Performance of SOFC coupled with n-C4H10 autothermal reformer: Carbon deposition and development of anode structure
Identifieur interne : 000621 ( PascalFrancis/Curation ); précédent : 000620; suivant : 000622Performance of SOFC coupled with n-C4H10 autothermal reformer: Carbon deposition and development of anode structure
Auteurs : Gyujong Bae [Corée du Sud] ; Joongmyeon Bae [Corée du Sud] ; Pattaraporn Kim-Lohsoontorn [Corée du Sud, Thaïlande] ; Jihoon Jeong [Corée du Sud]Source :
- International journal of hydrogen energy [ 0360-3199 ] ; 2010.
Descripteurs français
- Pascal (Inist)
- Performance, Pile combustible, Pile combustible oxyde solide, Anode, Nickel, Zircone, Oxyde de zirconium, Lanthane, Reformage vapeur, Oxydation partielle, Vapeur eau, Hydrocarbure, Mélange gaz, Conductivité électrique, Oxyde de cérium, Cobalt, Ferrite, Samarium, Catalyseur, Rhodium, Processus reformage autothermique, Hydrogène.
- Wicri :
- topic : Nickel, Hydrocarbure, Cobalt, Hydrogène.
English descriptors
- KwdEn :
- Anode, Autothermal reformer processes, Catalyst, Cerium oxide, Cobalt, Electrical conductivity, Ferrite, Fuel cell, Gas mixture, Hydrocarbon, Hydrogen, Lanthanum, Nickel, Partial oxidation, Performance, Rhodium, Samarium, Solid oxide fuel cell, Steam reforming, Water vapor, Zirconia, Zirconium oxide.
Abstract
The performance deterioration of solid oxide fuel cells (SOFCs, Nickel-Yttria stabilized zirconia (Ni-YSZ)/YSZ/lanthanum doped strontium manganite-YSZ (LSM-YSZ)) coupled with n-C4H10 steam reformers (SR), autothermal reformers (ATR), or catalytic partial oxidation reformers (CPOX) was examined using an integrated system of a micro-reactor reformer and SOFC unit. The terminal voltage rapidly degraded in CPOX-driven SOFC (oxygen to carbon ratio (OCR) = 0.5) while it was fairly stable for SR-driven SOFC (steam to carbon ratio (SCR) = 2) over 250 h. For ATR-driven SOFC at near the thermoneutral point (OCR = 0.5 and steam to carbon ration (SCR) = 1.3), significant deterioration of the terminal voltage was observed in 100 h of operation. The main precursors of carbon deposition on the SOFC were identified by reformate gas analysis during the tests. In this study, we reveal that the carbon deposition on the SOFC anode can be affected by not only lower-order hydrocarbons (C1C4), but also by the CO/H2 gas mixture. The change in electrical conductivity of the Ni-YSZ cermet used for the SOFC anode was investigated under different gas mixtures. To investigate the propensity for carbon deposition by each carbon-containing gas mixture, we defined the ratios of steam to specific carbon (C1C4 lower-order hydrocarbons and CO) in the reformate gas (SSCR, steam to specific carbon ratio). To inhibit carbon deposition on SOFC anode, the SSCR must be sufficiently high. However, the reformer operates near its maximum efficiency at low SSCR value and the higher the SSCR value, the lower the open circuit voltage and operating power density due to Nernst potential. In this study, a metal-foam supported SOFC single cell (Ni-YSZ/YSZ/Gd-doped ceria (CGO) buffer layer/lanthanum strontium cobalt ferrite-samarium doped ceria (LSCF-SDC)), impregnated with catalyst was designed; this novel SOFC was then examined for operation at a low SSCR value of the autothermal reformer conditions (near maximum efficiency of n-C4H10 reformer and thermal neutral point, SSCR = 0.5, OCR = 0.5 and SCR = 1.3). The voltage for the metal-foam supported SOFC impregnated with 0.5 wt% Rh/ CGO remained at a nearly constant value, around 0.8 V, for 200 h under a constant temperature of 750 °C and current load of 250 mA cm-2.
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H<sub>10</sub>
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<term>Cerium oxide</term>
<term>Cobalt</term>
<term>Electrical conductivity</term>
<term>Ferrite</term>
<term>Fuel cell</term>
<term>Gas mixture</term>
<term>Hydrocarbon</term>
<term>Hydrogen</term>
<term>Lanthanum</term>
<term>Nickel</term>
<term>Partial oxidation</term>
<term>Performance</term>
<term>Rhodium</term>
<term>Samarium</term>
<term>Solid oxide fuel cell</term>
<term>Steam reforming</term>
<term>Water vapor</term>
<term>Zirconia</term>
<term>Zirconium oxide</term>
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<term>Pile combustible</term>
<term>Pile combustible oxyde solide</term>
<term>Anode</term>
<term>Nickel</term>
<term>Zircone</term>
<term>Oxyde de zirconium</term>
<term>Lanthane</term>
<term>Reformage vapeur</term>
<term>Oxydation partielle</term>
<term>Vapeur eau</term>
<term>Hydrocarbure</term>
<term>Mélange gaz</term>
<term>Conductivité électrique</term>
<term>Oxyde de cérium</term>
<term>Cobalt</term>
<term>Ferrite</term>
<term>Samarium</term>
<term>Catalyseur</term>
<term>Rhodium</term>
<term>Processus reformage autothermique</term>
<term>Hydrogène</term>
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<front><div type="abstract" xml:lang="en">The performance deterioration of solid oxide fuel cells (SOFCs, Nickel-Yttria stabilized zirconia (Ni-YSZ)/YSZ/lanthanum doped strontium manganite-YSZ (LSM-YSZ)) coupled with n-C<sub>4</sub>
H<sub>10</sub>
steam reformers (SR), autothermal reformers (ATR), or catalytic partial oxidation reformers (CPOX) was examined using an integrated system of a micro-reactor reformer and SOFC unit. The terminal voltage rapidly degraded in CPOX-driven SOFC (oxygen to carbon ratio (OCR) = 0.5) while it was fairly stable for SR-driven SOFC (steam to carbon ratio (SCR) = 2) over 250 h. For ATR-driven SOFC at near the thermoneutral point (OCR = 0.5 and steam to carbon ration (SCR) = 1.3), significant deterioration of the terminal voltage was observed in 100 h of operation. The main precursors of carbon deposition on the SOFC were identified by reformate gas analysis during the tests. In this study, we reveal that the carbon deposition on the SOFC anode can be affected by not only lower-order hydrocarbons (C<sub>1</sub>
C<sub>4</sub>
), but also by the CO/H<sub>2</sub>
gas mixture. The change in electrical conductivity of the Ni-YSZ cermet used for the SOFC anode was investigated under different gas mixtures. To investigate the propensity for carbon deposition by each carbon-containing gas mixture, we defined the ratios of steam to specific carbon (C<sub>1</sub>
C<sub>4</sub>
lower-order hydrocarbons and CO) in the reformate gas (SSCR, steam to specific carbon ratio). To inhibit carbon deposition on SOFC anode, the SSCR must be sufficiently high. However, the reformer operates near its maximum efficiency at low SSCR value and the higher the SSCR value, the lower the open circuit voltage and operating power density due to Nernst potential. In this study, a metal-foam supported SOFC single cell (Ni-YSZ/YSZ/Gd-doped ceria (CGO) buffer layer/lanthanum strontium cobalt ferrite-samarium doped ceria (LSCF-SDC)), impregnated with catalyst was designed; this novel SOFC was then examined for operation at a low SSCR value of the autothermal reformer conditions (near maximum efficiency of n-C<sub>4</sub>
H<sub>10</sub>
reformer and thermal neutral point, SSCR = 0.5, OCR = 0.5 and SCR = 1.3). The voltage for the metal-foam supported SOFC impregnated with 0.5 wt% Rh/ CGO remained at a nearly constant value, around 0.8 V, for 200 h under a constant temperature of 750 °C and current load of 250 mA cm<sup>-2</sup>
.</div>
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H<sub>10</sub>
steam reformers (SR), autothermal reformers (ATR), or catalytic partial oxidation reformers (CPOX) was examined using an integrated system of a micro-reactor reformer and SOFC unit. The terminal voltage rapidly degraded in CPOX-driven SOFC (oxygen to carbon ratio (OCR) = 0.5) while it was fairly stable for SR-driven SOFC (steam to carbon ratio (SCR) = 2) over 250 h. For ATR-driven SOFC at near the thermoneutral point (OCR = 0.5 and steam to carbon ration (SCR) = 1.3), significant deterioration of the terminal voltage was observed in 100 h of operation. The main precursors of carbon deposition on the SOFC were identified by reformate gas analysis during the tests. In this study, we reveal that the carbon deposition on the SOFC anode can be affected by not only lower-order hydrocarbons (C<sub>1</sub>
C<sub>4</sub>
), but also by the CO/H<sub>2</sub>
gas mixture. The change in electrical conductivity of the Ni-YSZ cermet used for the SOFC anode was investigated under different gas mixtures. To investigate the propensity for carbon deposition by each carbon-containing gas mixture, we defined the ratios of steam to specific carbon (C<sub>1</sub>
C<sub>4</sub>
lower-order hydrocarbons and CO) in the reformate gas (SSCR, steam to specific carbon ratio). To inhibit carbon deposition on SOFC anode, the SSCR must be sufficiently high. However, the reformer operates near its maximum efficiency at low SSCR value and the higher the SSCR value, the lower the open circuit voltage and operating power density due to Nernst potential. In this study, a metal-foam supported SOFC single cell (Ni-YSZ/YSZ/Gd-doped ceria (CGO) buffer layer/lanthanum strontium cobalt ferrite-samarium doped ceria (LSCF-SDC)), impregnated with catalyst was designed; this novel SOFC was then examined for operation at a low SSCR value of the autothermal reformer conditions (near maximum efficiency of n-C<sub>4</sub>
H<sub>10</sub>
reformer and thermal neutral point, SSCR = 0.5, OCR = 0.5 and SCR = 1.3). The voltage for the metal-foam supported SOFC impregnated with 0.5 wt% Rh/ CGO remained at a nearly constant value, around 0.8 V, for 200 h under a constant temperature of 750 °C and current load of 250 mA cm<sup>-2</sup>
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<s5>13</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Steam reforming</s0>
<s5>13</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Reformación vapor</s0>
<s5>13</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Oxydation partielle</s0>
<s5>14</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Partial oxidation</s0>
<s5>14</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Oxidación parcial</s0>
<s5>14</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Vapeur eau</s0>
<s5>15</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Water vapor</s0>
<s5>15</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Vapor agua</s0>
<s5>15</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Hydrocarbure</s0>
<s2>FX</s2>
<s5>16</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Hydrocarbon</s0>
<s2>FX</s2>
<s5>16</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Hidrocarburo</s0>
<s2>FX</s2>
<s5>16</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Mélange gaz</s0>
<s5>17</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Gas mixture</s0>
<s5>17</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Mezcla gas</s0>
<s5>17</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>Conductivité électrique</s0>
<s5>18</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>Electrical conductivity</s0>
<s5>18</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Conductividad eléctrica</s0>
<s5>18</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Oxyde de cérium</s0>
<s5>19</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG"><s0>Cerium oxide</s0>
<s5>19</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA"><s0>Cerio óxido</s0>
<s5>19</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>Cobalt</s0>
<s2>NC</s2>
<s5>20</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG"><s0>Cobalt</s0>
<s2>NC</s2>
<s5>20</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA"><s0>Cobalto</s0>
<s2>NC</s2>
<s5>20</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Ferrite</s0>
<s5>21</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG"><s0>Ferrite</s0>
<s5>21</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA"><s0>Ferrita</s0>
<s5>21</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Samarium</s0>
<s2>NC</s2>
<s5>22</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Samarium</s0>
<s2>NC</s2>
<s5>22</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Samario</s0>
<s2>NC</s2>
<s5>22</s5>
</fC03>
<fC03 i1="19" i2="X" l="FRE"><s0>Catalyseur</s0>
<s5>23</s5>
</fC03>
<fC03 i1="19" i2="X" l="ENG"><s0>Catalyst</s0>
<s5>23</s5>
</fC03>
<fC03 i1="19" i2="X" l="SPA"><s0>Catalizador</s0>
<s5>23</s5>
</fC03>
<fC03 i1="20" i2="X" l="FRE"><s0>Rhodium</s0>
<s2>NC</s2>
<s5>24</s5>
</fC03>
<fC03 i1="20" i2="X" l="ENG"><s0>Rhodium</s0>
<s2>NC</s2>
<s5>24</s5>
</fC03>
<fC03 i1="20" i2="X" l="SPA"><s0>Rodio</s0>
<s2>NC</s2>
<s5>24</s5>
</fC03>
<fC03 i1="21" i2="3" l="FRE"><s0>Processus reformage autothermique</s0>
<s5>25</s5>
</fC03>
<fC03 i1="21" i2="3" l="ENG"><s0>Autothermal reformer processes</s0>
<s5>25</s5>
</fC03>
<fC03 i1="22" i2="X" l="FRE"><s0>Hydrogène</s0>
<s2>NC</s2>
<s5>26</s5>
</fC03>
<fC03 i1="22" i2="X" l="ENG"><s0>Hydrogen</s0>
<s2>NC</s2>
<s5>26</s5>
</fC03>
<fC03 i1="22" i2="X" l="SPA"><s0>Hidrógeno</s0>
<s2>NC</s2>
<s5>26</s5>
</fC03>
<fN21><s1>059</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
</standard>
</inist>
</record>
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