An extensive comparison of anisotropies in MBE grown (Ga,Mn)As material
Identifieur interne : 000F85 ( Istex/Corpus ); précédent : 000F84; suivant : 000F86An extensive comparison of anisotropies in MBE grown (Ga,Mn)As material
Auteurs : C. Gould ; S. Mark ; K. Pappert ; R G Dengel ; J. Wenisch ; R P Campion ; A W Rushforth ; D. Chiba ; Z. Li ; X. Liu ; W. Van Roy ; H. Ohno ; J K Furdyna ; B. Gallagher ; K. Brunner ; G. Schmidt ; L W MolenkampSource :
- New Journal of Physics [ 1367-2630 ] ; 2008.
Abstract
This paper reports on a detailed magnetotransport investigation of the magnetic anisotropies of (Ga,Mn)As layers produced by various sources worldwide. Using anisotropy fingerprints to identify the contributions of the various higher-order anisotropy terms, we show that the presence of both a [100] and a [110] uniaxial anisotropy in addition to the primary ([100] [010]) anisotropy is common to all medium doped (Ga,Mn)As layers typically used in transport measurement, with the amplitude of these uniaxial terms being characteristic of the individual layers.
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DOI: 10.1088/1367-2630/10/5/055007
Links to Exploration step
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<front><div type="abstract">This paper reports on a detailed magnetotransport investigation of the magnetic anisotropies of (Ga,Mn)As layers produced by various sources worldwide. Using anisotropy fingerprints to identify the contributions of the various higher-order anisotropy terms, we show that the presence of both a [100] and a [110] uniaxial anisotropy in addition to the primary ([100] [010]) anisotropy is common to all medium doped (Ga,Mn)As layers typically used in transport measurement, with the amplitude of these uniaxial terms being characteristic of the individual layers.</div>
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<abstract>This paper reports on a detailed magnetotransport investigation of the magnetic anisotropies of (Ga,Mn)As layers produced by various sources worldwide. Using anisotropy fingerprints to identify the contributions of the various higher-order anisotropy terms, we show that the presence of both a [100] and a [110] uniaxial anisotropy in addition to the primary ([100] [010]) anisotropy is common to all medium doped (Ga,Mn)As layers typically used in transport measurement, with the amplitude of these uniaxial terms being characteristic of the individual layers.</abstract>
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<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
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<author xml:id="author-6"><persName><forename type="first">R P</forename>
<surname>Campion</surname>
</persName>
<affiliation>School of Physics and Astronomy, University of Nottingham, Nottingham NG7 2RD, UK</affiliation>
</author>
<author xml:id="author-7"><persName><forename type="first">A W</forename>
<surname>Rushforth</surname>
</persName>
<affiliation>School of Physics and Astronomy, University of Nottingham, Nottingham NG7 2RD, UK</affiliation>
</author>
<author xml:id="author-8"><persName><forename type="first">D</forename>
<surname>Chiba</surname>
</persName>
<affiliation>Semiconductor Spintronics Project, Exploratory Research for Advanced Technology, Japan Science and Technology Agency, Kitamemachi 1-18, Aoba-ku, Sendai 980-0023, Japan</affiliation>
<affiliation>Laboratory for Nanoelectronics and Spintronics, Research Institute of Electrical Communication, Tohoku University, Katahira 2-1-1, Aoba-ku, Sendai 980-8577, Japan</affiliation>
</author>
<author xml:id="author-9"><persName><forename type="first">Z</forename>
<surname>Li</surname>
</persName>
<affiliation>IMEC, Kapeldreef 75, B-3001 Leuven, Belgium</affiliation>
</author>
<author xml:id="author-10"><persName><forename type="first">X</forename>
<surname>Liu</surname>
</persName>
<affiliation>Department of Physics, University of Notre Dame, Notre Dame, IN 46556, USA</affiliation>
</author>
<author xml:id="author-11"><persName><forename type="first">W</forename>
<surname>Van Roy</surname>
</persName>
<affiliation>IMEC, Kapeldreef 75, B-3001 Leuven, Belgium</affiliation>
</author>
<author xml:id="author-12"><persName><forename type="first">H</forename>
<surname>Ohno</surname>
</persName>
<affiliation>Laboratory for Nanoelectronics and Spintronics, Research Institute of Electrical Communication, Tohoku University, Katahira 2-1-1, Aoba-ku, Sendai 980-8577, Japan</affiliation>
<affiliation>Semiconductor Spintronics Project, Exploratory Research for Advanced Technology, Japan Science and Technology Agency, Kitamemachi 1-18, Aoba-ku, Sendai 980-0023, Japan</affiliation>
</author>
<author xml:id="author-13"><persName><forename type="first">J K</forename>
<surname>Furdyna</surname>
</persName>
<affiliation>Department of Physics, University of Notre Dame, Notre Dame, IN 46556, USA</affiliation>
</author>
<author xml:id="author-14"><persName><forename type="first">B</forename>
<surname>Gallagher</surname>
</persName>
<affiliation>School of Physics and Astronomy, University of Nottingham, Nottingham NG7 2RD, UK</affiliation>
</author>
<author xml:id="author-15"><persName><forename type="first">K</forename>
<surname>Brunner</surname>
</persName>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
</author>
<author xml:id="author-16"><persName><forename type="first">G</forename>
<surname>Schmidt</surname>
</persName>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
</author>
<author xml:id="author-17"><persName><forename type="first">L W</forename>
<surname>Molenkamp</surname>
</persName>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
</author>
</analytic>
<monogr><title level="j">New Journal of Physics</title>
<title level="j" type="abbrev">New J. Phys.</title>
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<abstract><p>This paper reports on a detailed magnetotransport investigation of the magnetic anisotropies of (Ga,Mn)As layers produced by various sources worldwide. Using anisotropy fingerprints to identify the contributions of the various higher-order anisotropy terms, we show that the presence of both a [100] and a [110] uniaxial anisotropy in addition to the primary ([100] [010]) anisotropy is common to all medium doped (Ga,Mn)As layers typically used in transport measurement, with the amplitude of these uniaxial terms being characteristic of the individual layers.</p>
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<header><title-group><title>An extensive comparison of anisotropies in MBE grown (Ga,Mn)As material</title>
<short-title>An extensive comparison of anisotropies in MBE grown (Ga,Mn)As material</short-title>
<ej-title>An extensive comparison of anisotropies in MBE grown (Ga,Mn)As material</ej-title>
</title-group>
<author-group><author address="nj268306ad1" alt-address="nj268306aad7" email="nj268306ea1"><first-names>C</first-names>
<second-name>Gould</second-name>
</author>
<author address="nj268306ad1"><first-names>S</first-names>
<second-name>Mark</second-name>
</author>
<author address="nj268306ad1"><first-names>K</first-names>
<second-name>Pappert</second-name>
</author>
<author address="nj268306ad1"><first-names>R G</first-names>
<second-name>Dengel</second-name>
</author>
<author address="nj268306ad1"><first-names>J</first-names>
<second-name>Wenisch</second-name>
</author>
<author address="nj268306ad2"><first-names>R P</first-names>
<second-name>Campion</second-name>
</author>
<author address="nj268306ad2"><first-names>A W</first-names>
<second-name>Rushforth</second-name>
</author>
<author address="nj268306ad4" second-address="nj268306ad5"><first-names>D</first-names>
<second-name>Chiba</second-name>
</author>
<author address="nj268306ad3"><first-names>Z</first-names>
<second-name>Li</second-name>
</author>
<author address="nj268306ad6"><first-names>X</first-names>
<second-name>Liu</second-name>
</author>
<author address="nj268306ad3"><first-names>W</first-names>
<second-name>Van Roy</second-name>
</author>
<author address="nj268306ad5" second-address="nj268306ad4"><first-names>H</first-names>
<second-name>Ohno</second-name>
</author>
<author address="nj268306ad6"><first-names>J K</first-names>
<second-name>Furdyna</second-name>
</author>
<author address="nj268306ad2"><first-names>B</first-names>
<second-name>Gallagher</second-name>
</author>
<author address="nj268306ad1"><first-names>K</first-names>
<second-name>Brunner</second-name>
</author>
<author address="nj268306ad1"><first-names>G</first-names>
<second-name>Schmidt</second-name>
</author>
<author address="nj268306ad1"><first-names>L W</first-names>
<second-name>Molenkamp</second-name>
</author>
<short-author-list>C Gould <italic>et al</italic>
</short-author-list>
</author-group>
<address-group><address id="nj268306ad1" showid="yes">Physikalisches Institut (EP3), <orgname>Universität Würzburg</orgname>
, Am Hubland, D-97074 Würzburg, <country>Germany</country>
</address>
<address id="nj268306ad2" showid="yes">School of Physics and Astronomy, <orgname>University of Nottingham</orgname>
, Nottingham NG7 2RD, <country>UK</country>
</address>
<address id="nj268306ad3" showid="yes"><orgname>IMEC</orgname>
, Kapeldreef 75, B-3001 Leuven, <country>Belgium</country>
</address>
<address id="nj268306ad4" showid="yes">Semiconductor Spintronics Project, <orgname>Exploratory Research for Advanced Technology, Japan Science and Technology Agency</orgname>
, Kitamemachi 1-18, Aoba-ku, Sendai 980-0023, <country>Japan</country>
</address>
<address id="nj268306ad5" showid="yes">Laboratory for Nanoelectronics and Spintronics, Research Institute of Electrical Communication, <orgname>Tohoku University</orgname>
, Katahira 2-1-1, Aoba-ku, Sendai 980-8577, <country>Japan</country>
</address>
<address id="nj268306ad6" showid="yes">Department of Physics, <orgname>University of Notre Dame</orgname>
, Notre Dame, IN 46556, <country>USA</country>
</address>
<address id="nj268306aad7" alt="yes" showid="yes">Author to whom any correspondence should be addressed.</address>
<e-address id="nj268306ea1"><email mailto="gould@physik.uni-wuerzburg.de">gould@physik.uni-wuerzburg.de</email>
</e-address>
</address-group>
<history received="18 December 2007" online="23 May 2008"></history>
<abstract-group><abstract><heading>Abstract</heading>
<p indent="no">This paper reports on a detailed magnetotransport investigation of the magnetic anisotropies of (Ga,Mn)As layers produced by various sources worldwide. Using anisotropy fingerprints to identify the contributions of the various higher-order anisotropy terms, we show that the presence of both a [100] and a [110] uniaxial anisotropy in addition to the primary ([100] + [010]) anisotropy is common to all medium doped (Ga,Mn)As layers typically used in transport measurement, with the amplitude of these uniaxial terms being characteristic of the individual layers.</p>
</abstract>
</abstract-group>
</header>
<body refstyle="numeric"><sec-level1 id="nj268306s1" label="1"><heading>Introduction</heading>
<p indent="no">A key prototypical material for investigations into spintronics is the ferromagnetic semiconductor (Ga,Mn)As. The marriage of magnetic and semiconductor properties brought about by strong spin–orbit coupling, which ties the density of states of this material to its magnetic properties, offers a host of new and exploitable magnetotransport effects. As investigations into this material continue to progress, it has become clear that a detailed understanding of the underlying magnetic anisotropy is a key issue in device design and optimization.</p>
<p>This magnetic anisotropy in (Ga,Mn)As is very rich and complicated, which led to various reports over the past decade that superficially appeared to be contradictory. In general, depending on growth strain, doping density and temperature, the material can have an easy axis of magnetization either perpendicular to the plane, or in the layer plane [<cite linkend="nj268306bib1">1</cite>
, <cite linkend="nj268306bib2">2</cite>
], and in the latter case, the primary anisotropy can be either biaxial along [100] and [010], or uniaxial along either [110] or <inline-eqn></inline-eqn>
[<cite linkend="nj268306bib3">3</cite>
, <cite linkend="nj268306bib4">4</cite>
].</p>
<p>It is generally accepted that for typical medium-doped transport samples with <inline-eqn><math-text>∼3</math-text>
</inline-eqn>
to 6% Mn, grown with compressive strain and measured at 4.2 K, the primary anisotropy is a biaxial term with easy axes along the [100] and [010] crystal directions. Second-order terms are also widely reported in the form of a uniaxial easy axis along [110] or <inline-eqn></inline-eqn>
[<cite linkend="nj268306bib5">5</cite>
] of various relative strengths, or a uniaxial along [010] [<cite linkend="nj268306bib6">6</cite>
].</p>
<p>Since it is well known in the community that the detailed properties of (Ga,Mn)As depend on exact growth conditions such as substrate temperature, growth rate, flux ratios, etc [<cite linkend="nj268306bib7">7</cite>
]–[<cite linkend="nj268306bib9">9</cite>
], it was initially widely assumed that the observation of these different higher-order anisotropy terms was primarily a result of the distinct properties of the various layers used.</p>
<p>It is now realized that part of the confusion arose from the fact that the various transport measurements from which these terms had been extracted differ in sensitivity to the different anisotropy terms. For example, in the non-volatile tunneling anisotropic magneoresistance (TAMR) experiments [<cite linkend="nj268306bib6">6</cite>
], the [010] plays a crucial role, whereas the [110] anisotropy is nearly irrelevant, because it has a significant impact only for volatile effects occurring at higher fields. On the other hand, the [010] term plays only a secondary role in the planar Hall measurements of Hall bars along the [110] direction [<cite linkend="nj268306bib5">5</cite>
].</p>
<p>Moreover, because these second-order uniaxial anisotropy terms are significantly weaker than the primary biaxial anisotropy, they cannot be reliably characterized by direct magnetization measurements such as superconducting quantum interference device (SQUID) or vibrating sample magnetometer (VSM). The challenge of fully characterizing the complex anisotropies in (Ga,Mn)As was recently successfully addressed with the development of an ‘anisotropy fingerprint’ technique [<cite linkend="nj268306bib10">10</cite>
], which consists of taking magnetotransport measurements for magnetic fields swept in multiple directions.</p>
<p>Using this method, we recently investigated [<cite linkend="nj268306bib11">11</cite>
] various transport samples produced on wafers grown in a given molecular beam epitaxy (MBE) system at Würzburg University, and showed that in all cases, a detailed investigation revealed the presence of both [010] and [110] uniaxial terms, with the sign and relative amplitude of these two terms varying from sample to sample. In the present paper, we expand this investigation to samples grown by multiple groups and show that indeed the co-existence of all anisotropy terms is a general property of (Ga,Mn)As, and that only the relative strength of the terms is characteristic of the layer growth.</p>
</sec-level1>
<sec-level1 id="nj268306s2" label="2"><heading>Anisotropy fingerprints</heading>
<p indent="no">All investigations are performed using Hall bars of the configuration shown in figure <figref linkend="nj268306fig1">1</figref>
(a) produced by standard optical lithography followed by chemically assisted ion beam etching (CAIBE). Magnetoresistance measurements are carried out in a magnetocryostat equipped with a vector field magnet capable of producing fields of up to 300 mT in any spatial direction. For the measurement discussed in this paper, fields are always applied in the plane of the sample, and the direction of the magnetic field is given by the angle <inline-eqn><math-text>&phis;</math-text>
</inline-eqn>
relative to the [100] crystal direction.</p>
<figure id="nj268306fig1" parts="single" width="column" position="float" pageposition="top" printstyle="normal" orientation="port"><graphic position="indented"><graphic-file version="print" format="EPS" width="26pc" printcolour="no" filename="images/nj268306fig1.eps"></graphic-file>
<graphic-file version="ej" format="JPEG" printcolour="yes" filename="images/nj268306fig1.jpg"></graphic-file>
</graphic>
<caption type="figure" id="nj268306fc1" label="Figure 1"><p indent="no">(a) Layout of the Hall bar used in the experiments. (b) Configuration for the simulation of a magnetoresistance scan along <inline-eqn><math-text>&phis;=70°</math-text>
</inline-eqn>
(c) showing the two switching events <inline-eqn><math-text><italic>H</italic>
<sub><italic>c</italic>
1</sub>
</math-text>
</inline-eqn>
and <inline-eqn><math-text><italic>H</italic>
<sub><italic>c</italic>
2</sub>
</math-text>
</inline-eqn>
corresponding to the two subsequent <inline-eqn><math-text>90°</math-text>
</inline-eqn>
domain wall propagation events. These data are then converted (d) to a sector of a resistance polar plot.</p>
</caption>
</figure>
<p>(Ga,Mn)As exhibits a strongly anisotropic magnetoresistance (AMR) where the resistivity <inline-eqn><math-text>ρ<sub>⊥</sub>
</math-text>
</inline-eqn>
for current flowing perpendicular to the direction of magnetization is larger than <inline-eqn><math-text>ρ<sub>∥</sub>
</math-text>
</inline-eqn>
for current along the magnetization [<cite linkend="nj268306bib12">12</cite>
]. As a result of this anisotropy in the resistivity tensor, the longitudinal resistivity <inline-eqn><math-text>ρ<sub><italic>xx</italic>
</sub>
</math-text>
</inline-eqn>
is given by [<cite linkend="nj268306bib13">13</cite>
, <cite linkend="nj268306bib14">14</cite>
]:
<display-eqn id="nj268306eqn1" textype="equation" notation="LaTeX" eqnnum="1"></display-eqn>
where <inline-eqn><math-text>ϑ</math-text>
</inline-eqn>
is the angle between the direction of magnetization and the current. Note that there is also a dependence of the resistivity on the angle between the direction of magnetization and the underlying crystal orientation [<cite linkend="nj268306bib15">15</cite>
]. This additional term modifies the resistivity value for a given magnetization direction, but does not affect the field position of the magnetization reorientation events, and can thus be neglected for the purposes of the present analysis.</p>
<p>For each sample, we measure the four terminal longitudinal resistance using the lead configuration given in figure <figref linkend="nj268306fig1">1</figref>
(a) by passing a current from the <inline-eqn><math-text><italic>I</italic>
<sub>+</sub>
</math-text>
</inline-eqn>
to the <inline-eqn><math-text><italic>I</italic>
<sub>−</sub>
</math-text>
</inline-eqn>
contacts, and measuring the voltage between <inline-eqn><math-text><italic>V</italic>
<sub>1</sub>
</math-text>
</inline-eqn>
and <inline-eqn><math-text><italic>V</italic>
<sub>2</sub>
</math-text>
</inline-eqn>
. We scan the magnetic field from <inline-eqn><math-text>−300</math-text>
</inline-eqn>
to <inline-eqn><math-text>+300 <upright>mT</upright>
</math-text>
</inline-eqn>
along a given direction <inline-eqn><math-text>&phis;</math-text>
</inline-eqn>
, and repeat this procedure for multiple angles. A simulation of such a scan for the case of <inline-eqn><math-text>&phis;=70°</math-text>
</inline-eqn>
is given in figure <figref linkend="nj268306fig1">1</figref>
(c), and shows two switching events, labeled <inline-eqn><math-text><italic>H</italic>
<sub><italic>c</italic>
1</sub>
</math-text>
</inline-eqn>
and <inline-eqn><math-text><italic>H</italic>
<sub><italic>c</italic>
2</sub>
</math-text>
</inline-eqn>
, associated with the two sequential <inline-eqn><math-text>90°</math-text>
</inline-eqn>
domain wall nucleation<inline-eqn><math-text>/</math-text>
</inline-eqn>
propagation events which account for the magnetization reversal in this material [<cite linkend="nj268306bib16">16</cite>
]. In order to analyze the data, the positive field half of each of these scans is converted to a sector of a polar plot as shown in figure <figref linkend="nj268306fig1">1</figref>
(d). The two switching events then show up as abrupt color changes as indicated in the figure. The compilation of all the sectors required for a full revolution produces an anisotropy fingerprint resistance polar plot such as the one simulated in figure <figref linkend="nj268306fig2">2</figref>
(a).</p>
<figure id="nj268306fig2" parts="single" width="column" position="float" pageposition="top" printstyle="normal" orientation="port"><graphic position="indented"><graphic-file version="print" format="EPS" width="22pc" printcolour="no" filename="images/nj268306fig2.eps"></graphic-file>
<graphic-file version="ej" format="JPEG" printcolour="yes" filename="images/nj268306fig2.jpg"></graphic-file>
</graphic>
<caption type="figure" id="nj268306fc2" label="Figure 2"><p indent="no">(a) Simulation of a full resistance polar plot comprised of sectors as in figure <figref linkend="nj268306fig1">1</figref>
. (b) Measurement of the inner region of the polar plot. The red ‘I’ indicates the direction of current flow during the measurement.</p>
</caption>
</figure>
<p>For the purposes of characterizing the various anisotropy terms, the most important part of the data is the innermost region whose boundaries are formed by the loci of first switching events (<inline-eqn><math-text><italic>H</italic>
<sub><italic>c</italic>
1</sub>
</math-text>
</inline-eqn>
). Figure <figref linkend="nj268306fig2">2</figref>
(b) shows a zoomed-in view of this region for an experimental measurement on a characteristic piece of (Ga,Mn)As.</p>
<p>For the model case of a purely biaxial anisotropy, this inner region would take the form of a perfect square with corners along the easy axis and the length of the half diagonal given by <inline-eqn><math-text>ϵ</math-text>
</inline-eqn>
, the domain wall nucleation<inline-eqn><math-text>/</math-text>
</inline-eqn>
propagation energy scales to the volume magnetization (figure <figref linkend="nj268306fig3">3</figref>
(a)). The inclusion of a uniaxial anisotropy bisecting two of the biaxial easy axes moves the resulting easy axes towards the direction of the uniaxial anisotropy [<cite linkend="nj268306bib17">17</cite>
] and elongates the square into a rectangle as schematically depicted in figure <figref linkend="nj268306fig3">3</figref>
(b). The strength of the uniaxial anisotropy constant in the [110] direction <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
</math-text>
</inline-eqn>
relative to the biaxial anisotropy constant <inline-eqn><math-text><italic>K</italic>
<sub><upright>biax</upright>
</sub>
</math-text>
</inline-eqn>
can be extracted from the angle <inline-eqn><math-text>δ</math-text>
</inline-eqn>
, as defined in figure <figref linkend="nj268306fig3">3</figref>
(b), by which the angle between two easy axes is modified. The relationship is given by [<cite linkend="nj268306bib11">11</cite>
]:
<display-eqn id="nj268306eqn2" textype="equation" notation="LaTeX" eqnnum="2"></display-eqn>
In practice, because the mixing of the anisotropy terms leads to a rectangle with open corners, it is often more convenient to work with the aspect ratio of the width (<inline-eqn><math-text><italic>W</italic>
</math-text>
</inline-eqn>
) to the length (<inline-eqn><math-text><italic>L</italic>
</math-text>
</inline-eqn>
) of the rectangle, instead of the angle <inline-eqn><math-text>δ</math-text>
</inline-eqn>
, which is related to the anisotropy terms as:
<display-eqn id="nj268306eqn3" textype="equation" notation="LaTeX" eqnnum="3"></display-eqn>
</p>
<figure id="nj268306fig3" parts="single" width="column" position="float" pageposition="top" printstyle="normal" orientation="port"><graphic position="indented"><graphic-file version="print" format="EPS" width="32pc" printcolour="no" filename="images/nj268306fig3.eps"></graphic-file>
<graphic-file version="ej" format="JPEG" printcolour="yes" filename="images/nj268306fig3.jpg"></graphic-file>
</graphic>
<caption type="figure" id="nj268306fc3" label="Figure 3"><p indent="no">Sketches of the expected shape of the inner region for (a) a sample with only a ([100] and [010]) biaxial anisotropy, (b) a sample with a biaxial plus a <inline-eqn></inline-eqn>
uniaxial easy axis and (c) a sample with a biaxial plus a [010] uniaxial easy axis. Note that the axes are in magnetic field units scaled to the volume magnetization (<italic>M</italic>
).</p>
</caption>
</figure>
<p>If a uniaxial anisotropy is instead added parallel to one of the biaxial easy axes, an asymmetry arises in the energy required to switch between the two biaxial easy axes. Essentially, the energy required to switch towards the easier of the two biaxial easy axes is less than that to switch towards the second biaxial. The inner pattern is then comprised of parts of an inner and an outer square, and the difference in the length of their half diagonal is a measure of <inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
</math-text>
</inline-eqn>
(figure <figref linkend="nj268306fig3">3</figref>
(c)), where <inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
</math-text>
</inline-eqn>
is the [010] anisotropy constant. Because of deformation of the fingerprint near the corners of the rectangle, which results from mixing of the anisotropy terms, it is often easier to identify the presence of an [010] uniaxial easy axis by looking at the spacing between the sides of the squares (or rectangles in the case that a [110] uniaxial term is also present), as indicated by the yellow line in figure <figref linkend="nj268306fig3">3</figref>
(c), which of course has a length equal to <inline-eqn></inline-eqn>
.</p>
</sec-level1>
<sec-level1 id="nj268306s3" label="3"><heading>Characteristics of a wafer</heading>
<p indent="no">We have previously shown [<cite linkend="nj268306bib11">11</cite>
] that the fingerprint technique can be used to characterize the properties of a given wafer, and for macroscopic-sized devices, the fingerprint is a signature of the underlying material. As an example of this, we present in figure <figref linkend="nj268306fig4">4</figref>
the fingerprints for two Hall bars patterned from different locations on the same (Ga,Mn)As wafer, and oriented orthogonal to each other. An inspection of both fingerprints shows that the pattern is identical, as would be expected from a homogeneous wafer. The colors are inverted because of the <inline-eqn><math-text>90°</math-text>
</inline-eqn>
difference in current orientation. Both fingerprints yield the values of 1 mT for <inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
/<italic>M</italic>
</math-text>
</inline-eqn>
, 18% for <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
/<italic>K</italic>
<sub><upright>biax</upright>
</sub>
</math-text>
</inline-eqn>
and 18 mT for <inline-eqn><math-text>ϵ/<italic>M</italic>
</math-text>
</inline-eqn>
.</p>
<figure id="nj268306fig4" parts="single" width="column" position="float" pageposition="top" printstyle="normal" orientation="port"><graphic position="indented"><graphic-file version="print" format="EPS" width="32pc" printcolour="no" filename="images/nj268306fig4.eps"></graphic-file>
<graphic-file version="ej" format="JPEG" printcolour="yes" filename="images/nj268306fig4.jpg"></graphic-file>
</graphic>
<caption type="figure" id="nj268306fc4" label="Figure 4"><p indent="no">Resistance polar plots taken at two different locations of the same (Ga,Mn)As layer.</p>
</caption>
</figure>
<p>Next, we demonstrate how this technique can also be used as a quality control process. Figure <figref linkend="nj268306fig5">5</figref>
shows three fingerprints from three pieces of the same (Ga,Mn)As layer, taken near the center of the 2 inch wafer, and 4 and 1 mm from the edge. Because of the geometry of the Würzburg MBE chamber, and given that the substrate is rotated during growth to enhance radial homogeneity, the uniformity of the sample is nearly perfect near the center and any fingerprint taken in that region is identical to that of figure <figref linkend="nj268306fig5">5</figref>
(a). From the figure, we see that the central part of the sample has rather typical values of 16% for <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
/<italic>K</italic>
<sub><upright>biax</upright>
</sub>
</math-text>
</inline-eqn>
, 0.7 mT for <inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
/<italic>M</italic>
</math-text>
</inline-eqn>
and 9.2 mT for <inline-eqn><math-text>ϵ/<italic>M</italic>
</math-text>
</inline-eqn>
. Because of nonlinearities in the molecular beam profile, stoichiometric deviations in the epilayer become significant near the edge of the wafer. The outermost 5 mm of samples are thus significantly less uniform. This area is normally discarded, and certainly not used for device studies. The fingerprint in figure <figref linkend="nj268306fig5">5</figref>
(c), taken on a piece 1 mm from the edge, very clearly shows why. It presents a fingerprint pattern very different from the homogeneous center, with an enormous discontinuity in the edges of the squares corresponding to a very large value of <inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
/<italic>M</italic>
=3.8 <upright>mT</upright>
</math-text>
</inline-eqn>
for the [010] uniaxial anisotropy term. This is well outside the range of what is found on the homogeneous part of any (Ga,Mn)As. The deformation is sufficient that it is impossible to reliably extract values <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
</math-text>
</inline-eqn>
or <inline-eqn><math-text>ϵ</math-text>
</inline-eqn>
. The fingerprint of figure <figref linkend="nj268306fig5">5</figref>
(b), on a piece 4 mm from the edge, is just outside the region that is normally considered usable. It has approximately the same value of <inline-eqn><math-text>ϵ</math-text>
</inline-eqn>
and <inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
</math-text>
</inline-eqn>
as the central part and is only slightly deformed with a smaller <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
/<italic>K</italic>
<sub><upright>biax</upright>
</sub>
</math-text>
</inline-eqn>
of 12%. These numbers are still within the typical range for (Ga,Mn)As, but show a change in layer properties as one approaches the edge.</p>
<figure id="nj268306fig5" parts="single" width="column" position="float" pageposition="top" printstyle="normal" orientation="port"><graphic position="indented"><graphic-file version="print" format="EPS" width="38pc" printcolour="no" filename="images/nj268306fig5.eps"></graphic-file>
<graphic-file version="ej" format="JPEG" printcolour="yes" filename="images/nj268306fig5.jpg"></graphic-file>
</graphic>
<caption type="figure" id="nj268306fc5" label="Figure 5"><p indent="no">Resistance polar plots taken (a) near the center of a (Ga,Ma)As wafer, (b) about 4 mm from the edge of the wafer and (c) about 1 mm from the edge.</p>
</caption>
</figure>
</sec-level1>
<sec-level1 id="nj268306s4" label="4"><heading>Comparison of wafers from multiple sources</heading>
<p indent="no">In order to confirm that the coexistence of both the [010] and [110] uniaxial anisotropy terms is not a particularity of (Ga,Mn)As grown in a certain MBE chamber or under particular conditions, but is indeed ubiquitous to the material, we now present the results of measurements performed on samples patterned from layers grown in various laboratories and thus under varied growth conditions.</p>
<p>Figure <figref linkend="nj268306fig4">4</figref>
shows fingerprints from a fairly typical layer grown in Würzburg, albeit one with a relatively large domain wall nucleation propagation energy. To illustrate the typical spread that can be expected, we present in figure <figref linkend="nj268306fig6">6</figref>
two additional Würzburg layers with rather pronounced [010] (figure <figref linkend="nj268306fig6">6</figref>
(a)) or [110] (figure <figref linkend="nj268306fig6">6</figref>
(b)), components. In figure <figref linkend="nj268306fig6">6</figref>
(c)–(f) we compare these to fingerprints on layers grown at IMEC, Nottingham, Tohoku, and Notre Dame. Values of the various parameters extracted from all these layers are given in table <tabref linkend="nj268306tab1">1</tabref>
. The figure illustrates that not only the amplitude, but also the sign of the two uniaxial components can vary between samples. For the [110] uniaxial, this change in sign can be seen by a <inline-eqn><math-text>90°</math-text>
</inline-eqn>
rotation of the long axis of the rectangle, whereas the sign of the [010] is determined by whether the quarter of the rectangle with its primary diagonal along [010] is larger or smaller than that with the diagonal along [100]. Note that the sign of the color scale (determining which regions are red and which are black) is determined by the direction of the current flow during the measurement, and is irrelevant to the current investigation.</p>
<figure id="nj268306fig6" parts="single" width="column" position="float" pageposition="top" printstyle="normal" orientation="port"><graphic position="indented"><graphic-file version="print" format="EPS" width="32pc" printcolour="no" filename="images/nj268306fig6.eps"></graphic-file>
<graphic-file version="ej" format="JPEG" printcolour="yes" filename="images/nj268306fig6.jpg"></graphic-file>
</graphic>
<caption type="figure" id="nj268306fc6" label="Figure 6"><p indent="no">Fingerprints from (Ga,Mn)As layers grown in various laboratories. (a) and (b) are layers grown in Würzburg with strong [010] and [110] easy axes, respectively. The other fingerprints are from layers grown at (c) IMEC, (d) Nottingham, (e) Tohoku and (f) Notre Dame.</p>
</caption>
</figure>
<table id="nj268306tab1" frame="topbot" position="float" width="fit" place="top"><caption type="table" id="nj268306tc1" label="Table 1"><p>Characterization parameters extracted from the anisotropy fingerprints on various layers.</p>
</caption>
<tgroup cols="4"><colspec colnum="1" colname="col1" align="left"></colspec>
<colspec colnum="2" colname="col2" align="center"></colspec>
<colspec colnum="3" colname="col3" align="center"></colspec>
<colspec colnum="4" colname="col4" align="center"></colspec>
<thead><row><entry></entry>
<entry><inline-eqn><math-text>ϵ/<italic>M</italic>
(<upright>mT</upright>
)</math-text>
</inline-eqn>
</entry>
<entry><inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
/<italic>K</italic>
<sub><upright>biax</upright>
</sub>
(%)</math-text>
</inline-eqn>
</entry>
<entry><inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
/<italic>M</italic>
(<upright>mT</upright>
)</math-text>
</inline-eqn>
</entry>
</row>
</thead>
<tbody><row><entry>Würzburg from figure <figref linkend="nj268306fig4">4</figref>
</entry>
<entry>18</entry>
<entry>18</entry>
<entry>1.0</entry>
</row>
<row><entry>Würzburg with large [010]</entry>
<entry>8.5</entry>
<entry>7</entry>
<entry>1.4</entry>
</row>
<row><entry>Würzburg with large [110]</entry>
<entry>12</entry>
<entry>21</entry>
<entry>0.7</entry>
</row>
<row><entry>IMEC</entry>
<entry>7.8</entry>
<entry>11</entry>
<entry>0.7</entry>
</row>
<row><entry>Nottingham</entry>
<entry>7.1</entry>
<entry>9</entry>
<entry>0.65</entry>
</row>
<row><entry>Tohoku</entry>
<entry>12</entry>
<entry>4</entry>
<entry>1.25</entry>
</row>
<row><entry>Notre Dame</entry>
<entry>16</entry>
<entry>9</entry>
<entry>0.75</entry>
</row>
</tbody>
</tgroup>
</table>
<p>As is clear from the table, all samples show a significant contribution of both a [110] and a [010] uniaxial anisotropy component. The values of the parameters that can be extracted from the fingerprints show variance from sample to sample, and typically fall in the range of some 7–18 mT for <inline-eqn><math-text>ϵ/<italic>M</italic>
</math-text>
</inline-eqn>
, 0.6–1.5 mT for <inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
/<italic>M</italic>
</math-text>
</inline-eqn>
and 4–20% for the ratio of <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
/<italic>K</italic>
<sub><upright>biax</upright>
</sub>
</math-text>
</inline-eqn>
. Note that while the fingerprint technique cannot be used to reliably extract exact values for <inline-eqn><math-text><italic>K</italic>
<sub><upright>biax</upright>
</sub>
</math-text>
</inline-eqn>
, the shape of the curve as the magnetization rotates away from the easy axis towards the external magnetic field at higher fields can be used to estimate the strength of <inline-eqn><math-text><italic>K</italic>
<sub><upright>biax</upright>
</sub>
/<italic>M</italic>
</math-text>
</inline-eqn>
. All samples investigated showed a value of approximately 100 mT for this parameter, which means that the values of <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
/<italic>K</italic>
<sub><upright>biax</upright>
</sub>
</math-text>
</inline-eqn>
quoted in percentage in the table are also estimates of <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
/<italic>M</italic>
</math-text>
</inline-eqn>
in mT.</p>
<p>While the table clearly shows significant variation from sample to sample, it nevertheless allows the extraction of useful rules of thumb for relative amplitude of the various terms. As a general statement, the ratio of <inline-eqn><math-text><italic>K</italic>
<sub><upright>biax</upright>
</sub>
: <italic>K</italic>
<sub>110</sub>
: <italic>K</italic>
<sub>010</sub>
</math-text>
</inline-eqn>
is of the order of <inline-eqn><math-text>100 : 10 : 1</math-text>
</inline-eqn>
, and the domain wall nucleation<inline-eqn><math-text>/</math-text>
</inline-eqn>
propagation energy is of the order of 10% of the biaxial anisotropy constant.</p>
<p>The range of values for <inline-eqn><math-text><italic>K</italic>
<sub>010</sub>
/<italic>M</italic>
</math-text>
</inline-eqn>
and <inline-eqn><math-text>ϵ/<italic>M</italic>
</math-text>
</inline-eqn>
seen in the samples discussed in this study is a fair representation of (Ga,Mn)As in general. The span of values for the <inline-eqn><math-text><italic>K</italic>
<sub>110</sub>
/<italic>K</italic>
<sub><upright>biax</upright>
</sub>
</math-text>
</inline-eqn>
ratio, which is already in the table larger than the other parameters, is however only a reflection of the subset of samples that we investigated. In general, this ratio can easily be tuned over a much larger range, for example as a function of hole concentration [<cite linkend="nj268306bib4">4</cite>
] or of temperature [<cite linkend="nj268306bib11">11</cite>
]. No systematic distinction is observed between samples from various sources.</p>
</sec-level1>
<sec-level1 id="nj268306s5" label="5"><heading>Conclusions</heading>
<p indent="no">In conclusion, we have used the anisotropy fingerprint technique to analyze the magnetic anisotropy properties of multiple (Ga,Mn)As layers. We have shown that this technique is a reliable means of characterizing a given layer and that it can be used as a quality control check of the growth. Moreover, we have examined pieces of (Ga,Mn)As grown in various laboratories around the world, and found that all samples exhibit three magnetic anisotropy components: a biaxial anisotropy along [100] and [010], a uniaxial along [110] (or <inline-eqn></inline-eqn>
) and a second uniaxial along [100] (or [010]), showing that the existence of all three terms is an inherent property of (Ga,Mn)As and that it is only the relative strength of the terms which varies from sample to sample. As a rough rule of thumb, the ratio of the biaxial anisotropy, the [110] uniaxial and the [010] uniaxial is of the order of <inline-eqn><math-text>100 : 10 : 1</math-text>
</inline-eqn>
.</p>
</sec-level1>
<acknowledgment><heading>Acknowledgments</heading>
<p indent="no">We thank S Hümpfner and V Hock for sample preparation and we acknowledge the financial support from the EU (NANOSPIN FP6-IST-015728) and the National Science Foundation (USA) grant DMR06-03752.</p>
</acknowledgment>
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<mods version="3.6"><titleInfo lang="eng"><title>An extensive comparison of anisotropies in MBE grown (Ga,Mn)As material</title>
</titleInfo>
<titleInfo type="abbreviated"><title>An extensive comparison of anisotropies in MBE grown (Ga,Mn)As material</title>
</titleInfo>
<titleInfo type="alternative" lang="eng"><title>An extensive comparison of anisotropies in MBE grown (Ga,Mn)As material</title>
</titleInfo>
<name type="personal"><namePart type="given">C</namePart>
<namePart type="family">Gould</namePart>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
<affiliation>Author to whom any correspondence should be addressed.</affiliation>
<affiliation>E-mail: gould@physik.uni-wuerzburg.de</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">S</namePart>
<namePart type="family">Mark</namePart>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">K</namePart>
<namePart type="family">Pappert</namePart>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">R G</namePart>
<namePart type="family">Dengel</namePart>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">J</namePart>
<namePart type="family">Wenisch</namePart>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">R P</namePart>
<namePart type="family">Campion</namePart>
<affiliation>School of Physics and Astronomy, University of Nottingham, Nottingham NG7 2RD, UK</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">A W</namePart>
<namePart type="family">Rushforth</namePart>
<affiliation>School of Physics and Astronomy, University of Nottingham, Nottingham NG7 2RD, UK</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">D</namePart>
<namePart type="family">Chiba</namePart>
<affiliation>Semiconductor Spintronics Project, Exploratory Research for Advanced Technology, Japan Science and Technology Agency, Kitamemachi 1-18, Aoba-ku, Sendai 980-0023, Japan</affiliation>
<affiliation>Laboratory for Nanoelectronics and Spintronics, Research Institute of Electrical Communication, Tohoku University, Katahira 2-1-1, Aoba-ku, Sendai 980-8577, Japan</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">Z</namePart>
<namePart type="family">Li</namePart>
<affiliation>IMEC, Kapeldreef 75, B-3001 Leuven, Belgium</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">X</namePart>
<namePart type="family">Liu</namePart>
<affiliation>Department of Physics, University of Notre Dame, Notre Dame, IN 46556, USA</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">W</namePart>
<namePart type="family">Van Roy</namePart>
<affiliation>IMEC, Kapeldreef 75, B-3001 Leuven, Belgium</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">H</namePart>
<namePart type="family">Ohno</namePart>
<affiliation>Laboratory for Nanoelectronics and Spintronics, Research Institute of Electrical Communication, Tohoku University, Katahira 2-1-1, Aoba-ku, Sendai 980-8577, Japan</affiliation>
<affiliation>Semiconductor Spintronics Project, Exploratory Research for Advanced Technology, Japan Science and Technology Agency, Kitamemachi 1-18, Aoba-ku, Sendai 980-0023, Japan</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">J K</namePart>
<namePart type="family">Furdyna</namePart>
<affiliation>Department of Physics, University of Notre Dame, Notre Dame, IN 46556, USA</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">B</namePart>
<namePart type="family">Gallagher</namePart>
<affiliation>School of Physics and Astronomy, University of Nottingham, Nottingham NG7 2RD, UK</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">K</namePart>
<namePart type="family">Brunner</namePart>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">G</namePart>
<namePart type="family">Schmidt</namePart>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">L W</namePart>
<namePart type="family">Molenkamp</namePart>
<affiliation>Physikalisches Institut (EP3), Universitt Wrzburg, Am Hubland, D-97074 Wrzburg, Germany</affiliation>
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<copyrightDate encoding="w3cdtf">2008</copyrightDate>
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<abstract>This paper reports on a detailed magnetotransport investigation of the magnetic anisotropies of (Ga,Mn)As layers produced by various sources worldwide. Using anisotropy fingerprints to identify the contributions of the various higher-order anisotropy terms, we show that the presence of both a [100] and a [110] uniaxial anisotropy in addition to the primary ([100] [010]) anisotropy is common to all medium doped (Ga,Mn)As layers typically used in transport measurement, with the amplitude of these uniaxial terms being characteristic of the individual layers.</abstract>
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<titleInfo type="abbreviated"><title>New J. Phys.</title>
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<identifier type="ISSN">1367-2630</identifier>
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<part><date>2008</date>
<detail type="volume"><caption>vol.</caption>
<number>10</number>
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<detail type="issue"><caption>no.</caption>
<number>5</number>
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<extent unit="pages"><start>1</start>
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