiguously confirmed. In addition, proceranone, an acetylated tetranortriterpenoid with limonoid structure, was identified for the first time in citrus.
C02	`01`	`X`		`@0 002A35B09`
C03	`01`	`X`	`FRE`	`@0 Chromatographie phase liquide @5 01`
C03	`01`	`X`	`ENG`	`@0 Liquid chromatography @5 01`
C03	`01`	`X`	`SPA`	`@0 Cromatografía fase líquida @5 01`
C03	`02`	`X`	`FRE`	`@0 Spectrométrie masse @5 02`
C03	`02`	`X`	`ENG`	`@0 Mass spectrometry @5 02`
C03	`02`	`X`	`SPA`	`@0 Espectrometría masa @5 02`
C03	`03`	`X`	`FRE`	`@0 Spectrométrie RMN @5 10`
C03	`03`	`X`	`ENG`	`@0 NMR spectrometry @5 10`
C03	`03`	`X`	`SPA`	`@0 Espectrometría RMN @5 10`
C03	`04`	`X`	`FRE`	`@0 Identification @5 19`
C03	`04`	`X`	`ENG`	`@0 Identification @5 19`
C03	`04`	`X`	`SPA`	`@0 Identificación @5 19`
C03	`05`	`X`	`FRE`	`@0 Flavone @2 NK @2 FR @5 20`
C03	`05`	`X`	`ENG`	`@0 Flavones @2 NK @2 FR @5 20`
C03	`06`	`X`	`FRE`	`@0 Résidu @5 24`
C03	`06`	`X`	`ENG`	`@0 Residue @5 24`
C03	`06`	`X`	`SPA`	`@0 Resíduo @5 24`
C03	`07`	`X`	`FRE`	`@0 Distillation @5 26`
C03	`07`	`X`	`ENG`	`@0 Distillation @5 26`
C03	`07`	`X`	`SPA`	`@0 Destilación @5 26`
C03	`08`	`X`	`FRE`	`@0 Flavonoïde @5 28`
C03	`08`	`X`	`ENG`	`@0 Flavonoid @5 28`
C03	`08`	`X`	`SPA`	`@0 Flavonoide @5 28`
C03	`09`	`X`	`FRE`	`@0 Orange @5 48`
C03	`09`	`X`	`ENG`	`@0 Orange @5 48`
C03	`09`	`X`	`SPA`	`@0 Naranja @5 48`
C03	`10`	`X`	`FRE`	`@0 Pelure @5 53`
C03	`10`	`X`	`ENG`	`@0 Peel @5 53`
C03	`10`	`X`	`SPA`	`@0 Cáscara @5 53`
C03	`11`	`X`	`FRE`	`@0 Huile @5 63`
C03	`11`	`X`	`ENG`	`@0 Oil @5 63`
C03	`11`	`X`	`SPA`	`@0 Aceite @5 63`
C03	`12`	`X`	`FRE`	`@0 Citrus sinensis @2 NS @5 64`
C03	`12`	`X`	`ENG`	`@0 Citrus sinensis @2 NS @5 64`
C03	`12`	`X`	`SPA`	`@0 Citrus sinensis @2 NS @5 64`
C03	`13`	`X`	`FRE`	`@0 Limonoïde @4 INC @5 91`
C07	`01`	`X`	`FRE`	`@0 Fruit @5 08`
C07	`01`	`X`	`ENG`	`@0 Fruit @5 08`
C07	`01`	`X`	`SPA`	`@0 Fruto @5 08`
C07	`02`	`X`	`FRE`	`@0 Agrume @5 49`
C07	`02`	`X`	`ENG`	`@0 Citrus fruit @5 49`
C07	`02`	`X`	`SPA`	`@0 Agrios @5 49`
C07	`03`	`X`	`FRE`	`@0 Polyphénol @5 50`
C07	`03`	`X`	`ENG`	`@0 Polyphenol @5 50`
C07	`03`	`X`	`SPA`	`@0 Polifenol @5 50`
C07	`04`	`X`	`FRE`	`@0 Rutaceae @2 NS`
C07	`04`	`X`	`ENG`	`@0 Rutaceae @2 NS`
C07	`04`	`X`	`SPA`	`@0 Rutaceae @2 NS`
C07	`05`	`X`	`FRE`	`@0 Dicotyledones @2 NS`
C07	`05`	`X`	`ENG`	`@0 Dicotyledones @2 NS`
C07	`05`	`X`	`SPA`	`@0 Dicotyledones @2 NS`
C07	`06`	`X`	`FRE`	`@0 Angiospermae @2 NS`
C07	`06`	`X`	`ENG`	`@0 Angiospermae @2 NS`
C07	`06`	`X`	`SPA`	`@0 Angiospermae @2 NS`
C07	`07`	`X`	`FRE`	`@0 Spermatophyta @2 NS`
C07	`07`	`X`	`ENG`	`@0 Spermatophyta @2 NS`
C07	`07`	`X`	`SPA`	`@0 Spermatophyta @2 NS`
N21				`@1 058`
N44	`01`			`@1 OTO`
N82				`@1 OTO`

Format Inist (serveur)

NO :	PASCAL 06-0098010 INIST
ET :	Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)
AU :	WEBER (Berthold); HARTMANN (Beate); STÖCKIGT (Detlef); SCHREIBER (Klaus); ROLOFF (Michael); BERTRAM (Heinz-Jürcen); SCHMIDT (Claus O.)
AF :	Symrise GmbH & Co. KG, Corporate Research Division/37601 Holzminden/Allemagne (1 aut., 2 aut., 3 aut., 4 aut., 5 aut., 6 aut., 7 aut.)
DT :	Publication en série; Niveau analytique
SO :	Journal of agricultural and food chemistry : (Print); ISSN 0021-8561; Coden JAFCAU; Etats-Unis; Da. 2006; Vol. 54; No. 2; Pp. 274-278; Bibl. 27 ref.
LA :	Anglais
EA :	Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance techniques with ultraviolet/diode array detection were used as complementary analytical tools for the reliable identification of polymethoxylated flavones in residues from molecular distillation of cold-pressed peel oils of Citrus sinensis. After development of a liquid chromatographic separation procedure, the presence of several polymethoxy flavones such as sinensetin, nobiletin, tangeretin, quercetogetin, heptamethoxyflavone, and other derivatives was unambiguously confirmed. In addition, proceranone, an acetylated tetranortriterpenoid with limonoid structure, was identified for the first time in citrus.
CC :	002A35B09
FD :	Chromatographie phase liquide; Spectrométrie masse; Spectrométrie RMN; Identification; Flavone; Résidu; Distillation; Flavonoïde; Orange; Pelure; Huile; Citrus sinensis; Limonoïde
FG :	Fruit; Agrume; Polyphénol; Rutaceae; Dicotyledones; Angiospermae; Spermatophyta
ED :	Liquid chromatography; Mass spectrometry; NMR spectrometry; Identification; Flavones; Residue; Distillation; Flavonoid; Orange; Peel; Oil; Citrus sinensis
EG :	Fruit; Citrus fruit; Polyphenol; Rutaceae; Dicotyledones; Angiospermae; Spermatophyta
SD :	Cromatografía fase líquida; Espectrometría masa; Espectrometría RMN; Identificación; Resíduo; Destilación; Flavonoide; Naranja; Cáscara; Aceite; Citrus sinensis
LO :	INIST-7332.354000133227560020
ID :	06-0098010

Links to Exploration step

Pascal:06-0098010

Le document en format XML

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<series><title level="j" type="main">Journal of agricultural and food chemistry : (Print)</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Citrus sinensis</term>
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<term>Flavones</term>
<term>Flavonoid</term>
<term>Identification</term>
<term>Liquid chromatography</term>
<term>Mass spectrometry</term>
<term>NMR spectrometry</term>
<term>Oil</term>
<term>Orange</term>
<term>Peel</term>
<term>Residue</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Chromatographie phase liquide</term>
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<term>Citrus sinensis</term>
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<front><div type="abstract" xml:lang="en">Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance techniques with ultraviolet/diode array detection were used as complementary analytical tools for the reliable identification of polymethoxylated flavones in residues from molecular distillation of cold-pressed peel oils of Citrus sinensis. After development of a liquid chromatographic separation procedure, the presence of several polymethoxy flavones such as sinensetin, nobiletin, tangeretin, quercetogetin, heptamethoxyflavone, and other derivatives was unambiguously confirmed. In addition, proceranone, an acetylated tetranortriterpenoid with limonoid structure, was identified for the first time in citrus.</div>
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<fA11 i1="01" i2="1"><s1>WEBER (Berthold)</s1>
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<fA11 i1="03" i2="1"><s1>STÖCKIGT (Detlef)</s1>
</fA11>
<fA11 i1="04" i2="1"><s1>SCHREIBER (Klaus)</s1>
</fA11>
<fA11 i1="05" i2="1"><s1>ROLOFF (Michael)</s1>
</fA11>
<fA11 i1="06" i2="1"><s1>BERTRAM (Heinz-Jürcen)</s1>
</fA11>
<fA11 i1="07" i2="1"><s1>SCHMIDT (Claus O.)</s1>
</fA11>
<fA14 i1="01"><s1>Symrise GmbH & Co. KG, Corporate Research Division</s1>
<s2>37601 Holzminden</s2>
<s3>DEU</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
<sZ>6 aut.</sZ>
<sZ>7 aut.</sZ>
</fA14>
<fA20><s1>274-278</s1>
</fA20>
<fA21><s1>2006</s1>
</fA21>
<fA23 i1="01"><s0>ENG</s0>
</fA23>
<fA43 i1="01"><s1>INIST</s1>
<s2>7332</s2>
<s5>354000133227560020</s5>
</fA43>
<fA44><s0>0000</s0>
<s1>© 2006 INIST-CNRS. All rights reserved.</s1>
</fA44>
<fA45><s0>27 ref.</s0>
</fA45>
<fA47 i1="01" i2="1"><s0>06-0098010</s0>
</fA47>
<fA60><s1>P</s1>
</fA60>
<fA61><s0>A</s0>
</fA61>
<fA64 i1="01" i2="1"><s0>Journal of agricultural and food chemistry : (Print)</s0>
</fA64>
<fA66 i1="01"><s0>USA</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance techniques with ultraviolet/diode array detection were used as complementary analytical tools for the reliable identification of polymethoxylated flavones in residues from molecular distillation of cold-pressed peel oils of Citrus sinensis. After development of a liquid chromatographic separation procedure, the presence of several polymethoxy flavones such as sinensetin, nobiletin, tangeretin, quercetogetin, heptamethoxyflavone, and other derivatives was unambiguously confirmed. In addition, proceranone, an acetylated tetranortriterpenoid with limonoid structure, was identified for the first time in citrus.</s0>
</fC01>
<fC02 i1="01" i2="X"><s0>002A35B09</s0>
</fC02>
<fC03 i1="01" i2="X" l="FRE"><s0>Chromatographie phase liquide</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="ENG"><s0>Liquid chromatography</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="SPA"><s0>Cromatografía fase líquida</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="X" l="FRE"><s0>Spectrométrie masse</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="ENG"><s0>Mass spectrometry</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="SPA"><s0>Espectrometría masa</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="X" l="FRE"><s0>Spectrométrie RMN</s0>
<s5>10</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG"><s0>NMR spectrometry</s0>
<s5>10</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA"><s0>Espectrometría RMN</s0>
<s5>10</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE"><s0>Identification</s0>
<s5>19</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG"><s0>Identification</s0>
<s5>19</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA"><s0>Identificación</s0>
<s5>19</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE"><s0>Flavone</s0>
<s2>NK</s2>
<s2>FR</s2>
<s5>20</s5>
</fC03>
<fC03 i1="05" i2="X" l="ENG"><s0>Flavones</s0>
<s2>NK</s2>
<s2>FR</s2>
<s5>20</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Résidu</s0>
<s5>24</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Residue</s0>
<s5>24</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Resíduo</s0>
<s5>24</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE"><s0>Distillation</s0>
<s5>26</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG"><s0>Distillation</s0>
<s5>26</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA"><s0>Destilación</s0>
<s5>26</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Flavonoïde</s0>
<s5>28</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG"><s0>Flavonoid</s0>
<s5>28</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Flavonoide</s0>
<s5>28</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE"><s0>Orange</s0>
<s5>48</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Orange</s0>
<s5>48</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Naranja</s0>
<s5>48</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Pelure</s0>
<s5>53</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Peel</s0>
<s5>53</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Cáscara</s0>
<s5>53</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Huile</s0>
<s5>63</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Oil</s0>
<s5>63</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Aceite</s0>
<s5>63</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Citrus sinensis</s0>
<s2>NS</s2>
<s5>64</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Citrus sinensis</s0>
<s2>NS</s2>
<s5>64</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Citrus sinensis</s0>
<s2>NS</s2>
<s5>64</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Limonoïde</s0>
<s4>INC</s4>
<s5>91</s5>
</fC03>
<fC07 i1="01" i2="X" l="FRE"><s0>Fruit</s0>
<s5>08</s5>
</fC07>
<fC07 i1="01" i2="X" l="ENG"><s0>Fruit</s0>
<s5>08</s5>
</fC07>
<fC07 i1="01" i2="X" l="SPA"><s0>Fruto</s0>
<s5>08</s5>
</fC07>
<fC07 i1="02" i2="X" l="FRE"><s0>Agrume</s0>
<s5>49</s5>
</fC07>
<fC07 i1="02" i2="X" l="ENG"><s0>Citrus fruit</s0>
<s5>49</s5>
</fC07>
<fC07 i1="02" i2="X" l="SPA"><s0>Agrios</s0>
<s5>49</s5>
</fC07>
<fC07 i1="03" i2="X" l="FRE"><s0>Polyphénol</s0>
<s5>50</s5>
</fC07>
<fC07 i1="03" i2="X" l="ENG"><s0>Polyphenol</s0>
<s5>50</s5>
</fC07>
<fC07 i1="03" i2="X" l="SPA"><s0>Polifenol</s0>
<s5>50</s5>
</fC07>
<fC07 i1="04" i2="X" l="FRE"><s0>Rutaceae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="04" i2="X" l="ENG"><s0>Rutaceae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="04" i2="X" l="SPA"><s0>Rutaceae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="05" i2="X" l="FRE"><s0>Dicotyledones</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="05" i2="X" l="ENG"><s0>Dicotyledones</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="05" i2="X" l="SPA"><s0>Dicotyledones</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="06" i2="X" l="FRE"><s0>Angiospermae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="06" i2="X" l="ENG"><s0>Angiospermae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="06" i2="X" l="SPA"><s0>Angiospermae</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="07" i2="X" l="FRE"><s0>Spermatophyta</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="07" i2="X" l="ENG"><s0>Spermatophyta</s0>
<s2>NS</s2>
</fC07>
<fC07 i1="07" i2="X" l="SPA"><s0>Spermatophyta</s0>
<s2>NS</s2>
</fC07>
<fN21><s1>058</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
</standard>
<server><NO>PASCAL 06-0098010 INIST</NO>
<ET>Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)</ET>
<AU>WEBER (Berthold); HARTMANN (Beate); STÖCKIGT (Detlef); SCHREIBER (Klaus); ROLOFF (Michael); BERTRAM (Heinz-Jürcen); SCHMIDT (Claus O.)</AU>
<AF>Symrise GmbH & Co. KG, Corporate Research Division/37601 Holzminden/Allemagne (1 aut., 2 aut., 3 aut., 4 aut., 5 aut., 6 aut., 7 aut.)</AF>
<DT>Publication en série; Niveau analytique</DT>
<SO>Journal of agricultural and food chemistry : (Print); ISSN 0021-8561; Coden JAFCAU; Etats-Unis; Da. 2006; Vol. 54; No. 2; Pp. 274-278; Bibl. 27 ref.</SO>
<LA>Anglais</LA>
<EA>Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance techniques with ultraviolet/diode array detection were used as complementary analytical tools for the reliable identification of polymethoxylated flavones in residues from molecular distillation of cold-pressed peel oils of Citrus sinensis. After development of a liquid chromatographic separation procedure, the presence of several polymethoxy flavones such as sinensetin, nobiletin, tangeretin, quercetogetin, heptamethoxyflavone, and other derivatives was unambiguously confirmed. In addition, proceranone, an acetylated tetranortriterpenoid with limonoid structure, was identified for the first time in citrus.</EA>
<CC>002A35B09</CC>
<FD>Chromatographie phase liquide; Spectrométrie masse; Spectrométrie RMN; Identification; Flavone; Résidu; Distillation; Flavonoïde; Orange; Pelure; Huile; Citrus sinensis; Limonoïde</FD>
<FG>Fruit; Agrume; Polyphénol; Rutaceae; Dicotyledones; Angiospermae; Spermatophyta</FG>
<ED>Liquid chromatography; Mass spectrometry; NMR spectrometry; Identification; Flavones; Residue; Distillation; Flavonoid; Orange; Peel; Oil; Citrus sinensis</ED>
<EG>Fruit; Citrus fruit; Polyphenol; Rutaceae; Dicotyledones; Angiospermae; Spermatophyta</EG>
<SD>Cromatografía fase líquida; Espectrometría masa; Espectrometría RMN; Identificación; Resíduo; Destilación; Flavonoide; Naranja; Cáscara; Aceite; Citrus sinensis</SD>
<LO>INIST-7332.354000133227560020</LO>
<ID>06-0098010</ID>
</server>
</inist>
</record>

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Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)

Liquid chromatography/mass spectrometry and liquid chromatography/nuclear magnetic resonance as complementary analytical techniques for unambiguous identification of polymethoxylated flavones in residues from molecular distillation of orange peel oils (Citrus sinensis)

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