Ethylenediammonium tetraaquadisulfatomagnesium(II)
Identifieur interne : 000162 ( Ncbi/Checkpoint ); précédent : 000161; suivant : 000163Ethylenediammonium tetraaquadisulfatomagnesium(II)
Auteurs : Walid Rekik [Tunisie] ; Houcine Naïli [Tunisie] ; Tahar Mhiri [Tunisie] ; Thierry Bataille [France]Source :
- Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2009.
Abstract
The title compound, [NH3(CH2)2NH3][Mg(SO4)2(H2O)4], was synthesized by the slow evaporation method. Its crystal structure can be described as an alternate stacking of inorganic layers of tetraaquabis(sulfato-
Url:
DOI: 10.1107/S1600536809041981
PubMed: 21578145
PubMed Central: 2971149
Affiliations:
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PMC:2971149Le document en format XML
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<country xml:lang="fr">Tunisie</country>
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<author><name sortKey="Naili, Houcine" sort="Naili, Houcine" uniqKey="Naili H" first="Houcine" last="Naïli">Houcine Naïli</name>
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<country xml:lang="fr">Tunisie</country>
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<author><name sortKey="Mhiri, Tahar" sort="Mhiri, Tahar" uniqKey="Mhiri T" first="Tahar" last="Mhiri">Tahar Mhiri</name>
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<country xml:lang="fr">France</country>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Ethylenediammonium tetraaquadisulfatomagnesium(II)</title>
<author><name sortKey="Rekik, Walid" sort="Rekik, Walid" uniqKey="Rekik W" first="Walid" last="Rekik">Walid Rekik</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de l’Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, BP 802, 3018 SFAX,<country>Tunisia</country>
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<country xml:lang="fr">Tunisie</country>
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<author><name sortKey="Naili, Houcine" sort="Naili, Houcine" uniqKey="Naili H" first="Houcine" last="Naïli">Houcine Naïli</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de l’Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, BP 802, 3018 SFAX,<country>Tunisia</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<author><name sortKey="Mhiri, Tahar" sort="Mhiri, Tahar" uniqKey="Mhiri T" first="Tahar" last="Mhiri">Tahar Mhiri</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de l’Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, BP 802, 3018 SFAX,<country>Tunisia</country>
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<country xml:lang="fr">Tunisie</country>
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<author><name sortKey="Bataille, Thierry" sort="Bataille, Thierry" uniqKey="Bataille T" first="Thierry" last="Bataille">Thierry Bataille</name>
<affiliation wicri:level="1"><nlm:aff id="b">Laboratoire de Chimie du Solide et Inorganique Moléculaire (CNRS, UMR 6511), Université de Rennes I, Avenue du Général Leclerc, 35042 Rennes CEDEX,<country>France</country>
</nlm:aff>
<country xml:lang="fr">France</country>
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<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
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<front><div type="abstract" xml:lang="en"><p>The title compound, [NH<sub>3</sub>
(CH<sub>2</sub>
)<sub>2</sub>
NH<sub>3</sub>
][Mg(SO<sub>4</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>4</sub>
], was synthesized by the slow evaporation method. Its crystal structure can be described as an alternate stacking of inorganic layers of tetraaquabis(sulfato-<italic>O</italic>
)magnesium [Mg(SO<sub>4</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>4</sub>
]<sup>2−</sup>
anions (<inline-formula><inline-graphic xlink:href="e-65-m1404-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
symmetry) and organic layers of [NH<sub>3</sub>
(CH<sub>2</sub>
)<sub>2</sub>
NH<sub>3</sub>
]<sup>2+</sup>
cations along the crystallographic <italic>b</italic>
axis. The anions, built up from tetrahedral SO<sub>4</sub>
units and octahedral Mg(H<sub>2</sub>
O)<sub>4</sub>
O<sub>2</sub>
units, and the cations are linked together through N—H⋯O hydrogen bonds, forming a three-dimensional network. O—H⋯O interactions are also present.</p>
</div>
</front>
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