Complete 1H- and 13C-n.m.r. assignments for two sulphated oligosaccharide alditols of hen ovomucin
Identifieur interne : 000395 ( France/Analysis ); précédent : 000394; suivant : 000396Complete 1H- and 13C-n.m.r. assignments for two sulphated oligosaccharide alditols of hen ovomucin
Auteurs : Gérard Strecker [France] ; Jean-Michel Wieruszeski [France] ; Claude Martel [France] ; Jean Montreuil [France]Source :
- Carbohydrate Research [ 0008-6215 ] ; 1988.
Abstract
The complete 1H- and 13C-n.m.r. assignments for β-d-Galp-(1→4)-β-d-GlcpNAc-6-SO3H-(1→6)-[β-d-Galp- (1→3)]-d-GalNAcol and α-NeuAcp-(2→3)-β-d-Galp-(1→3)-[β-d-Galp-(1→4)-β-d-GlcpNAc-6-SO3H-(1→6)]-d-GalNAcol were made by a combination of 2-D correlation experiments (Relayed-Cosy; and 13C, 1H Correlation-shift n.m.r. spectroscopy), and 1-D n.m.r. spectroscopy. The results illustrate the ability of these methods to locate sulphate and NeuAc groups in anionic mucinous glycoproteins.
Url:
DOI: 10.1016/0008-6215(89)84016-9
Affiliations:
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