CobaltMaghrebV1, Pmc, Curation, bibRecord, 000385

Ethylenediammonium tetraaquadisulfatomagnesium(II)

Identifieur interne : 000385 ( Pmc/Curation ); précédent : 000384; suivant : 000386

Ethylenediammonium tetraaquadisulfatomagnesium(II)

Auteurs : Walid Rekik [Tunisie] ; Houcine Naïli [Tunisie] ; Tahar Mhiri [Tunisie] ; Thierry Bataille [France]

Source :

Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2009.

RBID : PMC:2971149

Abstract

The title compound, [NH₃(CH₂)₂NH₃][Mg(SO₄)₂(H₂O)₄], was synthesized by the slow evaporation method. Its crystal structure can be described as an alternate stacking of inorganic layers of tetraaquabis(sulfato-O)magnesium [Mg(SO₄)₂(H₂O)₄]²⁻ anions ( symmetry) and organic layers of [NH₃(CH₂)₂NH₃]²⁺ cations along the crystallographic b axis. The anions, built up from tetrahedral SO₄ units and octahedral Mg(H₂O)₄O₂ units, and the cations are linked together through N—H⋯O hydrogen bonds, forming a three-dimensional network. O—H⋯O interactions are also present.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971149

DOI: 10.1107/S1600536809041981
PubMed: 21578145
PubMed Central: 2971149

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<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de l’Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, BP 802, 3018 SFAX,<country>Tunisia</country>
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<author><name sortKey="Naili, Houcine" sort="Naili, Houcine" uniqKey="Naili H" first="Houcine" last="Naïli">Houcine Naïli</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de l’Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, BP 802, 3018 SFAX,<country>Tunisia</country>
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<author><name sortKey="Bataille, Thierry" sort="Bataille, Thierry" uniqKey="Bataille T" first="Thierry" last="Bataille">Thierry Bataille</name>
<affiliation wicri:level="1"><nlm:aff id="b">Laboratoire de Chimie du Solide et Inorganique Moléculaire (CNRS, UMR 6511), Université de Rennes I, Avenue du Général Leclerc, 35042 Rennes CEDEX,<country>France</country>
</nlm:aff>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Ethylenediammonium tetraaquadisulfatomagnesium(II)</title>
<author><name sortKey="Rekik, Walid" sort="Rekik, Walid" uniqKey="Rekik W" first="Walid" last="Rekik">Walid Rekik</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de l’Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, BP 802, 3018 SFAX,<country>Tunisia</country>
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<country xml:lang="fr">Tunisie</country>
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<author><name sortKey="Naili, Houcine" sort="Naili, Houcine" uniqKey="Naili H" first="Houcine" last="Naïli">Houcine Naïli</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de l’Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, BP 802, 3018 SFAX,<country>Tunisia</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
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<author><name sortKey="Mhiri, Tahar" sort="Mhiri, Tahar" uniqKey="Mhiri T" first="Tahar" last="Mhiri">Tahar Mhiri</name>
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</nlm:aff>
<country xml:lang="fr">Tunisie</country>
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</author>
<author><name sortKey="Bataille, Thierry" sort="Bataille, Thierry" uniqKey="Bataille T" first="Thierry" last="Bataille">Thierry Bataille</name>
<affiliation wicri:level="1"><nlm:aff id="b">Laboratoire de Chimie du Solide et Inorganique Moléculaire (CNRS, UMR 6511), Université de Rennes I, Avenue du Général Leclerc, 35042 Rennes CEDEX,<country>France</country>
</nlm:aff>
<country xml:lang="fr">France</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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</author>
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<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2009">2009</date>
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<front><div type="abstract" xml:lang="en"><p>The title compound, [NH<sub>3</sub>
(CH<sub>2</sub>
)<sub>2</sub>
NH<sub>3</sub>
][Mg(SO<sub>4</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>4</sub>
], was synthesized by the slow evaporation method. Its crystal structure can be described as an alternate stacking of inorganic layers of tetraaquabis(sulfato-<italic>O</italic>
)magnesium [Mg(SO<sub>4</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>4</sub>
]<sup>2−</sup>
  anions (<inline-formula><inline-graphic xlink:href="e-65-m1404-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
 symmetry) and organic layers of [NH<sub>3</sub>
(CH<sub>2</sub>
)<sub>2</sub>
NH<sub>3</sub>
]<sup>2+</sup>
 cations along the crystallographic <italic>b</italic>
 axis. The anions, built up from tetrahedral SO<sub>4</sub>
 units and octahedral Mg(H<sub>2</sub>
O)<sub>4</sub>
O<sub>2</sub>
 units,  and the cations are linked together through N—H⋯O hydrogen bonds, forming a three-dimensional network. O—H⋯O interactions are also present.</p>
</div>
</front>
<back><div1 type="bibliography"><listBibl><biblStruct></biblStruct>
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</TEI>
<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
  <front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Structure Reports Online</journal-title>
</journal-title-group>
<issn pub-type="epub">1600-5368</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">21578145</article-id>
<article-id pub-id-type="pmc">2971149</article-id>
<article-id pub-id-type="publisher-id">pb2011</article-id>
<article-id pub-id-type="doi">10.1107/S1600536809041981</article-id>
<article-id pub-id-type="coden">ACSEBH</article-id>
<article-id pub-id-type="pii">S1600536809041981</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Metal-Organic Papers</subject>
</subj-group>
</article-categories>
<title-group><article-title>Ethylenediammonium tetraaquadisulfatomagnesium(II)</article-title>
<alt-title><italic>(C<sub>2</sub>
H<sub>10</sub>
N<sub>2</sub>
)[Mg(SO<sub>4</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>4</sub>
]</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Rekik</surname>
<given-names>Walid</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Naïli</surname>
<given-names>Houcine</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Mhiri</surname>
<given-names>Tahar</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Bataille</surname>
<given-names>Thierry</given-names>
</name>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<aff id="a"><label>a</label>
Laboratoire de l’Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, BP 802, 3018 SFAX,<country>Tunisia</country>
</aff>
<aff id="b"><label>b</label>
Laboratoire de Chimie du Solide et Inorganique Moléculaire (CNRS, UMR 6511), Université de Rennes I, Avenue du Général Leclerc, 35042 Rennes CEDEX,<country>France</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>w_rekik@alinto.com</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>11</month>
<year>2009</year>
</pub-date>
<pub-date pub-type="epub"><day>23</day>
<month>10</month>
<year>2009</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>23</day>
<month>10</month>
<year>2009</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the 
 							. </pmc-comment>
      <volume>65</volume>
<issue>Pt 11</issue>
<issue-id pub-id-type="publisher-id">e091100</issue-id>
<fpage>m1404</fpage>
<lpage>m1405</lpage>
<history><date date-type="received"><day>01</day>
<month>10</month>
<year>2009</year>
</date>
<date date-type="accepted"><day>13</day>
<month>10</month>
<year>2009</year>
</date>
</history>
<permissions><copyright-statement>© Rekik et al. 2009</copyright-statement>
<copyright-year>2009</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S1600536809041981">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract><p>The title compound, [NH<sub>3</sub>
(CH<sub>2</sub>
)<sub>2</sub>
NH<sub>3</sub>
][Mg(SO<sub>4</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>4</sub>
], was synthesized by the slow evaporation method. Its crystal structure can be described as an alternate stacking of inorganic layers of tetraaquabis(sulfato-<italic>O</italic>
)magnesium [Mg(SO<sub>4</sub>
)<sub>2</sub>
(H<sub>2</sub>
O)<sub>4</sub>
]<sup>2−</sup>
  anions (<inline-formula><inline-graphic xlink:href="e-65-m1404-efi1.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
 symmetry) and organic layers of [NH<sub>3</sub>
(CH<sub>2</sub>
)<sub>2</sub>
NH<sub>3</sub>
]<sup>2+</sup>
 cations along the crystallographic <italic>b</italic>
 axis. The anions, built up from tetrahedral SO<sub>4</sub>
 units and octahedral Mg(H<sub>2</sub>
O)<sub>4</sub>
O<sub>2</sub>
 units,  and the cations are linked together through N—H⋯O hydrogen bonds, forming a three-dimensional network. O—H⋯O interactions are also present.</p>
</abstract>
</article-meta>
</front>
<floats-group><table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Selected bond distances (Å)</title>
</caption>
<table frame="hsides" rules="groups"><tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Mg—O<italic>W</italic>
1</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.0632 (18)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Mg—O4</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.0826 (15)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Mg—O<italic>W</italic>
2</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.0833 (18)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">S—O1</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.4605 (17)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">S—O2</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.4688 (17)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">S—O3</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.4748 (16)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">S—O4</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.4844 (15)</td>
</tr>
</tbody>
</table>
</table-wrap>
<table-wrap id="table2" position="float"><label>Table 2</label>
<caption><title>Hydrogen-bond geometry (Å, °)</title>
</caption>
<table frame="hsides" rules="groups"><thead valign="bottom"><tr><th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom">H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
</tr>
</thead>
<tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">N—H0<italic>A</italic>
⋯O4<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.89</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.95</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.838 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">174</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">N—H0<italic>B</italic>
⋯O3<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.89</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.05</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.886 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">156</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">N—H0<italic>C</italic>
⋯O2</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.89</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.97</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.837 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">163</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O<italic>W</italic>
1—H11⋯O2<sup>v</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.866 (19)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.91 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.767 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">169 (4)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O<italic>W</italic>
1—H12⋯O3<sup>vi</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.869 (18)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.890 (19)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.758 (3)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">178 (3)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O<italic>W</italic>
2—H21⋯O1<sup>vii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.841 (19)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.95 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.729 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">153 (3)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O<italic>W</italic>
2—H22⋯O1<sup>viii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.871 (19)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.03 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.869 (2)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">162 (4)</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry codes: (iii) <inline-formula><inline-graphic xlink:href="e-65-m1404-efi3.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iv) <inline-formula><inline-graphic xlink:href="e-65-m1404-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (v) <inline-formula><inline-graphic xlink:href="e-65-m1404-efi5.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (vi) <inline-formula><inline-graphic xlink:href="e-65-m1404-efi6.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (vii) <inline-formula><inline-graphic xlink:href="e-65-m1404-efi7.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (viii) <inline-formula><inline-graphic xlink:href="e-65-m1404-efi8.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
</record>

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Ethyl­enediammonium tetraaquadi­sulfatomagnesium(II)

Ethyl­enediammonium tetraaquadi­sulfatomagnesium(II)

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Ethylenediammonium tetraaquadisulfatomagnesium(II)

Ethylenediammonium tetraaquadisulfatomagnesium(II)