Identification of individual and few layers of WS2 using Raman Spectroscopy
Identifieur interne : 000335 ( Main/Exploration ); précédent : 000334; suivant : 000336Identification of individual and few layers of WS2 using Raman Spectroscopy
Auteurs : Ayse Berkdemir [États-Unis] ; Humberto R. Gutiérrez [États-Unis] ; Andrés R. Botello-Méndez [Belgique] ; Néstor Perea-L Pez [États-Unis] ; Ana Laura Elías [États-Unis] ; Chen-Ing Chia [États-Unis] ; Bei Wang [États-Unis] ; Vincent H. Crespi [États-Unis] ; Florentino L Pez-Urías [États-Unis, Mexique] ; Jean-Christophe Charlier [Belgique] ; Humberto Terrones [États-Unis] ; Mauricio Terrones [États-Unis, Japon]Source :
- Scientific Reports [ 2045-2322 ] ; 2013.
Abstract
The Raman scattering of single- and few-layered WS2 is studied as a function of the number of S-W-S layers and the excitation wavelength in the visible range (488, 514 and 647 nm). For the three excitation wavelengths used in this study, the frequency of the A1g(Γ) phonon mode monotonically decreases with the number of layers. For single-layer WS2, the 514.5 nm laser excitation generates a second-order Raman resonance involving the longitudinal acoustic mode (LA(M)). This resonance results from a coupling between the electronic band structure and lattice vibrations. First-principles calculations were used to determine the electronic and phonon band structures of single-layer and bulk WS2. The reduced intensity of the 2LA mode was then computed, as a function of the laser wavelength, from the fourth-order Fermi golden rule. Our observations establish an unambiguous and nondestructive Raman fingerprint for identifying single- and few-layered WS2 films.
Url:
DOI: 10.1038/srep01755
PubMed: NONE
PubMed Central: 3639451
Affiliations:
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<affiliation><nlm:aff id="a4">These authors contributed equally to this work.</nlm:aff>
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<author><name sortKey="Gutierrez, Humberto R" sort="Gutierrez, Humberto R" uniqKey="Gutierrez H" first="Humberto R." last="Gutiérrez">Humberto R. Gutiérrez</name>
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<affiliation><nlm:aff id="a4">These authors contributed equally to this work.</nlm:aff>
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<affiliation wicri:level="2"><nlm:aff id="a5">Current address: Department of Physics & Astronomy, University of Louisville, Louisville, KY 40292 USA.</nlm:aff>
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<author><name sortKey="Chia, Chen Ing" sort="Chia, Chen Ing" uniqKey="Chia C" first="Chen-Ing" last="Chia">Chen-Ing Chia</name>
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, PA 16802, USA</nlm:aff>
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, PA 16802, USA</nlm:aff>
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, Chemin des étoiles 8, 1348 Louvain-la-Neuve, Belgium</nlm:aff>
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, Wakasato 4-17-1, Nagano 380-853, Japan</nlm:aff>
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<front><div type="abstract" xml:lang="en"><p>The Raman scattering of single- and few-layered WS<sub>2</sub>
is studied as a function of the number of S-W-S layers and the excitation wavelength in the visible range (488, 514 and 647 nm). For the three excitation wavelengths used in this study, the frequency of the A<sub>1g</sub>
(Γ) phonon mode monotonically decreases with the number of layers. For single-layer WS<sub>2</sub>
, the 514.5 nm laser excitation generates a second-order Raman resonance involving the longitudinal acoustic mode (LA(M)). This resonance results from a coupling between the electronic band structure and lattice vibrations. First-principles calculations were used to determine the electronic and phonon band structures of single-layer and bulk WS<sub>2.</sub>
The reduced intensity of the 2LA mode was then computed, as a function of the laser wavelength, from the fourth-order Fermi golden rule. Our observations establish an unambiguous and nondestructive Raman fingerprint for identifying single- and few-layered WS<sub>2</sub>
films.</p>
</div>
</front>
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